Phase Transfer Catalyzed Free Radical Polymerization Of Methyl Methacrylate With Potassium Peroxydisulfate And 18 Crown 6

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Crown Ethers and Phase Transfer Catalysis in Polymer Science

Author : Lon Mathias
Publisher : Springer Science & Business Media
ISBN 13 : 1461593492
Total Pages : 421 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Crown Ethers and Phase Transfer Catalysis in Polymer Science by : Lon Mathias

Download or read book Crown Ethers and Phase Transfer Catalysis in Polymer Science written by Lon Mathias and published by Springer Science & Business Media. This book was released on 2013-11-22 with total page 421 pages. Available in PDF, EPUB and Kindle. Book excerpt: Phase transfer catalysis or interfacial catalysis is a syn thetic technique involving transport of an organic or inorganic salt from a solid or aqueous phase into an organic liquid where reaction with an organic-soluble substrate takes place. Over the past 15 years there has been an enormous amount of effort invested in the development of this technique in organic synthe sis. Several books and numerous review articles have appeared summarizing applications in which low molecular weight catalysts are employed. These generally include either crown ethers or onium salts of various kinds. While the term phase transfer catalysis is relatively new, the concept of using a phasetrans fer agent (PTA) is much older~ Both Schnell and Morgan employed such catalysts in synthesis of polymeric species in the early 1950's. Present developments are really extensions of these early applications. It has only been within the last several years that the use of phase transfer processes have been employed in polymer synthesis and modification. Similarly, the use of polymer-bound phase transfer agents is also a recent development. These and related areas have nonetheless enjoyed explosive growth as mea sured by the number of publications and the variety of applica tions which have appeared. Several reviews dealing with these l 6 polymer-related investigations have been published.

Phase-transfer Catalysis

Author : Charles M. Starks
Publisher :
ISBN 13 :
Total Pages : 216 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Phase-transfer Catalysis by : Charles M. Starks

Download or read book Phase-transfer Catalysis written by Charles M. Starks and published by . This book was released on 1987 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Journal of the Chinese Chemical Society

Author : Zhongguo hua xue hui (Taipei, Taiwan)
Publisher :
ISBN 13 :
Total Pages : 380 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Journal of the Chinese Chemical Society by : Zhongguo hua xue hui (Taipei, Taiwan)

Download or read book Journal of the Chinese Chemical Society written by Zhongguo hua xue hui (Taipei, Taiwan) and published by . This book was released on 1994 with total page 380 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Dissertation Abstracts International

Author :
Publisher :
ISBN 13 :
Total Pages : 598 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Dissertation Abstracts International by :

Download or read book Dissertation Abstracts International written by and published by . This book was released on 1987 with total page 598 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Boletín de actualización

Author : Instituto Mexicano del Petróleo. División de Información y Difusión
Publisher :
ISBN 13 :
Total Pages : 376 pages
Book Rating : 4.A/5 ( download)

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Book Synopsis Boletín de actualización by : Instituto Mexicano del Petróleo. División de Información y Difusión

Download or read book Boletín de actualización written by Instituto Mexicano del Petróleo. División de Información y Difusión and published by . This book was released on 1986 with total page 376 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Textile Technology Digest

Author :
Publisher :
ISBN 13 :
Total Pages : 752 pages
Book Rating : 4.E/5 ( download)

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Book Synopsis Textile Technology Digest by :

Download or read book Textile Technology Digest written by and published by . This book was released on 2002 with total page 752 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Handbook of Phase Transfer Catalysis

Author : Y. Sasson
Publisher : Springer Science & Business Media
ISBN 13 : 9400900236
Total Pages : 579 pages
Book Rating : 4.4/5 (9 download)

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Book Synopsis Handbook of Phase Transfer Catalysis by : Y. Sasson

Download or read book Handbook of Phase Transfer Catalysis written by Y. Sasson and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 579 pages. Available in PDF, EPUB and Kindle. Book excerpt: Phase transfer catalysis is a sophisticated chemical technique which can be used to perform a variety of chemical reactions under mild conditions and with improved control. Since the concept was developed, both the theoretical and practical synthetic applications have seen considerable development, to the point where the technique can be applied to many areas of chemistry. Thus, phase transfer methods are now utilized in many applications, from research chemistry to full-scale production, where the benefits of faster, cleaner and more selective reactions are required. In this new book, the editors have brought together a range of contributors, each of whom is working at the forefront of the technology, to provide a clear, concise and ahtoritative review of this important area of chemistry. Industrial and academic chemists working on the synthesis, scale-up, production or analysis of a wide range of chemical products will find this book an essential reference on phase transfer technology.

Engineered Materials Abstracts

Author :
Publisher :
ISBN 13 :
Total Pages : 662 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Engineered Materials Abstracts by :

Download or read book Engineered Materials Abstracts written by and published by . This book was released on 1990-10 with total page 662 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Holographic Sensors

Author : Ali Kemal Yetisen
Publisher : Springer
ISBN 13 : 3319135848
Total Pages : 175 pages
Book Rating : 4.3/5 (191 download)

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Book Synopsis Holographic Sensors by : Ali Kemal Yetisen

Download or read book Holographic Sensors written by Ali Kemal Yetisen and published by Springer. This book was released on 2014-12-03 with total page 175 pages. Available in PDF, EPUB and Kindle. Book excerpt: This thesis presents a theoretical and experimental approach for the rapid fabrication, optimization and testing of holographic sensors for the quantification of pH, organic solvents, metal cations, and glucose in solutions. Developing non-invasive and reusable diagnostics sensors that can be easily manufactured will support the monitoring of high-risk individuals in any clinical or point-of-care setting. Sensor fabrication approaches outlined include silver-halide chemistry, laser ablation and photopolymerization. The sensors employ off-axis Bragg diffraction gratings of ordered silver nanoparticles and localized refractive index changes in poly (2-hydroxyethyl methacrylate) and polyacrylamide films. The sensors exhibited reversible Bragg peak shifts, and diffracted the spectrum of narrow-band light over the wavelength range λpeak ≈ 495-1100 nm. Clinical trials of glucose sensors in the urine samples of diabetic patients demonstrated that they offer superior performance compared to commercial high-throughput urinalysis devices. Lastly, a generic smartphone application to quantify colorimetric tests was developed and tested for both Android and iOS operating systems. The sensing platform and smartphone application may have implications for the development of low-cost, reusable and equipment-free point-of-care diagnostic devices.

Clay-Polymer Nanocomposites

Author : Khouloud Jlassi
Publisher : Elsevier
ISBN 13 : 0323461611
Total Pages : 548 pages
Book Rating : 4.3/5 (234 download)

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Book Synopsis Clay-Polymer Nanocomposites by : Khouloud Jlassi

Download or read book Clay-Polymer Nanocomposites written by Khouloud Jlassi and published by Elsevier. This book was released on 2017-07-26 with total page 548 pages. Available in PDF, EPUB and Kindle. Book excerpt: Clay–Polymer Nanocomposites is a complete summary of the existing knowledge on this topic, from the basic concepts of synthesis and design to their applications in timely topics such as high-performance composites, environment, and energy issues. This book covers many aspects of synthesis such as in- situ polymerization within the interlamellar spacing of the clays or by reaction of pristine or pre-modified clays with reactive polymers and prepolymers. Indeed, nanocomposites can be prepared at industrial scale by melt mixing. Regardless the synthesis method, much is said in this book about the importance of theclay pre-modification step, which is demonstrated to be effective, on many occasions, in obtaining exfoliated nanocomposites. Clay–Polymer Nanocomposites reports the background to numerous characterization methods including solid state NMR, neutron scattering, diffraction and vibrational techniques as well as surface analytical methods, namely XPS, inverse gas chromatography and nitrogen adsorption to probe surface composition, wetting and textural/structural properties. Although not described in dedicated chapters, numerous X-ray diffraction patterns of clay–polymer nanocomposites and reference materials are displayed to account for the effects of intercalation and exfoliations of layered aluminosilicates. Finally, multiscale molecular simulation protocols are presenting for predicting morphologies and properties of nanostructured polymer systems with industrial relevance. As far as applications are concerned, Clay–Polymer Nanocomposites examines structural composites such as clay–epoxy and clay–biopolymers, the use of clay–polymer nanocomposites as reactive nanocomposite fillers, catalytic clay-(conductive) polymers and similar nanocomposites for the uptake of hazardous compounds or for controlled drug release, antibacterial applications, energy storage, and more. - The most comprehensive coverage of the state of the art in clay–polymer nanocomposites, from synthesis and design to opportunities and applications - Covers the various methods of characterization of clay–polymer nanocomposites - including spectroscopy, thermal analyses, and X-ray diffraction - Includes a discussion of a range of application areas, including biomedicine, energy storage, biofouling resistance, and more

Principles of Polymerization

Author : George Odian
Publisher : John Wiley & Sons
ISBN 13 : 0471274003
Total Pages : 850 pages
Book Rating : 4.4/5 (712 download)

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Book Synopsis Principles of Polymerization by : George Odian

Download or read book Principles of Polymerization written by George Odian and published by John Wiley & Sons. This book was released on 2004-02-09 with total page 850 pages. Available in PDF, EPUB and Kindle. Book excerpt: The new edition of a classic text and reference The large chains of molecules known as polymers are currently used in everything from "wash and wear" clothing to rubber tires to protective enamels and paints. Yet the practical applications of polymers are only increasing; innovations in polymer chemistry constantly bring both improved and entirely new uses for polymers onto the technological playing field. Principles of Polymerization, Fourth Edition presents the classic text on polymer synthesis, fully updated to reflect today's state of the art. New and expanded coverage in the Fourth Edition includes: * Metallocene and post-metallocene polymerization catalysts * Living polymerizations (radical, cationic, anionic) * Dendrimer, hyperbranched, brush, and other polymer architectures and assemblies * Graft and block copolymers * High-temperature polymers * Inorganic and organometallic polymers * Conducting polymers * Ring-opening polymer ization * In vivo and in vitro polymerization Appropriate for both novice and advanced students as well as professionals, this comprehensive yet accessible resource enables the reader to achieve an advanced, up-to-date understanding of polymer synthesis. Different methods of polymerization, reaction parameters for synthesis, molecular weight, branching and crosslinking, and the chemical and physical structure of polymers all receive ample coverage. A thorough discussion at the elementary level prefaces each topic, with a more advanced treatment following. Yet the language throughout remains straightforward and geared towards the student. Extensively updated, Principles of Polymerization, Fourth Edition provides an excellent textbook for today's students of polymer chemistry, chemical engineering, and materials science, as well as a current reference for the researcher or other practitioner working in these areas.

Phase-Transfer Catalysis

Author : C.M. Starks
Publisher : Springer Science & Business Media
ISBN 13 : 9401106878
Total Pages : 682 pages
Book Rating : 4.4/5 (11 download)

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Book Synopsis Phase-Transfer Catalysis by : C.M. Starks

Download or read book Phase-Transfer Catalysis written by C.M. Starks and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 682 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since 1971 when useful working concepts for the technique of phase-transfer catalysis (PTC) were introduced, the understanding, development, and applica tions of this method for conducting organic reactions has expanded exponentially. PTC has brought vast new dimensions and options to chemists and chemical engineers. From its use in less than ten commercial processes in 1975, PTC use has increased so that in the early 1990s it is involved in more than 600 industrial applications to manufacture products valued at between 10 and 20 billion U.S. dollars. PTC is widely used for simple organic reactions, steps in synthesis of pharmaceuticals, agricultural chemicals, perfumes, ftavorants, and dyes; for specialty polymerization reactions, polymer modifications, and monomer synthe sis; for pollution and environmental control processes; for analysis oftrace organic and inorganic compounds; and for many other applications. Often, PTC offers the best (and sometimes only) practical technique to obtain certain products. The authors experience in teaching a short course on phase-transfer catalysis has shown to us that a newcomer to PTC can easily be frustrated and confused by the large amount of information available in the literature and in patents. The purpose of this book, therefore, was to bring this information together in a logical and user-friendly way, without sacrificing matters of scholarly and fundamental importance.

Polymers

Author : J.M.G. Cowie
Publisher : CRC Press
ISBN 13 : 9780748740734
Total Pages : 452 pages
Book Rating : 4.7/5 (47 download)

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Book Synopsis Polymers by : J.M.G. Cowie

Download or read book Polymers written by J.M.G. Cowie and published by CRC Press. This book was released on 1991-06-01 with total page 452 pages. Available in PDF, EPUB and Kindle. Book excerpt: This text follows a broad sequence of preparation, characterization, physical and mechanical properties and structure-property relations. Polymers: Chemistry and Physics of Modern Materials, Second Edition covers several methods of polymerization, properties, and advanced applications such as liquid crystals and polymers used in the electronics industry. Topics also include Step-Growth, Free Radical Addition, and Ionic Polymerization; Copolymerization; Polymer Stereochemistry and Characterization; Structure-Property Relationship; Polymer Liquid Crystals; and Polymers for the Electronics Industry.

Biomedical and Dental Applications of Polymers

Author : Charles Gebelein
Publisher : Springer Science & Business Media
ISBN 13 : 1475795106
Total Pages : 477 pages
Book Rating : 4.4/5 (757 download)

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Book Synopsis Biomedical and Dental Applications of Polymers by : Charles Gebelein

Download or read book Biomedical and Dental Applications of Polymers written by Charles Gebelein and published by Springer Science & Business Media. This book was released on 2013-11-11 with total page 477 pages. Available in PDF, EPUB and Kindle. Book excerpt: The development and use of medical and dental materials are highly interdisciplinary endeavors which require expertise in chemistry, materials science, medicine and/or dentistry, mechanics and design engineering. The Symposium upon which this treatise is based was organized to bring members from these communities together to explore problems of mutual interest. The biomaterials which are used in medical or dental prostheses must not only exhibit structural stability and provide the desired function, but they must also perform over extended periods of time in the environment of the body. The latter is a very stringent requirement. The oral and other physiological environments are designed by nature to break down many organic substances. Also of importance is the requirement that materials used in the prosthesis not have a deleterious effect on body tissues. Most foreign (to the body) substances are somewhat toxic to human tissues; in fact, few factors are more limiting in the medical prosthesis field than the biocompatibility problem. Some of these problems and the attempts to solve them are discussed in this volume.

Polymers

Author : J.M.G. Cowie
Publisher : CRC Press
ISBN 13 : 1420009877
Total Pages : 520 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Polymers by : J.M.G. Cowie

Download or read book Polymers written by J.M.G. Cowie and published by CRC Press. This book was released on 2007-07-27 with total page 520 pages. Available in PDF, EPUB and Kindle. Book excerpt: Extensively revised and updated to keep abreast of recent advances, Polymers: Chemistry and Physics of Modern Materials, Third Edition continues to provide a broad-based, high-information text at an introductory, reader-friendly level that illustrates the multidisciplinary nature of polymer science. Adding or amending roughly 50% of the material, t

Polymer Synthesis

Author :
Publisher : Springer Science & Business Media
ISBN 13 : 9783540217114
Total Pages : 228 pages
Book Rating : 4.2/5 (171 download)

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Book Synopsis Polymer Synthesis by :

Download or read book Polymer Synthesis written by and published by Springer Science & Business Media. This book was released on 2004-10-08 with total page 228 pages. Available in PDF, EPUB and Kindle. Book excerpt: 1. T. Takata, N. Kihara, Y. Furusho: Polyrotaxanes and Polycatenanes: Recent Advances in Syntheses and Applications of Polymers Comprising of Interlocked Structures.- 2. M. Suginome, Y. Ito: Transition Metal-Mediated Polymerization of Isocyanides.- 3. K. Osakada, D. Takeuchi: Coordination Polymerization of Dienes, Allenes and Methylenecycloalkanes.

Organic and Physical Chemistry of Polymers

Author : Yves Gnanou
Publisher : John Wiley & Sons
ISBN 13 : 0470238119
Total Pages : 629 pages
Book Rating : 4.4/5 (72 download)

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Book Synopsis Organic and Physical Chemistry of Polymers by : Yves Gnanou

Download or read book Organic and Physical Chemistry of Polymers written by Yves Gnanou and published by John Wiley & Sons. This book was released on 2008-03-03 with total page 629 pages. Available in PDF, EPUB and Kindle. Book excerpt: Organic and Physical Chemistry of Polymers provides a thorough introduction to the fundamentals of polymers, including their structure and synthesis as well as their chemical and physical properties. This accessible guide illuminates the increasingly important role of polymers in modern chemistry, beginning with the essentials, then covering thermodynamics, conformation, morphology, and measurements of molar masses; polymerization mechanisms, reaction of polymers, synthesis of block and graft polymers, and complex topologies; and the mechanical properties, rheology, polymer processing, and fabrication of fibers and films.