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Author : Robin Kingsley Harris
Publisher :
ISBN 13 :
Total Pages : 496 pages
Book Rating : 4.4/5 (91 download)
Download or read book NMR and the Periodic Table written by Robin Kingsley Harris and published by . This book was released on 1978 with total page 496 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : J.W. Akitt
Publisher : CRC Press
ISBN 13 : 148226837X
Total Pages : 400 pages
Book Rating : 4.4/5 (822 download)
Download or read book NMR and Chemistry written by J.W. Akitt and published by CRC Press. This book was released on 2017-12-21 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt: Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.
![Download Insights from Across the Periodic Table Into NMR Chemical Shift, Electric Field Gradient, and Spin-spin Coupling Tensors [microform] : New Information from Solid-state NMR and Computational Chemistry PDF Online Free](https://books.google.com/books/content/images/frontcover/8VkIywAACAAJ?fife=w200-h370)
Author : David L. (David Lawson) Bryce
Publisher : National Library of Canada = Bibliothèque nationale du Canada
ISBN 13 : 9780612756946
Total Pages : 488 pages
Book Rating : 4.7/5 (569 download)
Download or read book Insights from Across the Periodic Table Into NMR Chemical Shift, Electric Field Gradient, and Spin-spin Coupling Tensors [microform] : New Information from Solid-state NMR and Computational Chemistry written by David L. (David Lawson) Bryce and published by National Library of Canada = Bibliothèque nationale du Canada. This book was released on 2002 with total page 488 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : D. Michael P. Mingos
Publisher : Springer Nature
ISBN 13 : 3030400107
Total Pages : 250 pages
Book Rating : 4.0/5 (34 download)
Download or read book The Periodic Table II written by D. Michael P. Mingos and published by Springer Nature. This book was released on 2020-02-05 with total page 250 pages. Available in PDF, EPUB and Kindle. Book excerpt: As 2019 has been declared the International Year of the Periodic Table, it is appropriate that Structure and Bonding marks this anniversary with two special volumes. In 1869 Dmitri Ivanovitch Mendeleev first proposed his periodic table of the elements. He is given the major credit for proposing the conceptual framework used by chemists to systematically inter-relate the chemical properties of the elements. However, the concept of periodicity evolved in distinct stages and was the culmination of work by other chemists over several decades. For example, Newland’s Law of Octaves marked an important step in the evolution of the periodic system since it represented the first clear statement that the properties of the elements repeated after intervals of 8. Mendeleev’s predictions demonstrated in an impressive manner how the periodic table could be used to predict the occurrence and properties of new elements. Not all of his many predictions proved to be valid, but the discovery of scandium, gallium and germanium represented sufficient vindication of its utility and they cemented its enduring influence. Mendeleev’s periodic table was based on the atomic weights of the elements and it was another 50 years before Moseley established that it was the atomic number of the elements, that was the fundamental parameter and this led to the prediction of further elements. Some have suggested that the periodic table is one of the most fruitful ideas in modern science and that it is comparable to Darwin’s theory of evolution by natural selection, proposed at approximately the same time. There is no doubt that the periodic table occupies a central position in chemistry. In its modern form it is reproduced in most undergraduate inorganic textbooks and is present in almost every chemistry lecture room and classroom. This second volume provides chemists with an overview of the important role played by the Periodic Table in advancing our knowledge of solid state and bioinorganic chemistry. It also illustrates how it has been used to fine-tune the properties of compounds which have found commercial applications in catalysis, electronics, ceramics and in medicinal chemistry.
Author : J.B. Lambert
Publisher : Springer Science & Business Media
ISBN 13 : 9400971303
Total Pages : 552 pages
Book Rating : 4.4/5 (9 download)
Download or read book The Multinuclear Approach to NMR Spectroscopy written by J.B. Lambert and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 552 pages. Available in PDF, EPUB and Kindle. Book excerpt: The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispersion. In areas of new applicat ions, the life sciences particularly bene fited from these developments and probably saw the largest increase in usage. NMR imaging promises to offer a noninvasive alternative to X rays. High resolution is now achievable with solids, through magic angle spinning and cross polarization, so that the powers of NMR are applicable to previously intractable materials such as polymers, coal, and other geochemicals. The ease of obtaining relaxation times brought an important fourth variable, after the chemical shift, the coupling constant, and the rate constant, to the examination of structural and kinetic problems i~ all fields. Software development, particularly in the area of pulse sequences, created a host of useful tech niques, including difference decoupling and difference nuclear Overhauser effect spectra, multidimensional displays, signal enhancement (INEPT), coupling constant analysis for connectivity (INADEQUATE), and observation of specific structural classes such as only quaternary carbons. Finally, hardware development gave us access to the entire Periodic Table, to the particular advan tage of the inorganic and organometallic chemist. At the NATO Advanced Study Institute at Stirling, Scotland, the participants endeavored to examine all these advances, except imaging, from a multidisciplinary point of view.
Author : J. W. Akitt
Publisher :
ISBN 13 :
Total Pages : 400 pages
Book Rating : 4.:/5 (125 download)
Download or read book NMR and Chemistry written by J. W. Akitt and published by . This book was released on 2000 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Geoffrey Rayner-canham
Publisher : World Scientific
ISBN 13 : 9811218501
Total Pages : 311 pages
Book Rating : 4.8/5 (112 download)
Download or read book Periodic Table, The: Past, Present, And Future written by Geoffrey Rayner-canham and published by World Scientific. This book was released on 2020-08-04 with total page 311 pages. Available in PDF, EPUB and Kindle. Book excerpt: 'This is an an absolutely wonderful book that is full of gems about the elements and the periodic table … All in all, the book is highly recommended to philosophers of chemistry. As philosophers we have a natural tendency to concentrate on generalities and not to get too involved in the specifics and the details. Above all else, this new book reminds us that such an approach needs to be tempered by a detailed knowledge of the exceptions and features that go against the simplified generalities which we so cherish.' [Read Full Review]Eric ScerriFoundations of Chemistry'Many questions are dealt with in a clearly written way in this stimulating and innovative book. The reader will quickly become interested in the subject and will be taken on tour through this Periodic Table in a very readable way, both for students and teachers … The number of illustrations is good, and clear. This book is indeed unique and quite thought-provoking … This book is highly recommended for students, teachers, researchers and not only chemists! Geologists, biochemist and also physicists will find it very interesting to read.' [Read Full Review]Chemistry InternationalThat fossilized chart on every classroom wall — isn't that The Periodic Table? Isn't that what Mendeléev devised about a century ago? No and No. There are many ways of organizing the chemical elements, some of which are thought-provoking, and which reveal philosophical challenges. Where does hydrogen 'belong'? Can an element occupy more than one location on the chart? Which are the Group 3 elements? Is aluminum in the wrong place? Why is silver(I) like thallium(I)? Why is vanadium like molybdenum? Why does gold form an auride ion like a halide ion? Does an atom 'know' if it is a non-metal or metal? Which elements are the 'metalloids'? Which are the triels? So many questions! In this stimulating and innovative book, the Reader will be taken on a voyage from the past to the present to the future of the Periodic Table. This book is unique. This book is readable. This book is thought-provoking. It is a multi-dimensional examination of patterns and trends among the chemical elements. Every reader will discover something about the chemical elements which will provoke thought and a new appreciation as to how the elements relate together.
Author :
Publisher : Springer
ISBN 13 : 9783642877636
Total Pages : 238 pages
Book Rating : 4.8/5 (776 download)
Download or read book Oxygen-17 and Silicon-29 written by and published by Springer. This book was released on 2014-03-12 with total page 238 pages. Available in PDF, EPUB and Kindle. Book excerpt: Although it was shown very early [1] that the isotope 29Si is very valuable for NMR research, severe technical difficulties had to be overcome before silicon spectra could be recorded. This was due to the low sensitivity of the isotope resulting from its low gyro magnetic ratio, its low abundance and the rather long relaxation times. The introduction of the Fourier-Transform-Technique (FT-NMR) helped to surmount most of these problems, with the result, that more and more papers concerning silicon NMR appear. Thus, it seems now that most of the salient features of 29Si-NMR are known today. Some resume of the state of the art of 29Si_NMR have been reported [1-4]. Although the theory of 29Si-NMR is not yet understood beyond the basic features, it promises to be of value mainly for two reasons: 1. Silicon is strategically located in the Periodic Table of the elements between the elements carbon, aluminum and phosphorus. For an unified theory of chemical shifts and coupling constants of the heavier elements silicon NMR values will be important. 2. The normal coordination number of silicon is four. If the current view of the chemical shifts of the heavier elements is correct, then the paramagnetic part is dominant for the measured shift data. Two of the parameters used for the calcu lation of the paramagnetic part are bond orders and angles. Bond angles are rare ly determined experimentally with high precision.
Author : J. Mason
Publisher : Springer Science & Business Media
ISBN 13 : 1461317835
Total Pages : 642 pages
Book Rating : 4.4/5 (613 download)
Download or read book Multinuclear NMR written by J. Mason and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 642 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the power and range of modern pulse spectrometers the compass of NMR spec troscopy is now very large for a single book-but we have undertaken this. Our book covers the Periodic Table as multinuclear spectrometers do, and introductory chapters are devoted to the essentials of the NMR experiment and its products. Primary products are chemical shifts (including anisotropies), spin-spin coupling constants, and relaxation times; the ultimate product is a knowledge of content and constitution, dynamic as well as static. Our province is chemical and biochemical rather than physical or technical; only passing reference is made to metallic solids or unstable species, or to practical NMR spectroscopy. Our aim is depth as well as breadth, to explain the fundamental processes, whether of nuclear magnetic shielding, spin-spin coupling, relaxation, or the multiple pulse sequences that have allowed the development of high-resolution studies of solids, multidimensional NMR spectroscopy, techniques for sensitivity enhancement, and so on. This book therefore combines the functions of advanced textbook and reference book. For reasonably comprehensive coverage in a single volume we have sum marized the information in tables and charts, and included all leading references.
Author :
Publisher : Springer
ISBN 13 : 9783642877643
Total Pages : 238 pages
Book Rating : 4.8/5 (776 download)
Download or read book Oxygen-17 and Silicon-29 written by and published by Springer. This book was released on 2014-08-23 with total page 238 pages. Available in PDF, EPUB and Kindle. Book excerpt: Although it was shown very early [1] that the isotope 29Si is very valuable for NMR research, severe technical difficulties had to be overcome before silicon spectra could be recorded. This was due to the low sensitivity of the isotope resulting from its low gyro magnetic ratio, its low abundance and the rather long relaxation times. The introduction of the Fourier-Transform-Technique (FT-NMR) helped to surmount most of these problems, with the result, that more and more papers concerning silicon NMR appear. Thus, it seems now that most of the salient features of 29Si-NMR are known today. Some resume of the state of the art of 29Si_NMR have been reported [1-4]. Although the theory of 29Si-NMR is not yet understood beyond the basic features, it promises to be of value mainly for two reasons: 1. Silicon is strategically located in the Periodic Table of the elements between the elements carbon, aluminum and phosphorus. For an unified theory of chemical shifts and coupling constants of the heavier elements silicon NMR values will be important. 2. The normal coordination number of silicon is four. If the current view of the chemical shifts of the heavier elements is correct, then the paramagnetic part is dominant for the measured shift data. Two of the parameters used for the calcu lation of the paramagnetic part are bond orders and angles. Bond angles are rare ly determined experimentally with high precision.
Author : Thomas J. Bruno
Publisher : CRC Press
ISBN 13 : 1351613154
Total Pages : 900 pages
Book Rating : 4.3/5 (516 download)
Download or read book CRC Handbook of Basic Tables for Chemical Analysis written by Thomas J. Bruno and published by CRC Press. This book was released on 2020-07-30 with total page 900 pages. Available in PDF, EPUB and Kindle. Book excerpt: Researchers in chemistry, chemical engineering, pharmaceutical science, forensics, and environmental science make routine use of chemical analysis, but the information these researchers need is often scattered in different sources and difficult to access. The CRC Handbook of Basic Tables for Chemical Analysis: Data-Driven Methods and Interpretation, Fourth Edition is a one-stop reference that presents updated data in a handy format specifically designed for use when reaching a decision point in designing an analysis or interpreting results. This new edition offers expanded coverage of calibration and uncertainty, and continues to include the critical information scientists rely on to perform accurate analysis. Enhancements to the Fourth Edition: Compiles a huge array of useful and important data into a single, convenient source Explanatory text provides context for data and guidelines on applications Coalesces information from several different fields Provides information on the most useful "wet" chemistry methods as well as instrumental techniques, with an expanded discussion of laboratory safety Contains information of historical importance necessary to interpret the literature and understand current methodology. Unmatched in its coverage of the range of information scientists need in the lab, this resource will be referred to again and again by practitioners who need quick, easy access to the data that forms the basis for experimentation and analysis.
Author : John A. R. Newlands
Publisher :
ISBN 13 :
Total Pages : 68 pages
Book Rating : 4.0/5 ( download)
Download or read book On the Discovery of the Periodic Law, and on Relations Among the Atomic Weights written by John A. R. Newlands and published by . This book was released on 1884 with total page 68 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Emeritus Professor and Wei Lun Research Professor Thomas Cw Mak
Publisher : Oxford University Press
ISBN 13 : 019887295X
Total Pages : 593 pages
Book Rating : 4.1/5 (988 download)
Download or read book Structural Chemistry Across the Periodic Table written by Emeritus Professor and Wei Lun Research Professor Thomas Cw Mak and published by Oxford University Press. This book was released on 2023-10-12 with total page 593 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is an expanded and updated version of Part III of the authors' previous work, Advanced Structural Inorganic Chemistry (OUP 2008). The original part deals with main-group elements, the rare-earth elements, transition-metal clusters, and supramolecular systems. In this new book, selected material from significant advances in the past decade has been added, with particular emphasis on compounds that exemplify new types of bonds such as sigma-hole, triel bond, tetrel bond, pnictogen bond, chalcogen bond, halogen bond, halogen-halogen interaction, aerogen bond, as well as quintuple and sextuple metal-metal bonds. Other new topics include actinide compounds, metallophilicity, heterometallic macrocycles and cages, com- and dis-proportionation reactions, hydrogen-bonded organic frameworks (HOFs), halogen-bonded organic frameworks, halogen-halogen interactions in supramolecular frameworks, covalent organic frameworks (COFs), and metal-organic frameworks (MOFs).
Author : Atta-ur-Rahman
Publisher : Bentham Science Publishers
ISBN 13 : 168108287X
Total Pages : 289 pages
Book Rating : 4.6/5 (81 download)
Download or read book Applications of NMR Spectroscopy written by Atta-ur-Rahman and published by Bentham Science Publishers. This book was released on 2016-11-22 with total page 289 pages. Available in PDF, EPUB and Kindle. Book excerpt: Applications of NMR Spectroscopy is a book series devoted to publishing the latest advances in the applications of nuclear magnetic resonance (NMR) spectroscopy in various fields of organic chemistry, biochemistry, health and agriculture. The fifth volume of the series features several reviews focusing on NMR spectroscopic techniques for identifying natural and synthetic compounds (polymer and peptide characterization, GABA in tinnitus affected mice), medical diagnosis and therapy (gliomas) and food analysis. The spectroscopic methods highlighted in this volume include high resolution proton magnetic resonance spectroscopy and solid state NMR.
Author : Carmen J. Giunta
Publisher : Springer Nature
ISBN 13 : 3030679101
Total Pages : 453 pages
Book Rating : 4.0/5 (36 download)
Download or read book 150 Years of the Periodic Table written by Carmen J. Giunta and published by Springer Nature. This book was released on 2021-07-04 with total page 453 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides an overview of the origins and evolution of the periodic system from its prehistory to the latest synthetic elements and possible future additions. The periodic system of the elements first emerged as a comprehensive classificatory and predictive tool for chemistry during the 1860s. Its subsequent embodiment in various versions has made it one of the most recognizable icons of science. Based primarily on a symposium titled “150 Years of the Periodic Table” and held at the August 2019 national meeting of the American Chemical Society, this book describes the origins of the periodic law, developments that led to its acceptance, chemical families that the system struggled to accommodate, extension of the periodic system to include synthetic elements, and various cultural aspects of the system that were celebrated during the International Year of the Periodic Table.
Author : D. Michael P. Mingos
Publisher : Springer Nature
ISBN 13 : 3030400255
Total Pages : 274 pages
Book Rating : 4.0/5 (34 download)
Download or read book The Periodic Table I written by D. Michael P. Mingos and published by Springer Nature. This book was released on 2020-02-05 with total page 274 pages. Available in PDF, EPUB and Kindle. Book excerpt: As 2019 has been declared the International Year of the Periodic Table, it is appropriate that Structure and Bonding marks this anniversary with two special volumes. In 1869 Dmitri Ivanovitch Mendeleev first proposed his periodic table of the elements. He is given the major credit for proposing the conceptual framework used by chemists to systematically inter-relate the chemical properties of the elements. However, the concept of periodicity evolved in distinct stages and was the culmination of work by other chemists over several decades. For example, Newland’s Law of Octaves marked an important step in the evolution of the periodic system since it represented the first clear statement that the properties of the elements repeated after intervals of 8. Mendeleev’s predictions demonstrated in an impressive manner how the periodic table could be used to predict the occurrence and properties of new elements. Not all of his many predictions proved to be valid, but the discovery of scandium, gallium and germanium represented sufficient vindication of its utility and they cemented its enduring influence. Mendeleev’s periodic table was based on the atomic weights of the elements and it was another 50 years before Moseley established that it was the atomic number of the elements, that was the fundamental parameter and this led to the prediction of further elements. Some have suggested that the periodic table is one of the most fruitful ideas in modern science and that it is comparable to Darwin’s theory of evolution by natural selection, proposed at approximately the same time. There is no doubt that the periodic table occupies a central position in chemistry. In its modern form it is reproduced in most undergraduate inorganic textbooks and is present in almost every chemistry lecture room and classroom. This first volume provides chemists with an account of the historical development of the Periodic Table and an overview of how the Periodic Table has evolved over the last 150 years. It also illustrates how it has guided the research programmes of some distinguished chemists.
Author : James W. Robinson
Publisher : CRC Press
ISBN 13 : 0849306507
Total Pages : 1107 pages
Book Rating : 4.8/5 (493 download)
Download or read book Undergraduate Instrumental Analysis, Sixth Edition written by James W. Robinson and published by CRC Press. This book was released on 2004-12-02 with total page 1107 pages. Available in PDF, EPUB and Kindle. Book excerpt: Completely rewritten, revised, and updated, this Sixth Edition reflects the latest technologies and applications in spectroscopy, mass spectrometry, and chromatography. It illustrates practices and methods specific to each major chemical analytical technique while showcasing innovations and trends currently impacting the field. Many of the chapters have been individually reviewed by teaching professors and include descriptions of the fundamental principles underlying each technique, demonstrations of the instrumentation, and new problem sets and suggested experiments appropriate to the topic. About the authors... JAMES W. ROBINSON is Professor Emeritus of Chemistry, Louisiana State University, Baton Rouge. A Fellow of the Royal Chemical Society, he is the author of over 200 professional papers and book chapters and several books including Atomic Absorption Spectroscopy and Atomic Spectroscopy. He was Executive Editor of Spectroscopy Letters and the Journal of Environmental Science and Health (both titles, Marcel Dekker, Inc.) and the Handbook of Spectroscopy and the Practical Handbook of Spectroscopy (both titles, CRC Press). He received the B.Sc. (1949), Ph.D. (1952), and D.Sc. (1978) degrees from the University of Birmingham, England. EILEEN M. SKELLY FRAME recently was Clinical Assistant Professor and Visiting Research Professor, Rensselaer Polytechnic Institute, Troy, New York. Dr. Skelly Frame has extensive practical experience in the use of instrumental analysis to characterize a wide variety of substances, from biological samples and cosmetics to high temperature superconductors, polymers, metals, and alloys. Her industrial career includes supervisory roles at GE Corporate Research and Development, Stauffer Chemical Corporate R&D, and the Research Triangle Institute. She is a member of the American Chemical Society, the Society for Applied Spectroscopy, and the American Society for Testing and Materials. Dr. Skelly Frame received the B.S. degree in chemistry from Drexel University, Philadelphia, Pennsylvania, and the Ph.D. in analytical chemistry from Louisiana State University, Baton Rouge. GEORGE M. FRAME II is Scientific Director, Chemical Biomonitoring Section of the Wadsworth Laboratory, New York State Department of Health, Albany. He has a wide range of experience in the field and has worked at the GE Corporate R&D Center, Pfizer Central Research, the U.S. Coast Guard R&D Center, the Maine Medical Center, and the USAF Biomedical Sciences Corps. He is an American Chemical Society member. Dr. Frame received the B.A. degree in chemistry from Harvard College, Cambridge, Massachusetts, and the Ph.D. degree in analytical chemistry from Rutgers University, New Brunswick, New Jersey.
