Solid-State NMR III Organic Matter

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Publisher : Springer Science & Business Media
ISBN 13 : 3642612237
Total Pages : 218 pages
Book Rating : 4.6/5 (426 download)

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Book Synopsis Solid-State NMR III Organic Matter by : Bernhard Blümich

Download or read book Solid-State NMR III Organic Matter written by Bernhard Blümich and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 218 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.

Solid-State NMR III Organic Matter

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Publisher : Springer
ISBN 13 : 9783642647512
Total Pages : 0 pages
Book Rating : 4.6/5 (475 download)

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Book Synopsis Solid-State NMR III Organic Matter by : Bernhard Blümich

Download or read book Solid-State NMR III Organic Matter written by Bernhard Blümich and published by Springer. This book was released on 2011-09-28 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.

Solid-State NMR III Organic Matter

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Author :
Publisher : Springer
ISBN 13 : 9783540573999
Total Pages : 213 pages
Book Rating : 4.5/5 (739 download)

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Book Synopsis Solid-State NMR III Organic Matter by :

Download or read book Solid-State NMR III Organic Matter written by and published by Springer. This book was released on 1994-11-04 with total page 213 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.

Solid-State NMR III Organic Matter

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Author :
Publisher : Springer
ISBN 13 : 9783540573999
Total Pages : 0 pages
Book Rating : 4.5/5 (739 download)

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Book Synopsis Solid-State NMR III Organic Matter by : Bernhard Blümich

Download or read book Solid-State NMR III Organic Matter written by Bernhard Blümich and published by Springer. This book was released on 1994-11-04 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.

Solid-State NMR I Methods

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Author :
Publisher : Springer
ISBN 13 : 9783540571896
Total Pages : 282 pages
Book Rating : 4.5/5 (718 download)

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Book Synopsis Solid-State NMR I Methods by : B. Blümich

Download or read book Solid-State NMR I Methods written by B. Blümich and published by Springer. This book was released on 1993-12-21 with total page 282 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Solid-State NMR and Organic Geochemistry

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Author :
Publisher : Elsevier
ISBN 13 : 9780128195741
Total Pages : 710 pages
Book Rating : 4.1/5 (957 download)

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Book Synopsis Solid-State NMR and Organic Geochemistry by : Jingdong Mao

Download or read book Solid-State NMR and Organic Geochemistry written by Jingdong Mao and published by Elsevier. This book was released on 2021-11-15 with total page 710 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR and Organic Geochemistry explains solid-state NMR from the point of view of organic geochemists interested in applying solid-state NMR in their research. The book sets the scene in the first two chapters by describing the basic concepts of solid-state NMR adapted for non-NMR specialists as well as an overview of organic geochemistry for NMR specialists. The essentials for acquiring reliable spectra of complex organic matter are then described in Chapter 3. Chapter 4 introduces the systematic and advanced solid-state NMR techniques and approach to characterizing complex organic mixtures developed in Dr. Mao's laboratory. Practical aspects of performing solid-state NMR experiments of complex organic matter are discussed in Chapter 5. Chapters 6 through 15 are focused on applications of solid-state NMR in organic geochemistry, starting with geochemically important functional groups and biopolymers, followed by organic matter from soils, water, sediments, and aerosols, peat, coal, kerogen, and oil shale. The interactions of organic matter with organic contaminants probed by solid-state NMR are described in Chapter 16. Finally, the last chapter covers isotopic enrichment and labelling and solid-state NMR, and their applications in organic geochemistry. Bridges the gap between NMR specialists and organic geochemists, adapting solid-state NMR theory for non-NMR specialists Brings together NMR applications for a range of materials not often discussed in other NMR books, including applications to soil, aerosols, peat, coal, kerogen, and more Includes additional resources for further reading and problems to facilitate learning and application of key concepts in each chapter

Solid-state NMR Analysis of Soil Organic Matter Fractions from Integrated Physical-chemical Extraction

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Author :
Publisher :
ISBN 13 :
Total Pages : 11 pages
Book Rating : 4.:/5 (77 download)

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Book Synopsis Solid-state NMR Analysis of Soil Organic Matter Fractions from Integrated Physical-chemical Extraction by : Xiaoyan Cao

Download or read book Solid-state NMR Analysis of Soil Organic Matter Fractions from Integrated Physical-chemical Extraction written by Xiaoyan Cao and published by . This book was released on 2011 with total page 11 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Solid State NMR

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Author :
Publisher : John Wiley & Sons
ISBN 13 : 352731816X
Total Pages : 562 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Solid State NMR by : Klaus Müller

Download or read book Solid State NMR written by Klaus Müller and published by John Wiley & Sons. This book was released on 2021-08-23 with total page 562 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences. Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook: Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopy Provides helpful illustrations to explain the various SSNMR concepts and methods Features accessible descriptive text with self-consistent use of quantum mechanics Covers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequences Contains references to relevant literature Solid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.

Solid-State NMR IV Methods and Applications of Solid-State NMR

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Author :
Publisher : Springer Science & Business Media
ISBN 13 : 3642791271
Total Pages : 210 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Solid-State NMR IV Methods and Applications of Solid-State NMR by : B. Blümich

Download or read book Solid-State NMR IV Methods and Applications of Solid-State NMR written by B. Blümich and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 210 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance at NMR meetings, approaching that ofliquid state resonance. Important progress can be observed in the areas of methodological developments and applications to organic and inorganic matter. One volume devoted to more or less one of each of these areas has been published in the preceding three issues. This volume can be considered an addendum to this series. Selected methods and applications of Solid-State NMR are featured in three chapters. The first one treats the recoupling of dipolar interactions in solids, which are averaged by fast sample rotation. Following an introduction to effective Hamiltonians and Floquet theory, different types of experiment such as rotary resonance, dipolar chemical shift correlation spectroscopy, rotational resonance and multipulse recoupling are treated in the powerful Floquet formalism. In the second chapter, the different approaches to line narrowing of quadrupolar nuclei are reviewed in a. consistent formulation of double resonance (DaR) and dynamic angle spinning (DAS). Practical aspects of probe design are considered as well as advanced 2D experiments, sensitivity enhancement techniques, and spinning sideband manipulations. The use of such techniques dramatically increases the number of nuclei which can be probed in high resolution NMR spectroscopy. The final chapter describes new experimental approaches and results of structural studies of noncrystalline solids.

Modern Methods in Solid-state NMR

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Author :
Publisher : Royal Society of Chemistry
ISBN 13 : 1788014197
Total Pages : 452 pages
Book Rating : 4.7/5 (88 download)

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Book Synopsis Modern Methods in Solid-state NMR by : Paul Hodgkinson

Download or read book Modern Methods in Solid-state NMR written by Paul Hodgkinson and published by Royal Society of Chemistry. This book was released on 2018-04-05 with total page 452 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques. In this unique volume, a range of experts in different areas of modern solid-state NMR explain about their area of expertise, emphasising the “practical aspects” of implementing different techniques, and illustrating what questions can and cannot be addressed. Later chapters address complex materials, showing how different NMR techniques discussed in earlier chapters can be brought together to characterise important materials types. The volume as a whole focusses on topics relevant to the developing field of “NMR crystallography” – the use of solids NMR as a complement to diffraction crystallography. This book is an ideal complement to existing introductory texts and reviews on solid-state NMR. New researchers wanting to understand new areas of solid-state NMR will find each chapter to be the equivalent to spending time in the laboratory of an internationally leading expert, learning the hints and tips that make the difference between knowing about a technique and being ready to put it into action. With no equivalent on the market, it will be of interest to every solid-state NMR researcher (academic and postgraduate) working in the chemical sciences.

Solid-State NMR in Materials Science

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Publisher : CRC Press
ISBN 13 : 1439869634
Total Pages : 283 pages
Book Rating : 4.4/5 (398 download)

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Book Synopsis Solid-State NMR in Materials Science by : Vladimir I. Bakhmutov

Download or read book Solid-State NMR in Materials Science written by Vladimir I. Bakhmutov and published by CRC Press. This book was released on 2011-12-19 with total page 283 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-state NMR is a powerful physical method widely applied in modern fundamental and applied science, medicine, and industry. Its role is particularly valuable in materials chemistry due to the capability of solid-state NMR to rapidly solve tasks connected with structural descriptions of complex systems on macro and/or molecular levels, and the identification of the dynamics often responsible for complex systems mechanical properties. Written for non-specialists, Solid-State NMR in Materials Science: Principles and Applications introduces the general physical principles of pulsed NMR, by including elements of the theory and practice in the registration of NMR signals, and by explaining different NMR equipment. After the preliminaries, the book covers: The theory and features of solid-state NMR and nuclear relaxation in solids, including dynamics of materials Different materials, diamagnetic and paramagnetic, from metals and metal clusters to amorphous composites The methodology of collection and interpretations of solid-state NMR data, including strategies and criteria for structural characterizations of different materials Practical examples of multinuclear NMR and relaxation experiments as well as interpretations of data obtained Numerous solid-state NMR experiments performed for various materials to evaluate their structure and dynamics Written in clear and simple language, this book includes clear illustrations, numerous examples, and detailed bibliographies. It an excellent reference not only for young and experienced researchers, but also for students interested in a future in materials science.

Characterization of Soil Organic Matter by High-resolution Solid-state Carbon-13 Nuclear Magnetic Resonance Spectroscopy

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Publisher :
ISBN 13 : 9780549022695
Total Pages : 104 pages
Book Rating : 4.0/5 (226 download)

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Book Synopsis Characterization of Soil Organic Matter by High-resolution Solid-state Carbon-13 Nuclear Magnetic Resonance Spectroscopy by : Michael Schilling

Download or read book Characterization of Soil Organic Matter by High-resolution Solid-state Carbon-13 Nuclear Magnetic Resonance Spectroscopy written by Michael Schilling and published by . This book was released on 2004 with total page 104 pages. Available in PDF, EPUB and Kindle. Book excerpt: Soil organic matter (SOM) is the largest reservoir of organic carbon at the earth's surface. Its chemistry plays a crucial role in a wide range of issues including agricultural sustainability, pollution/contamination, and medicine. For instance, SOM is vital to soil fertility by affecting physical and chemical properties of soil and in controlling soil microbial activity by serving as a source for mineralizable C and N. Soil organic matter is also very influential in the transport and fate of organic and inorganic anthropogenic chemicals because of its heterogeneity and highly functionalized nature. Therefore, an understanding of SOM at the molecular level is a critical and worthwhile undertaking.

Multidimensional Solid-State NMR and Polymers

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Publisher : Elsevier
ISBN 13 : 0080925626
Total Pages : 501 pages
Book Rating : 4.0/5 (89 download)

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Book Synopsis Multidimensional Solid-State NMR and Polymers by : Klaus Schmidt-Rohr

Download or read book Multidimensional Solid-State NMR and Polymers written by Klaus Schmidt-Rohr and published by Elsevier. This book was released on 2012-12-02 with total page 501 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy is the most valuable and versatile analytical tool in chemistry. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better understanding of materials properties on the molecular level.Dramatic progress-much of it pioneered by the authors-has been achieved in this area, especially in synthetic polymers. Solid-state NMR now favorably competes with well-established techniques, such as light, x-ray, or neutron scattering, electron microscopy, and dielectric and mechanical relaxation.The application of multidimensional solid-state NMR inevitably involves use of concepts from different fields of science. This book also provides the first comprehensive treatment of both the new experimental techniques and the theoretical concepts needed in more complex data analysis. The text addresses spectroscopists and polymer scientists by treating the subject on different levels; descriptive, technical, and mathematical approaches are used when appropriate. It presents an overview of new developments with numerous experimental examples and illustrations, which will appeal to readers interested in both the information content as well as the potential of solid-state NMR. The book also contains many previously unpublished details that will be appreciated by those who want to perform the experiments. The techniques described are applicable not only to the study of synthetic polymers but to numerous problems in solid-state physics, chemistry, materials science, and biophysics. Presents original theories and new perspectives on scattering techniques Provides a systematic treatment of the whole subject Gives readers access to previously unpublished material Includes extensive illustrations

Nuclear Magnetic Resonance

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Publisher : Royal Society of Chemistry
ISBN 13 : 1847553818
Total Pages : 564 pages
Book Rating : 4.8/5 (475 download)

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Book Synopsis Nuclear Magnetic Resonance by : G A Webb

Download or read book Nuclear Magnetic Resonance written by G A Webb and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

Characterisation of Sedimentary Fossil Organic Matter Using Solid-state 13C NMR Spectroscopy and Sequential Degredation Techniques

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Publisher :
ISBN 13 :
Total Pages : 0 pages
Book Rating : 4.:/5 (141 download)

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Book Synopsis Characterisation of Sedimentary Fossil Organic Matter Using Solid-state 13C NMR Spectroscopy and Sequential Degredation Techniques by : Gordon D. Love

Download or read book Characterisation of Sedimentary Fossil Organic Matter Using Solid-state 13C NMR Spectroscopy and Sequential Degredation Techniques written by Gordon D. Love and published by . This book was released on 1994 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Solid-State NMR II

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Publisher : Springer Science & Business Media
ISBN 13 : 3642500498
Total Pages : 220 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis Solid-State NMR II by : B. Blümich

Download or read book Solid-State NMR II written by B. Blümich and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 220 pages. Available in PDF, EPUB and Kindle. Book excerpt: 1. G. Engelhardt, H. Koller, Stuttgart, FRG: 29Si NMR of Inorganic Solids 2. H. Pfeifer, Leizpig, FRG: NMR of Solid Surfaces 3. A. Sebald, Bayreuth, FRG: MAS and CP/MAS NMR of Less Common Spin-1/2 Nuclei 4. C. J{ger, Mainz, FRG: Satellite Transition Spectroscopy of Quadrupolar Nuclei 5. D. Brinkmann, M. Mali, Z}rich, CH: NMR-NQR Studies of High-Temperature Superconductors.

Nuclear Magnetic Resonance

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Author :
Publisher : Royal Society of Chemistry
ISBN 13 : 0854043373
Total Pages : 518 pages
Book Rating : 4.8/5 (54 download)

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Book Synopsis Nuclear Magnetic Resonance by : A. E. Aliev

Download or read book Nuclear Magnetic Resonance written by A. E. Aliev and published by Royal Society of Chemistry. This book was released on 2002 with total page 518 pages. Available in PDF, EPUB and Kindle. Book excerpt: For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.