Fast Scanning Calorimetry

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Fast Scanning Calorimetry

Author : Christoph Schick
Publisher : Springer
ISBN 13 : 3319313290
Total Pages : 796 pages
Book Rating : 4.3/5 (193 download)

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Book Synopsis Fast Scanning Calorimetry by : Christoph Schick

Download or read book Fast Scanning Calorimetry written by Christoph Schick and published by Springer. This book was released on 2016-06-28 with total page 796 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the past decades, the scan rate range of calorimeters has been extended tremendously at the high end, from approximately 10 up to 10 000 000 °C/s and more. The combination of various calorimeters and the newly-developed Fast Scanning Calorimeters (FSC) now span 11 orders of magnitude, by which many processes can be mimicked according to the time scale(s) of chemical and physical transitions occurring during cooling, heating and isothermal stays in case heat is exchanged. This not only opens new areas of research on polymers, metals, pharmaceuticals and all kinds of substances with respect to glass transition, crystallization and melting phenomena, it also enables in-depth study of metastability and reorganization of samples on an 1 to 1000 ng scale. In addition, FSC will become a crucial tool for understanding and optimization of processing methods at high speeds like injection molding. The book resembles the state-of-the art in Thermal Analysis & Calorimetry and is an excellent starting point for both experts and newcomers in the field.

Handbook of Thermal Analysis and Calorimetry

Author :
Publisher : Elsevier
ISBN 13 : 0444640630
Total Pages : 862 pages
Book Rating : 4.4/5 (446 download)

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Book Synopsis Handbook of Thermal Analysis and Calorimetry by :

Download or read book Handbook of Thermal Analysis and Calorimetry written by and published by Elsevier. This book was released on 2018-03-12 with total page 862 pages. Available in PDF, EPUB and Kindle. Book excerpt: Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. - Features 19 all-new chapters to bring readers up to date on the current status of the field - Provides a broad overview of recent progress in the most popular techniques and applications - Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry - Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics - Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications

Differential Scanning Calorimetry

Author : G.W.H. Höhne
Publisher : Springer Science & Business Media
ISBN 13 : 366203302X
Total Pages : 233 pages
Book Rating : 4.6/5 (62 download)

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Book Synopsis Differential Scanning Calorimetry by : G.W.H. Höhne

Download or read book Differential Scanning Calorimetry written by G.W.H. Höhne and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 233 pages. Available in PDF, EPUB and Kindle. Book excerpt: Differential Scanning Calorimetry (DSC) is a well established measuring method which is used on a large scale in different areas of research, development, and quality inspection and testing. Over a large temperature range, thermal effects can be quickly identified and the relevant temperature and the characteristic caloric values determined using substance quantities in the mg range. Measurement values obtained by DSC allow heat capacity, heat of transition, kinetic data, purity and glass transition to be determined. DSC curves serve to identify substances, to set up phase diagrams and to determine degrees of crystallinity. This book provides, for the first time, an overall description of the most impor tant applications of Differential Scanning Calorimetry. Prerequisites for reliable measurement results, optimum evaluation of the measurement curves and esti mation of the uncertainties of measurement are, however, the knowledge of the theoretical bases of DSC, a precise calibration of the calorimeter and the correct analysis of the measurement curve. The largest part of this book deals with these basic aspects: The theory of DSC is discussed for both heat flux and power compensated instruments; temperature calibration and caloric calibration are described on the basis of thermodynamic principles. Desmearing of the measurement curve in different ways is presented as a method for evaluating the curves of fast transitions.

Modulated Temperature Differential Scanning Calorimetry

Author : Mike Reading
Publisher : Springer Science & Business Media
ISBN 13 : 9781402037498
Total Pages : 352 pages
Book Rating : 4.0/5 (374 download)

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Book Synopsis Modulated Temperature Differential Scanning Calorimetry by : Mike Reading

Download or read book Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and published by Springer Science & Business Media. This book was released on 2006-02-22 with total page 352 pages. Available in PDF, EPUB and Kindle. Book excerpt: MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.

Principles and Applications of Thermal Analysis

Author : Paul Gabbott
Publisher : John Wiley & Sons
ISBN 13 : 0470698128
Total Pages : 480 pages
Book Rating : 4.4/5 (76 download)

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Book Synopsis Principles and Applications of Thermal Analysis by : Paul Gabbott

Download or read book Principles and Applications of Thermal Analysis written by Paul Gabbott and published by John Wiley & Sons. This book was released on 2008-04-30 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Handbook of Differential Scanning Calorimetry

Author : Joseph D Menczel
Publisher : Butterworth-Heinemann
ISBN 13 : 0128113480
Total Pages : 876 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Handbook of Differential Scanning Calorimetry by : Joseph D Menczel

Download or read book Handbook of Differential Scanning Calorimetry written by Joseph D Menczel and published by Butterworth-Heinemann. This book was released on 2023-02-22 with total page 876 pages. Available in PDF, EPUB and Kindle. Book excerpt: Differential scanning calorimetry (DSC) is the most important thermal analysis technique used today and the most common thermal analysis instrument found in chemical characterization laboratories. DSC has become an everyday tool in characterization laboratories, but many researchers using this technique have a limited understanding of the true breadth of its capabilities. Up to now, there has been no book that would describe the application of DSC in all the various areas of materials chemistry. The Handbook of Differential Scanning Calorimetry has been written to fill that void. This book is designed to summarize the knowledge of differential scanning calorimetry so that materials researchers and application chemists are given both a better understanding of techniques , as well as a review of the full scope of its capabilities. It also discusses how to properly interpret the DSC thermograms data obtained. Included in this work is the most up-to-date information written by some of the leaders in the field. It is written not only to help users get the most out of their equipment, After reading this book, people in all chemical and biological areas will have a broad overview of this measuring technique, and will be able to utilize this analytical technique more efficiently. - Provides a detail description of the theory behind differential scanning while simultaneously providing a wider breadth of understanding of the actual DSC technique - Includes a review of the basics of heat flux and power compensation DSC's, as well as separate chapters on inorganic and organic materials - Reviews the most common commercial DSC instruments on the market and their uses, including TA Instruments, Perkin-Elmer, Hitachi, Mettler Toledo, Netzsch, and Setaram

Thermal Analysis

Author : El-Zeiny Ebeid
Publisher : Elsevier
ISBN 13 : 0323901921
Total Pages : 324 pages
Book Rating : 4.3/5 (239 download)

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Book Synopsis Thermal Analysis by : El-Zeiny Ebeid

Download or read book Thermal Analysis written by El-Zeiny Ebeid and published by Elsevier. This book was released on 2021-06-23 with total page 324 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. - Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding - Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs - Contains chapters that cover the user of TA in materials science and crystal structures

Thermal Analysis of Polymers

Author : Joseph D. Menczel
Publisher : John Wiley & Sons
ISBN 13 : 1118995996
Total Pages : 607 pages
Book Rating : 4.1/5 (189 download)

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Book Synopsis Thermal Analysis of Polymers by : Joseph D. Menczel

Download or read book Thermal Analysis of Polymers written by Joseph D. Menczel and published by John Wiley & Sons. This book was released on 2014-07-09 with total page 607 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.

Solid State Development and Processing of Pharmaceutical Molecules

Author : Michael Gruss
Publisher : John Wiley & Sons
ISBN 13 : 352734635X
Total Pages : 578 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Solid State Development and Processing of Pharmaceutical Molecules by : Michael Gruss

Download or read book Solid State Development and Processing of Pharmaceutical Molecules written by Michael Gruss and published by John Wiley & Sons. This book was released on 2021-11-15 with total page 578 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid State Development and Processing of Pharmaceutical Molecules A guide to the lastest industry principles for optimizing the production of solid state active pharmaceutical ingredients Solid State Development and Processing of Pharmaceutical Molecules is an authoritative guide that covers the entire pharmaceutical value chain. The authors—noted experts on the topic—examine the importance of the solid state form of chemical and biological drugs and review the development, production, quality control, formulation, and stability of medicines. The book explores the most recent trends in the digitization and automation of the pharmaceutical production processes that reflect the need for consistent high quality. It also includes information on relevant regulatory and intellectual property considerations. This resource is aimed at professionals in the pharmaceutical industry and offers an in-depth examination of the commercially relevant issues facing developers, producers and distributors of drug substances. This important book: Provides a guide for the effective development of solid drug forms Compares different characterization methods for solid state APIs Offers a resource for understanding efficient production methods for solid state forms of chemical and biological drugs Includes information on automation, process control, and machine learning as an integral part of the development and production workflows Covers in detail the regulatory and quality control aspects of drug development Written for medicinal chemists, pharmaceutical industry professionals, pharma engineers, solid state chemists, chemical engineers, Solid State Development and Processing of Pharmaceutical Molecules reviews information on the solid state of active pharmaceutical ingredients for their efficient development and production.

Thermal Analysis in Practice

Author : Matthias Wagner
Publisher :
ISBN 13 : 9781569906439
Total Pages : 352 pages
Book Rating : 4.9/5 (64 download)

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Book Synopsis Thermal Analysis in Practice by : Matthias Wagner

Download or read book Thermal Analysis in Practice written by Matthias Wagner and published by . This book was released on 2017-12 with total page 352 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.

TMS 2019 148th Annual Meeting & Exhibition Supplemental Proceedings

Author : & The Minerals, Metals Materials Society
Publisher : Springer
ISBN 13 : 3030058611
Total Pages : 1631 pages
Book Rating : 4.0/5 (3 download)

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Book Synopsis TMS 2019 148th Annual Meeting & Exhibition Supplemental Proceedings by : & The Minerals, Metals Materials Society

Download or read book TMS 2019 148th Annual Meeting & Exhibition Supplemental Proceedings written by & The Minerals, Metals Materials Society and published by Springer. This book was released on 2019-02-26 with total page 1631 pages. Available in PDF, EPUB and Kindle. Book excerpt: This collection features papers presented at the 148th Annual Meeting & Exhibition of The Minerals, Metals & Materials Society.

Calorimetry in Food Processing

Author : Gönül Kaletunç
Publisher : John Wiley & Sons
ISBN 13 : 0813814839
Total Pages : 412 pages
Book Rating : 4.8/5 (138 download)

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Book Synopsis Calorimetry in Food Processing by : Gönül Kaletunç

Download or read book Calorimetry in Food Processing written by Gönül Kaletunç and published by John Wiley & Sons. This book was released on 2009-10-27 with total page 412 pages. Available in PDF, EPUB and Kindle. Book excerpt: Calorimetry in Food Processing: Analysis and Design of Food Systems introduces the basic principles of calorimetry and highlights various applications of calorimetry to characterize temperature-induced changes including starch gelatinization and crystallization, lipid transitions, protein denaturation, and inactivation of microorganisms in a variety of food and biological materials. Emphasis is given to the use of calorimetry as a tool for evaluation of processing requirements in order to assess the efficacy of food processing and for characterization of the effects of changes in formulation and processing conditions.

Thermal Methods of Analysis

Author : P.J. Haines
Publisher : Springer Science & Business Media
ISBN 13 : 9401113246
Total Pages : 297 pages
Book Rating : 4.4/5 (11 download)

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Book Synopsis Thermal Methods of Analysis by : P.J. Haines

Download or read book Thermal Methods of Analysis written by P.J. Haines and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 297 pages. Available in PDF, EPUB and Kindle. Book excerpt: The wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu tors by colleagues and instrument manufacturers is most gratefully ack nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC).

Calorimetry and Thermal Analysis of Polymers

Author : Vincent B. F. Mathot
Publisher : Hanser Gardner Publications
ISBN 13 : 9781569901267
Total Pages : 369 pages
Book Rating : 4.9/5 (12 download)

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Book Synopsis Calorimetry and Thermal Analysis of Polymers by : Vincent B. F. Mathot

Download or read book Calorimetry and Thermal Analysis of Polymers written by Vincent B. F. Mathot and published by Hanser Gardner Publications. This book was released on 1994-01 with total page 369 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Glass Transition and Phase Transitions in Food and Biological Materials

Author : Jasim Ahmed
Publisher : John Wiley & Sons
ISBN 13 : 1118935721
Total Pages : 490 pages
Book Rating : 4.1/5 (189 download)

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Book Synopsis Glass Transition and Phase Transitions in Food and Biological Materials by : Jasim Ahmed

Download or read book Glass Transition and Phase Transitions in Food and Biological Materials written by Jasim Ahmed and published by John Wiley & Sons. This book was released on 2017-04-24 with total page 490 pages. Available in PDF, EPUB and Kindle. Book excerpt: Glass and State Transitions in Food and Biological Materials describes how glass transition has been applied to food micro-structure, food processing, product development, storage studies, packaging development and other areas. This book has been structured so that readers can initially grasp the basic principles and instrumentation, before moving through the various applications. In summary, the book will provide the “missing link” between food science and material science/polymer engineering. This will allow food scientists to better understand the concept and applications of thermal properties.

Applications of Calorimetry in a Wide Context

Author : Amal Ali Elkordy
Publisher : BoD – Books on Demand
ISBN 13 : 9535109472
Total Pages : 488 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Applications of Calorimetry in a Wide Context by : Amal Ali Elkordy

Download or read book Applications of Calorimetry in a Wide Context written by Amal Ali Elkordy and published by BoD – Books on Demand. This book was released on 2013-01-23 with total page 488 pages. Available in PDF, EPUB and Kindle. Book excerpt: Calorimetry, as a technique for thermal analysis, has a wide range of applications which are not only limited to studying the thermal characterisation (e.g. melting temperature, denaturation temperature and enthalpy change) of small and large drug molecules, but are also extended to characterisation of fuel, metals and oils. Differential Scanning Calorimetry is used to study the thermal behaviours of drug molecules and excipients by measuring the differential heat flow needed to maintain the temperature difference between the sample and reference cells equal to zero upon heating at a controlled programmed rate. Microcalorimetry is used to study the thermal transition and folding of biological macromolecules in dilute solutions. Microcalorimetry is applied in formulation and stabilisation of therapeutic proteins. This book presents research from all over the world on the applications of calorimetry on both solid and liquid states of materials.

Thermal Analysis of Pharmaceuticals

Author : Duncan Q.M. Craig
Publisher : CRC Press
ISBN 13 : 1420014897
Total Pages : 416 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Thermal Analysis of Pharmaceuticals by : Duncan Q.M. Craig

Download or read book Thermal Analysis of Pharmaceuticals written by Duncan Q.M. Craig and published by CRC Press. This book was released on 2006-12-21 with total page 416 pages. Available in PDF, EPUB and Kindle. Book excerpt: As a result of the Process Analytical Technologies (PAT) initiative launched by the U.S. Food and Drug Administration (FDA), analytical development is receiving more attention within the pharmaceutical industry. Illustrating the importance of analytical methodologies, Thermal Analysis of Pharmaceuticals presents reliable and versatile charac