Single Crystal Neutron Diffraction

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Single Crystal Neutron Diffraction from Molecular Materials

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Author : Chick C. Wilson
Publisher : World Scientific
ISBN 13 : 9789810237769
Total Pages : 390 pages
Book Rating : 4.2/5 (377 download)

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Book Synopsis Single Crystal Neutron Diffraction from Molecular Materials by : Chick C. Wilson

Download or read book Single Crystal Neutron Diffraction from Molecular Materials written by Chick C. Wilson and published by World Scientific. This book was released on 2000 with total page 390 pages. Available in PDF, EPUB and Kindle. Book excerpt: This important book presents a comprehensive account of the techniques & applications of single crystal neutron diffraction in the area of chemical crystallography & molecular structure. Beginning with a brief description of the general principles & the reasons for choosing the technique - the "why" - the book covers the methods for both the production of neutrons & the measurement of their scattering by molecular crystals - the "how" - followed by a detailed survey of past, present & future applications - the "what". The coverage of both steady state & pulsed neutron sources & instrumentation is extensive, while the survey of applications is the most comprehensive yet undertaken. The book endeavours to show why the technique is an essential method for studying areas as diverse as hydrogen bonding & weak interactions, organometallics, supramolecular chemistry & crystal engineering, metal hydrides, charge density & pharmaceuticals. It is an ideal reference source for the research worker interested in using neutron diffraction to study the structure of molecules. Contents: Crystallography & the Importance of Structural Information; Neutron Scattering; Neutron Diffractometers; Review of Applications I: The Accurate Location of Atoms; Review of Applications II: Hydrogen Bonding & Other Intermolecular Interactions; Review of Applications III: Probing Vibrations & Disorder; Impact on Material Properties & Design; The Future: New Instruments, New Sources, New Techniques. Readership: Students & researchers involved in structural science, especially chemical crystallography.

Crystal Structure Analysis

Author : Jenny Pickworth Glusker
Publisher : OUP Oxford
ISBN 13 : 0191604240
Total Pages : 304 pages
Book Rating : 4.1/5 (916 download)

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Book Synopsis Crystal Structure Analysis by : Jenny Pickworth Glusker

Download or read book Crystal Structure Analysis written by Jenny Pickworth Glusker and published by OUP Oxford. This book was released on 2010-05-27 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book aims to explain how and why the detailed three-dimensional architecture of molecules can be determined by an analysis of the diffraction patterns obtained when X rays or neutrons are scattered by the atoms in single crystals. Part 1 deals with the nature of the crystalline state, diffraction generally, and diffraction by crystals in particular, and, briefly, the experimental procedures that are used. Part II examines the problem of converting the experimentally obtained data into a model of the atomic arrangement that scattered these beams. Part III is concerned with the techniques for refining the approximate structure to the degree warranted by the experimental data. It also describes the many types of information that can be learned by modern crystal structure analysis. There is a glossary of terms used and several appendixes to which most of the mathematical details have been relegated.

Neutron Diffraction of Magnetic Materials

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Author : Izyumov
Publisher : Springer Science & Business Media
ISBN 13 : 1461536588
Total Pages : 349 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Neutron Diffraction of Magnetic Materials by : Izyumov

Download or read book Neutron Diffraction of Magnetic Materials written by Izyumov and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 349 pages. Available in PDF, EPUB and Kindle. Book excerpt: Detennination of the magnetic structure of magnetic materials is a fundamental problem that can be solved by magnetic neutron diffraction techniques. By magnetic structures we refer to the mutual alignment of the magnetic moments of the atoms in a crystal and their overall alignment relative to the crystallographic axes. Some indirect, tentative data on the magnetic structure of magnetic materials can be obtained from research on their magnetic, mechanical, thermal, and other properties. But only neutron diffraction is a unique direct method of detennining the magnetic structure of a crystal. The magnetic structure of more than one thousand crystals with magnetic order has been studied during 30 years of neutron diffraction research made on reactors in a large number of laboratories in the world. The results of this research work are extensively described in the handbook Magnetic Structures Determined by Neutron Diffraction [176]; in the present book, we will often refer to this handbook. The first extensive theoretical generalization of the principles of magnetic neutron diffraction and the results of research on magnetic structures appeared in the book by Yu. A. Izyumov and R. P. Ozerov Magnetic Neutron Diffraction [24, 134].

Magnetic Neutron Diffraction

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Author : Yurii A. Izyumov
Publisher : Springer Science & Business Media
ISBN 13 : 1468407120
Total Pages : 607 pages
Book Rating : 4.4/5 (684 download)

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Book Synopsis Magnetic Neutron Diffraction by : Yurii A. Izyumov

Download or read book Magnetic Neutron Diffraction written by Yurii A. Izyumov and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 607 pages. Available in PDF, EPUB and Kindle. Book excerpt: The inter action between the magnetic field generated by the neutron and the magnetic moment of atoms containing unpaired electrons was experimentally demonstrated for the first time about twenty years ago. The basic theory describing such an in teraction had already been developed and the first nuclear reactors with large available thermal neutron fluxes had recently been con structed. The power of the magnetic neutron interaction for in vestigating the structure of magnetic materials was immediately recognized and put to use where possible. Neutron diffraction, however, was practicable only in countries with nuclear reactors. The earliest neutron determinations of magnetic ordering were hence primarily carried out at Oak Ridge and Brookhaven in the US, at Chalk River in Canada and at Harwell in England. Diffraction patterns from polycrystalline ferromagnets and antiferromagnets are interpretable if produced by simple spin arrays. More complex magnetic scattering patterns could often be unravelled, in terms of a three-dimensional array of atomic moments, if the specimen studied is a single crystal. The devel opment of sophisticated cryogenic equipment, with independently alignable magnetic fields, opened the way to greater complexity in the magnetic structures that could be successfully determined, as did also the introduction of polarized neutron beams. By the end of the 'sixties, many countries were contributing significantly to neutron diffraction studies of a wide variety of magnetic materials.

Structure Determination by X-Ray Crystallography

Author : M. F. C. Ladd
Publisher : Springer Science & Business Media
ISBN 13 : 1461579333
Total Pages : 404 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Structure Determination by X-Ray Crystallography by : M. F. C. Ladd

Download or read book Structure Determination by X-Ray Crystallography written by M. F. C. Ladd and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 404 pages. Available in PDF, EPUB and Kindle. Book excerpt: Crystallography may be described as the science of the structure of materi als, using this word in its widest sense, and its ramifications are apparent over a broad front of current scientific endeavor. It is not surprising, therefore, to find that most universities offer some aspects of crystallography in their undergraduate courses in the physical sciences. It is the principal aim of this book to present an introduction to structure determination by X-ray crystal lography that is appropriate mainly to both final-year undergraduate studies in crystallography, chemistry, and chemical physics, and introductory post graduate work in this area of crystallography. We believe that the book will be of interest in other disciplines, such as physics, metallurgy, biochemistry, and geology, where crystallography has an important part to play. In the space of one book, it is not possible either to cover all aspects of crystallography or to treat all the subject matter completely rigorously. In particular, certain mathematical results are assumed in order that their applications may be discussed. At the end of each chapter, a short bibliog raphy is given, which may be used to extend the scope of the treatment given here. In addition, reference is made in the text to specific sources of information. We have chosen not to discuss experimental methods extensively, as we consider that this aspect of crystallography is best learned through practical experience, but an attempt has been made to simulate the interpretive side of experimental crystallography in both examples and exercises.

Elements of Slow-Neutron Scattering

Author : J. M. Carpenter
Publisher : Cambridge University Press
ISBN 13 : 0521857813
Total Pages : 539 pages
Book Rating : 4.5/5 (218 download)

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Book Synopsis Elements of Slow-Neutron Scattering by : J. M. Carpenter

Download or read book Elements of Slow-Neutron Scattering written by J. M. Carpenter and published by Cambridge University Press. This book was released on 2015-09-24 with total page 539 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a comprehensive and up-to-date introduction to the fundamental theory and applications of slow-neutron scattering.

Structural Biology in Drug Discovery

Author : Jean-Paul Renaud
Publisher : John Wiley & Sons
ISBN 13 : 1118900502
Total Pages : 1437 pages
Book Rating : 4.1/5 (189 download)

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Book Synopsis Structural Biology in Drug Discovery by : Jean-Paul Renaud

Download or read book Structural Biology in Drug Discovery written by Jean-Paul Renaud and published by John Wiley & Sons. This book was released on 2020-01-09 with total page 1437 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the most comprehensive and up-to-date overview of structure-based drug discovery covering both experimental and computational approaches, Structural Biology in Drug Discovery: Methods, Techniques, and Practices describes principles, methods, applications, and emerging paradigms of structural biology as a tool for more efficient drug development. Coverage includes successful examples, academic and industry insights, novel concepts, and advances in a rapidly evolving field. The combined chapters, by authors writing from the frontlines of structural biology and drug discovery, give readers a valuable reference and resource that: Presents the benefits, limitations, and potentiality of major techniques in the field such as X-ray crystallography, NMR, neutron crystallography, cryo-EM, mass spectrometry and other biophysical techniques, and computational structural biology Includes detailed chapters on druggability, allostery, complementary use of thermodynamic and kinetic information, and powerful approaches such as structural chemogenomics and fragment-based drug design Emphasizes the need for the in-depth biophysical characterization of protein targets as well as of therapeutic proteins, and for a thorough quality assessment of experimental structures Illustrates advances in the field of established therapeutic targets like kinases, serine proteinases, GPCRs, and epigenetic proteins, and of more challenging ones like protein-protein interactions and intrinsically disordered proteins

Neutron Protein Crystallography

Author : Nobuo Niimura
Publisher : Oxford University Press
ISBN 13 : 0199578869
Total Pages : 250 pages
Book Rating : 4.1/5 (995 download)

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Book Synopsis Neutron Protein Crystallography by : Nobuo Niimura

Download or read book Neutron Protein Crystallography written by Nobuo Niimura and published by Oxford University Press. This book was released on 2011-02-17 with total page 250 pages. Available in PDF, EPUB and Kindle. Book excerpt: One of the first books dedicated to the emerging field of neutron protein crystallography (NPC). It covers all of the practical aspects of NPC and demonstrates how NPC can explore protein features such as hydrogen bonds, protonation and deprotonation of amino acid residues, and hydration structures.

Single Crystal Diffractometry

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Author : U. W. Arndt
Publisher : Cambridge University Press
ISBN 13 : 0521040604
Total Pages : 0 pages
Book Rating : 4.5/5 (21 download)

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Book Synopsis Single Crystal Diffractometry by : U. W. Arndt

Download or read book Single Crystal Diffractometry written by U. W. Arndt and published by Cambridge University Press. This book was released on 1966 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Originally published in 1966, this book covers all aspects of single crystal diffractometry.

Single Crystal Neutron Diffraction From Molecular Materials

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Author : Chick C Wilson
Publisher : World Scientific Publishing Company
ISBN 13 : 9813105402
Total Pages : 386 pages
Book Rating : 4.8/5 (131 download)

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Book Synopsis Single Crystal Neutron Diffraction From Molecular Materials by : Chick C Wilson

Download or read book Single Crystal Neutron Diffraction From Molecular Materials written by Chick C Wilson and published by World Scientific Publishing Company. This book was released on 2000-02-18 with total page 386 pages. Available in PDF, EPUB and Kindle. Book excerpt: This important book presents a comprehensive account of the techniques and applications of single crystal neutron diffraction in the area of chemical crystallography and molecular structure. Beginning with a brief description of the general principles and the reasons for choosing the technique — the “why” — the book covers the methods for both the production of neutrons and the measurement of their scattering by molecular crystals — the “how” — followed by a detailed survey of past, present and future applications — the “what”. The coverage of both steady state and pulsed neutron sources and instrumentation is extensive, while the survey of applications is the most comprehensive yet undertaken. The book endeavours to show why the technique is an essential method for studying areas as diverse as hydrogen bonding and weak interactions, organometallics, supramolecular chemistry and crystal engineering, metal hydrides, charge density and pharmaceuticals. It is an ideal reference source for the research worker interested in using neutron diffraction to study the structure of molecules.

X-Ray and Neutron Diffraction

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Author : G. E. Bacon
Publisher : Elsevier
ISBN 13 : 1483158292
Total Pages : 393 pages
Book Rating : 4.4/5 (831 download)

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Book Synopsis X-Ray and Neutron Diffraction by : G. E. Bacon

Download or read book X-Ray and Neutron Diffraction written by G. E. Bacon and published by Elsevier. This book was released on 2013-09-03 with total page 393 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-Ray and Neutron Diffraction describes the developments of the X-ray and the various research done in neutron diffraction. Part I of the book concerns the principles and applications of the X-ray and neutrons through their origins from classical crystallography. The book explains the use of diffraction methods to show the highly regular arrangement of atoms that forms a continuous pattern in three-dimensional space. The text evaluates the limitations and benefits of using the different types of radiation sources, whether these are X-rays, neutrons, or electrons. Part II is a collection of reprints discussing the development of techniques that includes a modification of the Bragg method, which is a method of X-ray crystal analysis. One paper presents an improved numerical method of two-dimensional Fourier synthesis for crystals. This method uses a greatly reduced process of arrangement of sets of figures found in the two-dimensional Fourier series. The book also notes the theoretical considerations and the practical details, and then addresses precautions against possible inclusions of errors in this method. The text deals as well with the magnetic scattering of neutrons, and one paper presents a simple method of gathering information about the magnetic moment of the neutron besides the traditional Stern-Gerlach method. Nuclear scientists and physicists, atomic researchers, and nuclear engineers will greatly appreciate the book.

Techniques in High Pressure Neutron Scattering

Author : Stefan Klotz
Publisher : CRC Press
ISBN 13 : 1439835632
Total Pages : 274 pages
Book Rating : 4.4/5 (398 download)

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Book Synopsis Techniques in High Pressure Neutron Scattering by : Stefan Klotz

Download or read book Techniques in High Pressure Neutron Scattering written by Stefan Klotz and published by CRC Press. This book was released on 2012-12-04 with total page 274 pages. Available in PDF, EPUB and Kindle. Book excerpt: Drawing on the author's practical work from the last 20 years, Techniques in High Pressure Neutron Scattering is one of the first books to gather recent methods that allow neutron scattering well beyond 10 GPa. The author shows how neutron scattering has to be adapted to the pressure range and type of measurement.Suitable for both newcomers and exp

Experimental Neutron Scattering

Author : B. T. M. Willis
Publisher : Oxford University Press
ISBN 13 : 0191545473
Total Pages : 325 pages
Book Rating : 4.1/5 (915 download)

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Book Synopsis Experimental Neutron Scattering by : B. T. M. Willis

Download or read book Experimental Neutron Scattering written by B. T. M. Willis and published by Oxford University Press. This book was released on 2017-03-23 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first systematic experiments in neutron scattering were carried out in the late 1940s using fission reactors built for the nuclear power programme. Crystallographers were amongst the first to exploit the new technique, but they were soon followed by condensed matter physicists and chemists. Engineers and biologists are the most recent recruits to the club of neutron users. The aim of the book is to provide a broad survey of the experimental activities of all these users. There are many specialist monographs describing particular examples of the application of neutron scattering: fifteen of such monographs have been published already in the Oxford University Press series edited by S. Lovesey and E. Mitchell. However this book will appeal to newcomers to the field of neutron scattering, who may be intimidated by the bewildering array of instruments at central facilities (such as the Institut Laue Langevin in France, the ISIS Laboratory in the UK, or the PSI Laboratory in Switzerland), and who may be uncertain as to which instrument to use.

Neutron Scattering in Biology

Author : Jörg Fitter
Publisher : Springer Science & Business Media
ISBN 13 : 3540291113
Total Pages : 571 pages
Book Rating : 4.5/5 (42 download)

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Book Synopsis Neutron Scattering in Biology by : Jörg Fitter

Download or read book Neutron Scattering in Biology written by Jörg Fitter and published by Springer Science & Business Media. This book was released on 2006-05-01 with total page 571 pages. Available in PDF, EPUB and Kindle. Book excerpt: The advent of new neutron facilities and the improvement of existing sources and instruments world wide supply the biological community with many new opportunities in the areas of structural biology and biological physics. The present volume offers a clear description of the various neutron-scattering techniques currently being used to answer biologically relevant questions. Their utility is illustrated through examples by some of the leading researchers in the field of neutron scattering. This volume will be a reference for researchers and a step-by-step guide for young scientists entering the field and the advanced graduate student.

Neutron Scattering in Earth Sciences

Author : Hans-Rudolf Wenk
Publisher : de Gruyter
ISBN 13 :
Total Pages : 496 pages
Book Rating : 4.:/5 (318 download)

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Book Synopsis Neutron Scattering in Earth Sciences by : Hans-Rudolf Wenk

Download or read book Neutron Scattering in Earth Sciences written by Hans-Rudolf Wenk and published by de Gruyter. This book was released on 2006 with total page 496 pages. Available in PDF, EPUB and Kindle. Book excerpt: Reviews in Mineralogy & Geochemistry (RiMG) volumes contain concise advances in theoretical and/or applied mineralogy, crystallography, petrology, and geochemistry.

Neutron Scattering from Magnetic Materials

Author : Tapan Chatterji
Publisher : Elsevier
ISBN 13 : 0080457053
Total Pages : 574 pages
Book Rating : 4.0/5 (84 download)

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Book Synopsis Neutron Scattering from Magnetic Materials by : Tapan Chatterji

Download or read book Neutron Scattering from Magnetic Materials written by Tapan Chatterji and published by Elsevier. This book was released on 2005-11-29 with total page 574 pages. Available in PDF, EPUB and Kindle. Book excerpt: Neutron Scattering from Magnetic Materials is a comprehensive account of the present state of the art in the use of the neutron scattering for the study of magnetic materials. The chapters have been written by well-known researchers who are at the forefront of this field and have contributed directly to the development of the techniques described. Neutron scattering probes magnetic phenomena directly. The generalized magnetic susceptibility, which can be expressed as a function of wave vector and energy, contains all the information there is to know about the statics and dynamics of a magnetic system and this quantity is directly related to the neutron scattering cross section. Polarized neutron scattering techniques raise the sophistication of measurements to even greater levels and gives additional information in many cases. The present book is largely devoted to the application of polarized neutron scattering to the study of magnetic materials. It will be of particular interest to graduate students and researchers who plan to investigate magnetic materials using neutron scattering.· Written by a group of scientist who have contributed directly in developing the techniques described.· A complete treatment of the polarized neutron scattering not available in literature.· Gives practical hits to solve magnetic structure and determine exchange interactions in magnetic solids.· Application of neutron scattering to the study of the novel electronic materials.

Local Structure from Diffraction

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Author : S.J.L. Billinge
Publisher : Springer Science & Business Media
ISBN 13 : 0306470772
Total Pages : 397 pages
Book Rating : 4.3/5 (64 download)

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Book Synopsis Local Structure from Diffraction by : S.J.L. Billinge

Download or read book Local Structure from Diffraction written by S.J.L. Billinge and published by Springer Science & Business Media. This book was released on 2006-02-04 with total page 397 pages. Available in PDF, EPUB and Kindle. Book excerpt: This series of books, which is published at the rate of about one per year, addresses fundamental problems in materials science. The contents cover a broad range of topics from small clusters of atoms to engineering materials and involve chemistry, physics, materials science and engineering, with length scales ranging from Ångstroms up to millimeters. The emphasis is on basic science rather than on applications. Each book focuses on a single area of current interest and brings together leading experts to give an up-to-date discussion of their work and the work of others. Each article contains enough references that the interested reader can access the relevant literature. Thanks are given to the Center for Fundamental Materials Research at Michigan State University for supporting this series. M.F. Thorpe, Series Editor E-mail: thorpe @ pa.msu.edu East Lansing, Michigan PREFACE One of the most challenging problems in the study of structure is to characterize the atomic short-range order in materials. Long-range order can be determined with a high degree of accuracy by analyzing Bragg peak positions and intensities in data from single crystals or powders. However, information about short-range order is contained in the diffuse scattering intensity. This is difficult to analyze because it is low in absolute intensity (though the integrated intensity may be significant) and widely spread in reciprocal space.