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Author : James G. Clothier (Jr.)
Publisher :
ISBN 13 :
Total Pages : 272 pages
Book Rating : 4.:/5 (345 download)
Download or read book Chiral Separations Using Bile Salts in Capillary Electrophoresis written by James G. Clothier (Jr.) and published by . This book was released on 1995 with total page 272 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Virginia R. DiGuglielmo
Publisher :
ISBN 13 :
Total Pages : 236 pages
Book Rating : 4.:/5 (564 download)
Download or read book Optimizing Bile Salt-mediated Chiral Separations in Capillary Electrophoresis written by Virginia R. DiGuglielmo and published by . This book was released on 2004 with total page 236 pages. Available in PDF, EPUB and Kindle. Book excerpt: Work described in this thesis pertains to the optimization of chiral separations of (R, S) 1,1'-Bi-2-napthol, (BN), and (R, S) 1,1'-Binaphthyl-2,2'-diylhydrogenphosphate, (BNDHP), using micellar electrokinetic capillary chromatography. Effectiveness of a number of chiral surfactants, particularly cholate, were investigated by systematic alteration of the chiral surfactant concentration, the buffering system, the ionic strength, the pH, the addition of MeOH and capillary preconditioning.
Author : Kevin D. Altria
Publisher : Springer Science & Business Media
ISBN 13 : 1592595391
Total Pages : 347 pages
Book Rating : 4.5/5 (925 download)
Download or read book Capillary Electrophoresis Guidebook written by Kevin D. Altria and published by Springer Science & Business Media. This book was released on 2008-02-02 with total page 347 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is intended to be a working guide to the operation of capillary electrophoresis (CE) instrumentation. Since CE is still a rap idly maturing technique, detailed validated protocols are not widely established. Therefore, extensive experimental procedures are not pro vided for individual analyses. The intention is to provide general guide lines on the principles and practice of CE and to give an overview of the specific technologies and important application areas. Part I provides operating instructions for standard commercially available instruments. Guidelines are included for activities such as changing capillaries, method development, quantitative procedures, optimization of precision and sensitivity, and the validation of meth ods, fraction collection, and troubleshooting, as well as a quick guide to running a separation. The application range of CE is possibly the most diverse of all analytical techniques and ranges from large, complex macromolecules, such as proteins and nucleic acids, to small solutes, such as organic drugs and inorganic anions and cations.
Author : Ann Van Eeckhaut
Publisher : CRC Press
ISBN 13 : 1420069349
Total Pages : 546 pages
Book Rating : 4.4/5 (2 download)
Download or read book Chiral Separations by Capillary Electrophoresis written by Ann Van Eeckhaut and published by CRC Press. This book was released on 2009-11-11 with total page 546 pages. Available in PDF, EPUB and Kindle. Book excerpt: Covers the Fundamentals of Chiral Separation, Available Chiral Selectors, and Numerous Applications of Chiral Separation by Capillary ElectrophoresisSince the 1980s, modern analytical tools have enabled capillary electrophoresis to become a standard part of the chemist's toolkit. With contributions from international experts, Chiral Separations by
Author : Benno Allard Ingelse
Publisher :
ISBN 13 : 9789038609584
Total Pages : 162 pages
Book Rating : 4.6/5 (95 download)
Download or read book Chiral Separations Using Capillary Electrophoresis written by Benno Allard Ingelse and published by . This book was released on 1997 with total page 162 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Peter Mikuš
Publisher : BoD – Books on Demand
ISBN 13 : 9535106570
Total Pages : 211 pages
Book Rating : 4.5/5 (351 download)
Download or read book Chiral Capillary Electrophoresis in Current Pharmaceutical and Biomedical Analysis written by Peter Mikuš and published by BoD – Books on Demand. This book was released on 2012-08-29 with total page 211 pages. Available in PDF, EPUB and Kindle. Book excerpt: The scientific monograph by the author Peter Mikus entitled "Chiral Capillary Electrophoresis in Current Pharmaceutical and Biomedical Analysis" provides a comprehensive view on the advanced capillary electrophoresis techniques aimed to current chiral bioanalysis. The advances in the chiral electrophoresis analytical approaches are divided and theoretically described in three sections involving (i) advanced chiral separations for the optimization of chiral resolution (separation mechanisms; electrophoresis techniques in capillary and microchip format; electrophoretic modes such as ITP, CZE/EKC, CEC; chiral additives / pseudophases / phases), (ii) advanced sample preparation for the on-line preconcentration, sample clean-up and analyte derivatization (implementation of electrophoretic effects such as stacking; non-electrophoretic effects such as SPE, chromatography, dialysis; combinations of these effects; multidimensional CE systems; instrumental schemes), (iii) advanced combinations of detection and electrophoresis for the optimization in qualitative and quantitative evaluation (the most important universal as well as selective detection approaches such as absorption and fluorescence spectrophotometry, electrochemical detection, mass spectrometry vs. (i) and/or (ii)). Real analytical potential (benefits and limitations) of these advanced analytical approaches is emphasized by selected performance parameters of the methods and illustrated by many current practical applications including chiral analyses of drugs, their (bio)degradation products and biomarkers in pharmaceutical and biological matrices. The author wishes the readers many inspirations in the creation of new innovative approaches in the field of advanced chiral electrophoresis techniques with the aim to overcome capabilities of the current analytical techniques.
Author : Reinhard H. H. Neubert
Publisher : CRC Press
ISBN 13 : 0203912136
Total Pages : 392 pages
Book Rating : 4.2/5 (39 download)
Download or read book Affinity Capillary Electrophoresis in Pharmaceutics and Biopharmaceutics written by Reinhard H. H. Neubert and published by CRC Press. This book was released on 2003-01-14 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt: This reference presents the most recent breakthroughs and techniques in affinity capillary electrophoresis (ACE) to measure and determine the physicochemical and thermodynamic parameters of drug compounds. The authors offer strategies to explore and characterize interactions between drugs, drug vehicles, and biological membranes to facilitate devel
Author : Lisa M. Daley
Publisher :
ISBN 13 :
Total Pages : 188 pages
Book Rating : 4.:/5 (356 download)
Download or read book Chiral Separations Using Bile Salt Solutions in High Performance Liquid Chromatography and Micellar Electrokinetic Capillary Chromatography written by Lisa M. Daley and published by . This book was released on 1996 with total page 188 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Kyle W. Eckenroad
Publisher :
ISBN 13 :
Total Pages : 244 pages
Book Rating : 4.:/5 (173 download)
Download or read book Examination of Bile Salt Mediated Chiral Separations Using Micellar Electrokinetic Capillary Chromatography and NMR written by Kyle W. Eckenroad and published by . This book was released on 2007 with total page 244 pages. Available in PDF, EPUB and Kindle. Book excerpt: Work described herein is aimed at understanding the structure and aggregation mechanisms of bile salt micelles as well as the interactions that allow bile salt micelles to perform chiral recognition. NMR spectra allow for the creation of models useful for understanding micellar structure(s) and the interactions that allow for chiral recognition.
Author : Gerald Gübitz
Publisher : Springer Science & Business Media
ISBN 13 : 1592596487
Total Pages : 427 pages
Book Rating : 4.5/5 (925 download)
Download or read book Chiral Separations written by Gerald Gübitz and published by Springer Science & Business Media. This book was released on 2008-02-02 with total page 427 pages. Available in PDF, EPUB and Kindle. Book excerpt: Prominent experts from around the world detail the chromatographic and electroseparation techniques they have developed for chiral separations on an analytical scale. Described in step-by-step detail to ensure successful experimental results, the procedures are presented as either general methods or as specific applications to substance classes and special compounds, with emphasis on high performance liquid chromatography and capillary electrophoresis techniques, but also including thin layer chromotographic, gas chromatographic, supercritical fluid chromatographic as well as recent electrochromotographic techniques.
Author : Bezhan Chankvetadze
Publisher : John Wiley & Sons
ISBN 13 : 9780471974154
Total Pages : 586 pages
Book Rating : 4.9/5 (741 download)
Download or read book Capillary Electrophoresis in Chiral Analysis written by Bezhan Chankvetadze and published by John Wiley & Sons. This book was released on 1997-12-29 with total page 586 pages. Available in PDF, EPUB and Kindle. Book excerpt: Das weltweite Interesse an der Trennung von Enantiomeren, Spiegelbildern ein und derselben chemischen Verbindung, nimmt zu, da diese Formen beispielsweise verschiedene physiologische Wirkungen hervorrufen können. Eine hochaktuelle Technik der Stofftrennung in diesem Zusammenhang ist die Kapillarelektrophorese, die hier von den theoretischen Grundlagen bis hin zu analytischen Details und Anbieterlisten ausführlich beschrieben wird.
Author : Imran Ali
Publisher : John Wiley & Sons
ISBN 13 : 0470867817
Total Pages : 368 pages
Book Rating : 4.4/5 (78 download)
Download or read book Chiral Pollutants written by Imran Ali and published by John Wiley & Sons. This book was released on 2005-07-15 with total page 368 pages. Available in PDF, EPUB and Kindle. Book excerpt: Today, among the various chiral discrimination methods, chromatography and capillary electrophoresis techniques have become powerful tools in environmental analysis. Therefore, there is a need to describe the art of the determination of the chiral pollutants in the environmental matrices. This book provides the complete information on the types of the chiral pollutants, their toxicities and methods of determination by chromatography and capillary electrophoresis.
Author : Salvatore Fanali
Publisher :
ISBN 13 :
Total Pages : 220 pages
Book Rating : 4.:/5 (14 download)
Download or read book Paper Symposium Capillary Electrophoresis Chiral Separations written by Salvatore Fanali and published by . This book was released on 1999 with total page 220 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Chiral Separation Using Capillary Electrophoresis (CE) and Continuous Free Flow Electrophoresis (CFFE) written by and published by . This book was released on 2003 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: In this report, chiral separations of hydrobenzoin (HB), piperoxan (PI) and methoxyphenamine (MPA) using capillary electrophoresis (CE) are discussed. In the experimental part, separation conditions such as buffer pH, buffer concentration, CE instrumental polarity, capillary length, capillary temperature and sample matrix, etc., were considered and their impact on the chiral separations compared. All selected analytes - hydrobenzoin, piperoxan and methoxyphenamine could be well separated by CE using sulfated?-cyclodextrin (SCD) as chiral additive (CA). Preparative scale separation of MPA and PI was carried out by a continuous free flow electrophoresis (CFFE) instrument using SCD with two different degrees of substitution as CA. Rapid chiral CE methods were developed for the fractionated CFFE samples. Buffer concentration, SCD concentration, applied voltage, sample feeding rate and position, and electrode washing conditions were investigated. Experiments with dyes as surrogates were also completed on the CFFE and UV-Vis instruments. The CFFE instrument PI sample capacity was investigated using optimized conditions.
Author : Salvatore Fanali
Publisher :
ISBN 13 :
Total Pages : 116 pages
Book Rating : 4.:/5 (263 download)
Download or read book Chiral Separations by Capillary Electrophoresis written by Salvatore Fanali and published by . This book was released on 1994 with total page 116 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Salvatore Fanali
Publisher :
ISBN 13 :
Total Pages : 116 pages
Book Rating : 4.:/5 (722 download)
Download or read book Paper symposium Chiral separations by capillary electrophoresis written by Salvatore Fanali and published by . This book was released on 1994 with total page 116 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author :
Publisher :
ISBN 13 :
Total Pages : 223 pages
Book Rating : 4.:/5 (437 download)
Download or read book Capillary Electrophoresis Chiral Separations written by and published by . This book was released on 1999 with total page 223 pages. Available in PDF, EPUB and Kindle. Book excerpt:
