Microextraction Techniques In Analytical Toxicology

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Microextraction Techniques in Analytical Toxicology

Author : Rajeev Jain
Publisher : CRC Press
ISBN 13 : 1000473740
Total Pages : 268 pages
Book Rating : 4.0/5 (4 download)

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Book Synopsis Microextraction Techniques in Analytical Toxicology by : Rajeev Jain

Download or read book Microextraction Techniques in Analytical Toxicology written by Rajeev Jain and published by CRC Press. This book was released on 2021-12-31 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microextraction Techniques in Analytical Toxicology provides the information readers need to include about cutting-edge sample preparation techniques into their everyday analytical practice, including comprehensive information about principles and state-of-the-art microextraction sample preparation techniques for the analysis of drugs and poisons in biological specimens, especially in forensic and clinical settings. This book also focuses on theoretical discussions of solid-based and liquid-based microextraction techniques, their method development, validation, and applications. A detailed compilation of analytical protocols based on published microextraction procedures to aid in method development, synthesis, and the application of green solvents (ionic liquids and deep eutectic solvents) and new sorbents, such as molecularly imprinted polymers, and their application in microextraction techniques are also covered. Features: Provides a systematic review of microextraction techniques applied in analytical toxicology A comprehensive guide for the practical implementation of microextraction techniques in forensic, clinical, and analytical laboratories Contains figures and tables for easy understanding and quick adaptation of the parameters of microextraction techniques Fundamentals, development, and applications of microextraction techniques as a sample preparation procedure are discussed in detail Extremely useful for the researchers and academicians engaged in analytical method development using microextraction techniques This book appeals to a wide readership of forensic, clinical, and analytical toxicologists, as well as academicians and researchers. Written by eminent scientists and leading experts on sample preparation techniques, this book serves as a desk reference for routine laboratory analysis and as an indispensable teaching tool in the classroom for graduate and Ph.D. students.

Analytical Microextraction Techniques

Author : M. Valcárcel
Publisher : Bentham Science Publishers
ISBN 13 : 1681083795
Total Pages : 430 pages
Book Rating : 4.6/5 (81 download)

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Book Synopsis Analytical Microextraction Techniques by : M. Valcárcel

Download or read book Analytical Microextraction Techniques written by M. Valcárcel and published by Bentham Science Publishers. This book was released on 2017-01-13 with total page 430 pages. Available in PDF, EPUB and Kindle. Book excerpt: Sample treatment has been the focus of intensive research in the last 20 years since it still remains a bottleneck in precise analytical procedures. The low concentration of the target analytes, the large amount of potential interfering agents and the incompatibility of the sample matrix with the instrumental techniques are the main reasons for these bottlenecks. In most of these methods, sample treatment is an unavoidable step and it has a clear influence on the quality (sensitivity, selectivity, and accuracy) of the final analytical results. While the usefulness of microextraction techniques has been established, their complete acceptance in analytical laboratories (including official methods of analysis) depends on their successful automation and integration with conventional analytical instrumentation. Analytical Microextraction Techniques presents comprehensive information about several analytical methods that are useful in the laboratory. These include: sorptive microextraction, solid and liquid phase microextraction, packed sorbent microextraction, miniaturized dispersive solid-phase extraction, thin film and nanoparticle based techniques, and membrane-based techniques. This is a vital reference on microextraction and sample preparation techniques for applied chemistry students, analytical chemists and laboratory technicians.

Microextraction Techniques

Author : Miguel Ángel Rodríguez-Delgado
Publisher : Springer
ISBN 13 : 9783031505263
Total Pages : 0 pages
Book Rating : 4.5/5 (52 download)

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Book Synopsis Microextraction Techniques by : Miguel Ángel Rodríguez-Delgado

Download or read book Microextraction Techniques written by Miguel Ángel Rodríguez-Delgado and published by Springer. This book was released on 2024-03-16 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents detailed descriptions of the most relevant sorbent based and solvent-based microextraction techniques. The development of such miniaturised techniques is an important focus area in Green Analytical Chemistry as it allows for the reduction of toxic solvents and hazardous substances and decreases the complexity, cost, and time of analytical procedures. Numerous advances have been made in this field, and currently, there are a great number of microextraction techniques thanks to the development of novel materials such as nanomaterials and green solvents. This book provides an overview of the two main groups of microextractions, sorbent-based, and solvent-based. Each chapter focuses on the description of the technique fundamentals, the main applications, and the novel developments carried out in recent years written by a renowned expert or group of experts in the field. The main audience will be graduates, postgraduates, and researchers. It is also a useful resource for Master and Ph.D. students that are working in the development of sustainable extraction techniques

Solvent Microextraction

Author : John M Kokosa
Publisher : John Wiley & Sons
ISBN 13 : 0470278595
Total Pages : 340 pages
Book Rating : 4.4/5 (72 download)

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Book Synopsis Solvent Microextraction by : John M Kokosa

Download or read book Solvent Microextraction written by John M Kokosa and published by John Wiley & Sons. This book was released on 2009-10-05 with total page 340 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book offers both a practical as well a theoretical approach to Solvent Microextraction (SME) and will help analytical chemists to evaluate SME for a given sample preparation. Introductory chapters overview a comparison of SME with other sample preparation methods, a summary of the technical aspects, and a detailed theoretical treatment of SME. The book then describes the practical aspects of the technique, with detailed “how to” chapters devoted to the preparation and analysis of atmospheric, solid and liquid environmental, clinical and industrial samples. This text will serve as both a handy laboratory desk-reference and an indispensible instructional tool.

Forensic and Clinical Applications of Solid Phase Extraction

Author : Michael J. Telepchak
Publisher : Springer Science & Business Media
ISBN 13 : 1592592929
Total Pages : 398 pages
Book Rating : 4.5/5 (925 download)

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Book Synopsis Forensic and Clinical Applications of Solid Phase Extraction by : Michael J. Telepchak

Download or read book Forensic and Clinical Applications of Solid Phase Extraction written by Michael J. Telepchak and published by Springer Science & Business Media. This book was released on 2004-04-28 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt: This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.

Fundamentals of Analytical Toxicology

Author : Robert J. Flanagan
Publisher : John Wiley & Sons
ISBN 13 : 0470319348
Total Pages : 605 pages
Book Rating : 4.4/5 (73 download)

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Book Synopsis Fundamentals of Analytical Toxicology by : Robert J. Flanagan

Download or read book Fundamentals of Analytical Toxicology written by Robert J. Flanagan and published by John Wiley & Sons. This book was released on 2008-03-03 with total page 605 pages. Available in PDF, EPUB and Kindle. Book excerpt: The analytical toxicologist may be required to detect, identify, and in many cases measure a wide variety of compounds in samples from almost any part of the body or in related materials such as residues in syringes or in soil. This book gives principles and practical information on the analysis of drugs and poisons in biological specimens, particularly clinical and forensic specimens. After providing some background information the book covers aspects of sample collection, transport, storage and disposal, and sample preparation. Analytical techniques - colour tests and spectrophotometry, chromatography and electrophoresis, mass spectrometry, and immunoassay – are covered in depth, and a chapter is devoted to the analysis of trace elements and toxic metals. General aspects of method implementation/validation and laboratory operation are detailed, as is the role of the toxicology laboratory in validating and monitoring the performance of point of care testing (POCT) devices. The book concludes with reviews of xenobiotic absorption, distribution and metabolism, pharmacokinetics, and general aspects of the interpretation of analytical toxicology results. A clearly written, practical, integrated approach to the basics of analytical toxicology. Focuses on analytical, statistical and pharmacokinetic principles rather than detailed applications. Assumes only a basic knowledge of analytical chemistry. An accompanying website provides additional material and links to related sites. Written by an experienced team of authors,Fundamentals of Analytical Toxicology is an invaluable resource for those starting out in a career in analytical toxicology across a wide range of disciplines including clinical and forensic science, food safety, and pharmaceutical development. Praise from the reviews: “This is an ambitious effort to describe in detail the many and varied aspects of the science of toxicological analysis. The 17 chapters cover every foreseeable aspect, from specimen collection through analytical techniques and quality control to pharmacological principles and interpretation of results. The authors bring together a great deal of experience in the field and have succeeded admirably in achieving their goal: "to give principles and practical information on the analysis of drugs, poisons and other relevant analytes in biological specimens...". The book is very readable and quite up-to-date, and contains many illustrative figures, charts and tables. Both the student and the practicing professional would do well to study this material carefully, as there is something here for every conceivable level of interest.” Review from Randall Baselt "This text comes highly recommended for any analytical toxicology trainee." The Bulletin of the Royal College of Pathologists “Overall, this book provides a comprehensive, thorough, clear, up to date and practical treatment of analytical toxicology at a high standard. Understanding of the text is enhanced by the use of many illustrations. Specifications, guidelines, and methods are highlighted in grey background “Boxes”. The many and up to date literature references in each chapter demonstrate the authors’ thorough work and permit easy access to deeper information. Therefore this book can be highly recommended as a valuable source of knowledge in analytical toxicology both as an introduction and for the advanced reader.” GTFCh Bulletin “Toxichem + Krimtech”, May 2008 (translated, original review in German) “Many toxicologists will add this important reference to their libraries because it competently fills a need ...” International Journal of Toxicology “The book is very well illustrated, easy to understand and pleasant to read, and contains a wealth of dedicated information.” International Journal of Environmental Analytical Chemistry

Solid Phase Microextraction

Author : Gangfeng Ouyang
Publisher : Springer
ISBN 13 : 366253598X
Total Pages : 313 pages
Book Rating : 4.6/5 (625 download)

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Book Synopsis Solid Phase Microextraction by : Gangfeng Ouyang

Download or read book Solid Phase Microextraction written by Gangfeng Ouyang and published by Springer. This book was released on 2016-11-24 with total page 313 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book offers comprehensive information on the developments and applications of the solid phase microextraction (SPME) technique. The first part of the book briefly introduces readers to the fundamentals of SPME, while subsequent sections describe the applications of SPME technique in detail, including environmental analysis (air, water, soil/sediments), food analysis (volatile/nonvolatile compounds), and bioanalysis (plants, animal tissues, body fluids). The advantages and future challenges of the SPME technique are also discussed. Including recent research advances and further developments of SPME, the book offers a practical reference guide and a valuable resource for researchers and users of SPME techniques. The target audience includes analytical chemists, environmental scientists, biological scientists, material scientists, and analysts, as well as students at universities/institutes in related fields. Dr. Gangfeng Ouyang is a Professor at the School of Chemistry and Chemical Engineering, Sun Yat-sen University, China. Dr. Ruifen Jiang is an Associate Professor at the School of Environment, Jinan University, China.

Trends in Microextraction Techniques for Sample Preparation

Author :
Publisher : Mdpi AG
ISBN 13 : 9783038427056
Total Pages : 246 pages
Book Rating : 4.4/5 (27 download)

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Book Synopsis Trends in Microextraction Techniques for Sample Preparation by :

Download or read book Trends in Microextraction Techniques for Sample Preparation written by and published by Mdpi AG. This book was released on 2018-01-17 with total page 246 pages. Available in PDF, EPUB and Kindle. Book excerpt: Micro-extraction techniques in sample preparation are gaining interest among analytical chemists as they comply with green analytical chemistry demands and ensure environmental protection and public safety. Savings in cost and time are considered as valuable benefits by using novel micro-extraction approaches in sample handling. Selectivity, sensitivity and lower detection limits are also included among the performance characteristics required to meet the legislation criteria. The target of this special issue is to present the state of art in microextraction sample preparation techniques. Modern, simple and efficient methods for preconcentration and separation are described for different analytes isolated from various matrices.

Handbook of Solid Phase Microextraction

Author : Janusz Pawliszyn
Publisher : Elsevier
ISBN 13 : 0123914493
Total Pages : 497 pages
Book Rating : 4.1/5 (239 download)

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Book Synopsis Handbook of Solid Phase Microextraction by : Janusz Pawliszyn

Download or read book Handbook of Solid Phase Microextraction written by Janusz Pawliszyn and published by Elsevier. This book was released on 2011-12-01 with total page 497 pages. Available in PDF, EPUB and Kindle. Book excerpt: The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. - Practical application of Solid Phase Microextraction methods including detailed steps - Provides history of extraction methods to better understand the process - Suitable for all levels, from beginning student to experienced practitioner

Trends in Microextraction Techniques for Sample Preparation

Author :
Publisher :
ISBN 13 : 9783038427063
Total Pages : 0 pages
Book Rating : 4.4/5 (27 download)

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Book Synopsis Trends in Microextraction Techniques for Sample Preparation by :

Download or read book Trends in Microextraction Techniques for Sample Preparation written by and published by . This book was released on with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Annotation Micro-extraction techniques in sample preparation are gaining interest among analytical chemists as they comply with green analytical chemistry demands and ensure environmental protection and public safety. Savings in cost and time are considered as valuable benefits by using novel micro-extraction approaches in sample handling. Selectivity, sensitivity and lower detection limits are also included among the performance characteristics required to meet the legislation criteria. The target of this special issue is to present the state of art in microextraction sample preparation techniques. Modern, simple and efficient methods for preconcentration and separation are described for different analytes isolated from various matrices.

Green Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis

Author : Rajeev Jain
Publisher : Elsevier
ISBN 13 : 9780443139079
Total Pages : 0 pages
Book Rating : 4.1/5 (39 download)

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Book Synopsis Green Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis by : Rajeev Jain

Download or read book Green Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis written by Rajeev Jain and published by Elsevier. This book was released on 2024-10-01 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Green Analytical Methods and Miniaturized Sample Preparation techniques for Forensic Drug Analysis provides a comprehensive overview of GAMs in forensic drug analysis, including green sample preparation techniques, in-situ analytical platforms (such as DIC and µPADs), and on-site sample preparation. The book discusses not only eco-friendly GAM’s, but also methods which provide high sample throughput and cost-effective analysis, and are therefore of immense use in resource limited laboratories of developing countries. This is a comprehensive source of literature for analytical scientists in this developing area of sustainable and affordable analytical methods.

Solid Phase Microextraction

Author : Sue Ann Wercinski
Publisher : CRC Press
ISBN 13 : 9781439832387
Total Pages : 274 pages
Book Rating : 4.8/5 (323 download)

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Book Synopsis Solid Phase Microextraction by : Sue Ann Wercinski

Download or read book Solid Phase Microextraction written by Sue Ann Wercinski and published by CRC Press. This book was released on 1999-07-09 with total page 274 pages. Available in PDF, EPUB and Kindle. Book excerpt: An explanation of proven methods of chemical analysis, focusing on the myriad applications of solid phase microextraction (SPME) to laboratories performing high-sample throughput, quick sample turnaround time, low detection levels, and dirty sample matrices. It supplies commentary on developments in SPME technology from its inventor, Janusz Pawliszyn.

Bioanalysis of Pharmaceuticals

Author : Steen Honoré Hansen
Publisher : John Wiley & Sons
ISBN 13 : 1118716825
Total Pages : 332 pages
Book Rating : 4.1/5 (187 download)

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Book Synopsis Bioanalysis of Pharmaceuticals by : Steen Honoré Hansen

Download or read book Bioanalysis of Pharmaceuticals written by Steen Honoré Hansen and published by John Wiley & Sons. This book was released on 2015-07-20 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bioanalysis of Pharmaceuticals: Sample Preparation, Separation Techniques and Mass Spectrometry is the first student textbook on the separation science and mass spectrometry of pharmaceuticals present in biological fluids with an educational presentation of the principles, concepts and applications. It discusses the chemical structures and properties of low- and high-molecular drug substances; the different types of biological samples and fluids that are used; how to prepare the samples by extraction, and how to perform the appropriate analytical measurements by chromatographic and mass spectrometric methods. Bioanalysis of Pharmaceuticals: Sample Preparation, Separation Techniques and Mass Spectrometry: Is an introductory student textbook discussing the different principles and concepts clearly and comprehensively, with many relevant and educational examples Focuses on substances that are administered as human drugs, including low-molecular drug substances, peptides, and proteins Presents both the basic principles that are regularly taught in universities, along with the practical use of bioanalysis as carried out by researchers in the pharmaceutical industry and in hospital laboratories Is aimed at undergraduate students, scientists, technicians and researchers in industry working in the areas of pharmaceutical analyses, biopharmaceutical analyses, biological and life sciences The book includes multiple examples to illustrate the theory and application, with many practical aspects including calculations, thus helping the student to learn how to convert the data recorded by instruments into the real concentration of the drug substances within the biological sample.

Applications of LC-MS in Toxicology

Author : Aldo Polettini
Publisher : Pharmaceutical Press
ISBN 13 : 9780853696292
Total Pages : 310 pages
Book Rating : 4.6/5 (962 download)

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Book Synopsis Applications of LC-MS in Toxicology by : Aldo Polettini

Download or read book Applications of LC-MS in Toxicology written by Aldo Polettini and published by Pharmaceutical Press. This book was released on 2006 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical toxicologists are involved in the analysis of drugs and poisons in biological samples in different environments. Many scientists in the field of analytical toxicology have adopted LC-MS in their daily work, and this is illustrated by the increasing numbers of research papers published and presented at relevant conferences.

Information Resources in Toxicology, Volume 1: Background, Resources, and Tools

Author : Steve Gilbert
Publisher : Academic Press
ISBN 13 : 0128137258
Total Pages : 1055 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Information Resources in Toxicology, Volume 1: Background, Resources, and Tools by : Steve Gilbert

Download or read book Information Resources in Toxicology, Volume 1: Background, Resources, and Tools written by Steve Gilbert and published by Academic Press. This book was released on 2020-05-16 with total page 1055 pages. Available in PDF, EPUB and Kindle. Book excerpt: This new fifth edition of Information Resources in Toxicology offers a consolidated entry portal for the study, research, and practice of toxicology. Both volumes represents a unique, wide-ranging, curated, international, annotated bibliography, and directory of major resources in toxicology and allied fields such as environmental and occupational health, chemical safety, and risk assessment. The editors and authors are among the leaders of the profession sharing their cumulative wisdom in toxicology’s subdisciplines. This edition keeps pace with the digital world in directing and linking readers to relevant websites and other online tools. Due to the increasing size of the hardcopy publication, the current edition has been divided into two volumes to make it easier to handle and consult. Volume 1: Background, Resources, and Tools, arranged in 5 parts, begins with chapters on the science of toxicology, its history, and informatics framework in Part 1. Part 2 continues with chapters organized by more specific subject such as cancer, clinical toxicology, genetic toxicology, etc. The categorization of chapters by resource format, for example, journals and newsletters, technical reports, organizations constitutes Part 3. Part 4 further considers toxicology’s presence via the Internet, databases, and software tools. Among the miscellaneous topics in the concluding Part 5 are laws and regulations, professional education, grants and funding, and patents. Volume 2: The Global Arena offers contributed chapters focusing on the toxicology contributions of over 40 countries, followed by a glossary of toxicological terms and an appendix of popular quotations related to the field. The book, offered in both print and electronic formats, is carefully structured, indexed, and cross-referenced to enable users to easily find answers to their questions or serendipitously locate useful knowledge they were not originally aware they needed. Among the many timely topics receiving increased emphasis are disaster preparedness, nanotechnology, -omics, risk assessment, societal implications such as ethics and the precautionary principle, climate change, and children’s environmental health. Introductory chapters provide a backdrop to the science of toxicology, its history, the origin and status of toxicoinformatics, and starting points for identifying resources Offers an extensive array of chapters organized by subject, each highlighting resources such as journals, databases,organizations, and review articles Includes chapters with an emphasis on format such as government reports, general interest publications, blogs, and audiovisuals Explores recent internet trends, web-based databases, and software tools in a section on the online environment Concludes with a miscellany of special topics such as laws and regulations, chemical hazard communication resources, careers and professional education, K-12 resources, funding, poison control centers, and patents Paired with Volume Two, which focuses on global resources, this set offers the most comprehensive compendium of print, digital, and organizational resources in the toxicological sciences with over 120 chapters contributions by experts and leaders in the field

Encyclopedia of Analytical Science

Author :
Publisher : Elsevier
ISBN 13 : 008101984X
Total Pages : 5142 pages
Book Rating : 4.0/5 (81 download)

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Book Synopsis Encyclopedia of Analytical Science by :

Download or read book Encyclopedia of Analytical Science written by and published by Elsevier. This book was released on 2019-04-02 with total page 5142 pages. Available in PDF, EPUB and Kindle. Book excerpt: The third edition of the Encyclopedia of Analytical Science, Ten Volume Set is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science, Ten Volume Set provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher

Liquid-Phase Extraction

Author : Colin F. Poole
Publisher : Elsevier
ISBN 13 : 0128169125
Total Pages : 818 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Liquid-Phase Extraction by : Colin F. Poole

Download or read book Liquid-Phase Extraction written by Colin F. Poole and published by Elsevier. This book was released on 2019-08-29 with total page 818 pages. Available in PDF, EPUB and Kindle. Book excerpt: Liquid Phase Extraction thoroughly presents both existing and new techniques in liquid phase extraction. It not only provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample, but also showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including countercurrent chromatography, pressurized-liquid extraction, single-drop Microextraction, and more. Written by recognized experts in their respective fields, it serves as a one-stop reference for those who need to know which technique to choose for liquid phase extraction. Used in conjunction with a similar release, Solid Phase Extraction, it allows users to master this crucial aspect of sample preparation. - Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice - Includes extensive referencing that facilitates the identification of key information - Aimed at both entry-level scientists and those who want to explore new techniques and methods