NMR Spectroscopy

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Publisher : John Wiley & Sons
ISBN 13 : 3527674772
Total Pages : 842 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis NMR Spectroscopy by : Harald Günther

Download or read book NMR Spectroscopy written by Harald Günther and published by John Wiley & Sons. This book was released on 2013-12-13 with total page 842 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is important for determining the 3D-structure of molecules. This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.

High-resolution NMR Techniques in Organic Chemistry

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Author :
Publisher : Elsevier
ISBN 13 : 9780080427997
Total Pages : 408 pages
Book Rating : 4.4/5 (279 download)

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Book Synopsis High-resolution NMR Techniques in Organic Chemistry by : T. Claridge

Download or read book High-resolution NMR Techniques in Organic Chemistry written by T. Claridge and published by Elsevier. This book was released on 1999-12-24 with total page 408 pages. Available in PDF, EPUB and Kindle. Book excerpt: From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.

Essential Practical NMR for Organic Chemistry

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Publisher : John Wiley & Sons
ISBN 13 : 0470977221
Total Pages : 345 pages
Book Rating : 4.4/5 (79 download)

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Book Synopsis Essential Practical NMR for Organic Chemistry by : S. A. Richards

Download or read book Essential Practical NMR for Organic Chemistry written by S. A. Richards and published by John Wiley & Sons. This book was released on 2010-12-07 with total page 345 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book describes the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation. It features a significant amount of vital chemical shift and coupling information but more importantly, it presents sound principles for the selection of the techniques relevant to the solving of particular types of problem, whilst stressing the importance of extracting the maximum available information from the simple 1-D proton experiment and of using this to plan subsequent experiments. Proton NMR is covered in detail, with a description of the fundamentals of the technique, the instrumentation and the data that it provides before going on to discuss optimal solvent selection and sample preparation. This is followed by a detailed study of each of the important classes of protons, breaking the spectrum up into regions (exchangeables, aromatics, heterocyclics, alkenes etc.). This is followed by consideration of the phenomena that we know can leave chemists struggling; chiral centres, restricted rotation, anisotropy, accidental equivalence, non-first-order spectra etc. Having explained the potential pitfalls that await the unwary, the book then goes on to devote chapters to the chemical techniques and the most useful instrumental ones that can be employed to combat them. A discussion is then presented on carbon-13 NMR, detailing its pros and cons and showing how it can be used in conjunction with proton NMR via the pivotal 2-D techniques (HSQC and HMBC) to yield vital structural information. Some of the more specialist techniques available are then discussed, i.e. flow NMR, solvent suppression, Magic Angle Spinning, etc. Other important nuclei are then discussed and useful data supplied. This is followed by a discussion of the neglected use of NMR as a tool for quantification and new techniques for this explained. The book then considers the safety aspects of NMR spectroscopy, reviewing NMR software for spectral prediction and data handling and concludes with a set of worked Q&As.

Nuclear Magnetic Resonance

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Publisher :
ISBN 13 : 0198703414
Total Pages : 121 pages
Book Rating : 4.1/5 (987 download)

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Book Synopsis Nuclear Magnetic Resonance by : P. J. Hore

Download or read book Nuclear Magnetic Resonance written by P. J. Hore and published by . This book was released on 2015 with total page 121 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear Magnetic Resonance offers an accessible introduction to the physical principles of liquid-state NMR, with examples, applications, and exercises provided throughout to enable beginning undergraduates to get to grips with this important analytical technique.

NMR Spectroscopy Explained

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Publisher : John Wiley & Sons
ISBN 13 : 0470173343
Total Pages : 640 pages
Book Rating : 4.4/5 (71 download)

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Book Synopsis NMR Spectroscopy Explained by : Neil E. Jacobsen

Download or read book NMR Spectroscopy Explained written by Neil E. Jacobsen and published by John Wiley & Sons. This book was released on 2007-09-10 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.

Modern NMR Techniques for Chemistry Research

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Publisher : Elsevier
ISBN 13 : 1483286428
Total Pages : 299 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis Modern NMR Techniques for Chemistry Research by : A.E. Derome

Download or read book Modern NMR Techniques for Chemistry Research written by A.E. Derome and published by Elsevier. This book was released on 2013-10-22 with total page 299 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.

NMR in Chemistry

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Publisher : Free Press
ISBN 13 : 9780029494011
Total Pages : 240 pages
Book Rating : 4.4/5 (94 download)

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Book Synopsis NMR in Chemistry by : William Kemp

Download or read book NMR in Chemistry written by William Kemp and published by Free Press. This book was released on 1988 with total page 240 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Applications of NMR Spectroscopy

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Publisher : Bentham Science Publishers
ISBN 13 : 168108287X
Total Pages : 289 pages
Book Rating : 4.6/5 (81 download)

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Book Synopsis Applications of NMR Spectroscopy by : Atta-ur-Rahman

Download or read book Applications of NMR Spectroscopy written by Atta-ur-Rahman and published by Bentham Science Publishers. This book was released on 2016-11-22 with total page 289 pages. Available in PDF, EPUB and Kindle. Book excerpt: Applications of NMR Spectroscopy is a book series devoted to publishing the latest advances in the applications of nuclear magnetic resonance (NMR) spectroscopy in various fields of organic chemistry, biochemistry, health and agriculture. The fifth volume of the series features several reviews focusing on NMR spectroscopic techniques for identifying natural and synthetic compounds (polymer and peptide characterization, GABA in tinnitus affected mice), medical diagnosis and therapy (gliomas) and food analysis. The spectroscopic methods highlighted in this volume include high resolution proton magnetic resonance spectroscopy and solid state NMR.

NMR Spectroscopy in Organic Chemistry

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Publisher : Springer Science & Business Media
ISBN 13 : 1468417851
Total Pages : 396 pages
Book Rating : 4.4/5 (684 download)

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Book Synopsis NMR Spectroscopy in Organic Chemistry by : B. I. Ionin

Download or read book NMR Spectroscopy in Organic Chemistry written by B. I. Ionin and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 396 pages. Available in PDF, EPUB and Kindle. Book excerpt: In recent years high-resolution nuclear magnetic resonance spec troscopy has found very wide application in organie chemistry in structural and physicochemical investigations and. also in the study of the characteristics of organic compounds which are re lated to the distribution of the electron cloud in the molecules. The vigorous development of this method, which may really be re garded as an independent branch of science, is the result of ex tensive progress in NMR technology, the refinement of its theory, and the accumulation of large amounts of experimental material, which has been correlated by empiricallaws and principles. The literature directly concerned with the NMR method and its applica tion has now grown to such an extent that a complete review of it is practically impossible. Therefore the authors have limited themselves to an examination of only the most important, funda mental, and general investigations. The book consists of six chapters. In the first chapter we have attempted to present the fundamentals of the NMR method in such a way that the reader with little knowledge of the subject will be able to use the method in practical work for investigating simple compounds and solving simple problems. The three subsequent chapters give a deeper analysis of the method, while the last two chapters and the appendix illustrate the various applications of NMR spectroscopy in organic chemistry.

NMR Spectroscopy

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Author :
Publisher : John Wiley & Sons
ISBN 13 : 3527330003
Total Pages : 739 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis NMR Spectroscopy by : Harald Günther

Download or read book NMR Spectroscopy written by Harald Günther and published by John Wiley & Sons. This book was released on 2013-11-04 with total page 739 pages. Available in PDF, EPUB and Kindle. Book excerpt: Auch die komplett überarbeitete 3. Auflage dieses bewährten Lehrbuchs überzeugt durch Klarheit, eine didaktisch gelungene Aufbereitung des Stoffes und ein hohes Maß an Praxisbezug. Das komplexe Thema wird mit einem Mindestmaß an Mathematik erklärt - ideal für Studenten, die die Grundlagen der NMR-Spektroskopie verstehen und das Verfahren effizient und präzise anwenden möchten. Die neue Auflage ist vollständig überarbeitet und aktualisiert. So sind rund 25% der Inhalte neu, darunter auch Kapitel zur biologischen NMR-Spektroskopie sowie viele Beispiele aus der organischen Chemie. Daher stellt dieses Fachbuch auch für Studenten in Grund- und Hauptstudium verwandter Fachrichtungen wie der Biochemie, Medizinischen Chemie, Pharmazeutischen Chemie und Materialwissenschaften einen wertvollen Leitfaden dar. Außerdem findet der Leser eine Vielzahl von Übungsaufgaben mit zugehörigen Lösungen.

Modern NMR Spectroscopy

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Publisher : Oxford University Press, USA
ISBN 13 :
Total Pages : 150 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis Modern NMR Spectroscopy by : Jeremy K. M. Sanders

Download or read book Modern NMR Spectroscopy written by Jeremy K. M. Sanders and published by Oxford University Press, USA. This book was released on 1993 with total page 150 pages. Available in PDF, EPUB and Kindle. Book excerpt: Erros I have made; Interpretation of spectra; Symmetry and exchange; Structure determination using NMR alone; Structure and mechanism; Hints; Solutions.

NMR in Supramolecular Chemistry

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Publisher : Springer Science & Business Media
ISBN 13 : 0792356217
Total Pages : 360 pages
Book Rating : 4.7/5 (923 download)

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Book Synopsis NMR in Supramolecular Chemistry by : Miquel Pons

Download or read book NMR in Supramolecular Chemistry written by Miquel Pons and published by Springer Science & Business Media. This book was released on 1999-03-31 with total page 360 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR is better suited than any other experimental technique for the characterization of supramolecular systems in solution. The presentations included here can be broadly divided into three classes. The first class illustrates the state of the art in the design of supramolecular systems and includes examples of different classes of supramolecular complexes: catenanes, rotaxanes, hydrogen-bonded rosettes, tubes, capsules, dendrimers, and metal-containing hosts. The second class comprises contributions to NMR methods that can be applied to address the main structural problems that arise in supramolecular chemistry. The third class includes biological supramolecular systems studied by state-of-the-art NMR techniques.

NMR and Chemistry

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Publisher : CRC Press
ISBN 13 : 1351991124
Total Pages : 422 pages
Book Rating : 4.3/5 (519 download)

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Book Synopsis NMR and Chemistry by : J.W. Akitt

Download or read book NMR and Chemistry written by J.W. Akitt and published by CRC Press. This book was released on 2017-12-21 with total page 422 pages. Available in PDF, EPUB and Kindle. Book excerpt: Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.

Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry

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Publisher : Elsevier
ISBN 13 : 1483280942
Total Pages : 474 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry by : L. M. Jackman

Download or read book Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry written by L. M. Jackman and published by Elsevier. This book was released on 2013-10-22 with total page 474 pages. Available in PDF, EPUB and Kindle. Book excerpt: Application of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry, Second Edition covers the theoretical background necessary for the intelligent application of NMR spectroscopy to common problems encountered in organic chemistry. This book is composed of five parts, and begins with introduction to the theory and practice of nuclear magnetic resonance. The succeeding chapter deals with the theory of chemical effects in NMR spectroscopy. These topics are followed by a discussion on the application of chemical shift to organic compound analysis and the principles of the spin-spin coupling .The final chapter considers the applications of time- dependent phenomena in NMR spectroscopy. This book will prove useful to analytical chemists and researchers in the allied fields.

NMR

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Publisher : Oxford University Press, USA
ISBN 13 : 0198703422
Total Pages : 133 pages
Book Rating : 4.1/5 (987 download)

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Book Synopsis NMR by : P. J. Hore

Download or read book NMR written by P. J. Hore and published by Oxford University Press, USA. This book was released on 2015 with total page 133 pages. Available in PDF, EPUB and Kindle. Book excerpt: This primer describes the range of NMR techniques commonly used in modern research, and explains how these experiments actually work, giving a unique perspective on this powerful experimental tool.

Nuclear Magnetic Resonance

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Publisher : Royal Society of Chemistry
ISBN 13 : 1847553869
Total Pages : 584 pages
Book Rating : 4.8/5 (475 download)

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Book Synopsis Nuclear Magnetic Resonance by : G A Webb

Download or read book Nuclear Magnetic Resonance written by G A Webb and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 584 pages. Available in PDF, EPUB and Kindle. Book excerpt: As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

Solid State NMR

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Publisher : John Wiley & Sons
ISBN 13 : 352731816X
Total Pages : 562 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Solid State NMR by : Klaus Müller

Download or read book Solid State NMR written by Klaus Müller and published by John Wiley & Sons. This book was released on 2021-08-23 with total page 562 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences. Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook: Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopy Provides helpful illustrations to explain the various SSNMR concepts and methods Features accessible descriptive text with self-consistent use of quantum mechanics Covers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequences Contains references to relevant literature Solid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.