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Author : George C. Levy
Publisher :
ISBN 13 :
Total Pages : 370 pages
Book Rating : 4.0/5 ( download)
Download or read book Carbon-13 Nuclear Magnetic Resonance Spectroscopy written by George C. Levy and published by . This book was released on 1992 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : George C. Levy
Publisher :
ISBN 13 :
Total Pages : 248 pages
Book Rating : 4.:/5 (318 download)
Download or read book Carbon-13 Nuclear Magnetic Resonance for Organic Chemists written by George C. Levy and published by . This book was released on 1972 with total page 248 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Nicolau Beckmann
Publisher : Elsevier
ISBN 13 : 0080528554
Total Pages : 334 pages
Book Rating : 4.0/5 (85 download)
Download or read book Carbon-13 NMR Spectroscopy of Biological Systems written by Nicolau Beckmann and published by Elsevier. This book was released on 1995-04-06 with total page 334 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is intended to provide an in-depth understanding of 13C NMR as a tool in biological research. 13C NMR has provided unique information concerning complex biological systems, from proteins and nucleic acids to animals and humans. The subjects addressed include multidimensional heteronuclear techniques for structural studies of molecules in the liquid and solid states, the investigation of interactions in model membranes, the elucidation of metabolic pathwaysin vitro and in vivo on animals, and noninvasive metabolic studies performed on humans. The book is a unique mix of NMR methods and biological applications which makes it a convenient reference for those interested in research in this interdisciplinary area of physics, chemistry, biology, and medicine. An interdisciplinary text with emphasis on both 13C NMR methodology and the relevant biological and biomedical issues State-of-the-art 13C NMR techniques are described; Whenever possible, their advantages over other approaches are emphasized The chapters constitute comprehensive reviews and are written by acknowledged experts in their fields Chapters are written in a clear style, and include a large number of illustrations and comprehensive references
Author : Metin Balci
Publisher : Elsevier
ISBN 13 : 9780080525532
Total Pages : 430 pages
Book Rating : 4.5/5 (255 download)
Download or read book Basic 1H- and 13C-NMR Spectroscopy written by Metin Balci and published by Elsevier. This book was released on 2005-01-19 with total page 430 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful and theoretically complex analytical tool. Basic 1H- and 13C-NMR Spectroscopy provides an introduction to the principles and applications of NMR spectroscopy. Whilst looking at the problems students encounter when using NMR spectroscopy, the author avoids the complicated mathematics that are applied within the field. Providing a rational description of the NMR phenomenon, this book is easy to read and is suitable for the undergraduate and graduate student in chemistry. Describes the fundamental principles of the pulse NMR experiment and 2D NMR spectra Easy to read and written with the undergraduate and graduate chemistry student in mind Provides a rational description of NMR spectroscopy without complicated mathematics
Author : Eberhard Breitmaier
Publisher : Wiley-VCH
ISBN 13 :
Total Pages : 550 pages
Book Rating : 4.:/5 (318 download)
Download or read book Carbon-13 NMR Spectroscopy written by Eberhard Breitmaier and published by Wiley-VCH. This book was released on 1987 with total page 550 pages. Available in PDF, EPUB and Kindle. Book excerpt: E. Breitmaier, W. Voelter Carbon-13 NMR Spectroscopy High-Resolution Methods and Applications in Organic Chemistry and Biochemistry Third, completely revised edition New techniques and increased use of computers have led to rapid development in 13C NMR spectroscopy with enhanced instrumental sensitivity and improved quality of the spectra. This necessitated a complete revision when the third edition of this successful monograph was prepared. The new methods described include those for multiplicity analysis and two-dimensional homo- or hetero-nuclear shift correlations. As in the second edition, the authors survey the large number of 13C NMR applications to organic molecules and natural products in a representative and systematic rather than an exhaustive way. New sections about coupling constants, organophosphorus and organometallic compounds as well as synthetic polymers have been added. The scope remains limited to high-resolution methods and molecular systems.
Author : P.K. Agrawal
Publisher : Elsevier
ISBN 13 : 1483290743
Total Pages : 581 pages
Book Rating : 4.4/5 (832 download)
Download or read book Carbon-13 NMR of Flavonoids written by P.K. Agrawal and published by Elsevier. This book was released on 2013-10-22 with total page 581 pages. Available in PDF, EPUB and Kindle. Book excerpt: This detailed treatise is written for chemists who are not NMR spectroscopists but who wish to use carbon-13 NMR spectroscopy. It shows why measurement of carbon-13 NMR is needed and explains how the method can - or should - be used for rapid characterization of flavonoids, one of the most diverse and widespread groups of natural constituents. The first part of the book presents background information and discussion of the essential aspects of flavonoids and carbon-13 NMR spectroscopy and demonstrates its significant role in the revision of several earlier established chemical structures. It discusses various one- and two-dimensional NMR spectroscopic techniques and other relevant experimental methodologies for the interpretation of spectral details which enable individual resonance lines to be associated with the appropriate carbons in a molecule. The second part provides a comprehensive coverage of the carbon-13 chemical shifts of various classes and subclasses of flavonoids. It also illustrates how to utilize carbon-13 data to gain information for the determination of the nature, number and site of any substituent in flavonoids. Vital information for the differential and complete structure elucidation of the various classes of flavonoids by carbon-13 NMR shielding data is described in-depth in the third part of the book. The book will be welcomed by all those working in natural product chemistry who will appreciate the non-mathematical approach and the fact that such a wealth of theoretical and practical information has been assembled in a single volume.
Author : Norbert W. Lutz
Publisher : Cambridge University Press
ISBN 13 : 0521765900
Total Pages : 641 pages
Book Rating : 4.5/5 (217 download)
Download or read book Methodologies for Metabolomics written by Norbert W. Lutz and published by Cambridge University Press. This book was released on 2013-01-21 with total page 641 pages. Available in PDF, EPUB and Kindle. Book excerpt: Metabolomics, the global characterisation of the small molecule complement involved in metabolism, has evolved into a powerful suite of approaches for understanding the global physiological and pathological processes occurring in biological organisms. The diversity of metabolites, the wide range of metabolic pathways and their divergent biological contexts require a range of methodological strategies and techniques. Methodologies for Metabolomics provides a comprehensive description of the newest methodological approaches in metabolomic research. The most important technologies used to identify and quantify metabolites, including nuclear magnetic resonance and mass spectrometry, are highlighted. The integration of these techniques with classical biological methods is also addressed. Furthermore, the book presents statistical and chemometric methods for evaluation of the resultant data. The broad spectrum of topics includes a vast variety of organisms, samples and diseases, ranging from in vivo metabolomics in humans and animals to in vitro analysis of tissue samples, cultured cells and biofluids.
Author : Eberhard Breitmaier
Publisher : Wiley-VCH
ISBN 13 :
Total Pages : 540 pages
Book Rating : 4.3/5 (121 download)
Download or read book Carbon-13 NMR Spectroscopy written by Eberhard Breitmaier and published by Wiley-VCH. This book was released on 1987 with total page 540 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : Peder Larson
Publisher : Academic Press
ISBN 13 : 0128222700
Total Pages : 298 pages
Book Rating : 4.1/5 (282 download)
Download or read book Hyperpolarized Carbon-13 Magnetic Resonance Imaging and Spectroscopy written by Peder Larson and published by Academic Press. This book was released on 2021-11-28 with total page 298 pages. Available in PDF, EPUB and Kindle. Book excerpt: MRI with hyperpolarized carbon-13 agents is a powerful emerging imaging modality that can measure real-time metabolism in cells, animals, and humans. It uses endogenous, non-toxic contrast agents that a hyperpolarized, resulting in up to 100,000-fold increases in sensitivity. This technique uses no ionizing radiation, and is being applied in a range of human trials. It’s primary use is for metabolic imaging, but it can also measure perfusion, pH, and necrosis. Hyperpolarized Carbon-13 Magnetic Resonance Imaging and Spectroscopy is designed to be a one stop shop for understanding hyperpolarized 13C MRI. This book explains the principles of this imaging modality, the requirements for performing studies, shows how to interpret the results, and gives an overview of current biomedical applications. It is suitable for engineers, scientists and clinicians in radiology and biomedical imaging who want to understand this technology. Presents the physics and hardware of dissolution dynamic nuclear polarization Explains the behaviour of hyperpolarized carbon-13 agents and how to image them Detailed guidance on experimental design and data interpretation Identifies promising and potential applications of hyperpolarized carbon-13 MR
Author : Robert B. Bates
Publisher : Springer Science & Business Media
ISBN 13 : 1461259959
Total Pages : 280 pages
Book Rating : 4.4/5 (612 download)
Download or read book Carbon-13 NMR Spectral Problems written by Robert B. Bates and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 280 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the advent of Fourier transform spectrometers of great sensitivity, it has become practical to obtain carbon-13 nuclear magnetic resonance (C-13 NMR; l3C NMR; CMR) spectra routinely on organic molecules, and this technique has become one of the highest utility in determining structures of organic unknowns. When the usual spectrometric techniques proton magnetic resonance (H-I NMR; IH NMR; PMR), infrared (lR), mass (MS), and ultraviolet (UV)-do not readily reveal a compound's structure, a C-13 NMR spectrum will often provide sufficient additional information to yield it unequivocally. With this in mind, the present work was designed to give advanced undergraduates, graduate students, and practicing chemists a working knowledge of and facility with the use of this valuable technique. Some familiarity with other spectrometric techniques is assumed (recommended book: Silverstein, Bassler, and Morrill, Spectrometric Identification of Organic Compounds), but no prior knowledge of C-13 NMR -which is treated very lightly, if at all, in the widely used elementary organic texts-is necessary. A discussion of C-13 NMR spectroscopy is followed by 125 problems, each consisting of a molecular formula, two types of C-13 NMR spectra (partially and completely proton decoupled, with connecting lines to facilitate multiplicity assignments), an integrated H-I NMR spectrum, and the most important IR, UV, and MS data. These problems have been very carefully prepared, thoroughly tested by students at the University of Arizona, and we believe that very few errors remain.
Author : F. W. Wehrli
Publisher :
ISBN 13 :
Total Pages : 504 pages
Book Rating : 4.:/5 (318 download)
Download or read book Interpretation of Carbon-13 NMR Spectra written by F. W. Wehrli and published by . This book was released on 1988-06-23 with total page 504 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the second edition of a very successful book which provides the conceptual and experimental basis for the interpretation of 13 C NMR spectra.
Author : Kalevi Pihlaja
Publisher : VCH Publishers
ISBN 13 :
Total Pages : 408 pages
Book Rating : 4.3/5 (91 download)
Download or read book Carbon-13 NMR Chemical Shifts in Structural and Stereochemical Analysis written by Kalevi Pihlaja and published by VCH Publishers. This book was released on 1994 with total page 408 pages. Available in PDF, EPUB and Kindle. Book excerpt: A review of recent research on strategies and applications of the C-13 chemical shift, a method for determining configuration of organic compounds. Introduces C-13 NMR spectroscopy, and describes conditions for collecting the FID, for data handling, and for obtaining a well- resolved C-13 NMR spectrum, as well as various substituent effect correlations, their derivations, and the origin of the effects. Also discusses the use of multidimensional NMR methods. For organic, physical, and natural products chemists. Includes bandw diagrams. Annotation copyright by Book News, Inc., Portland, OR
Author : Eberhard Breitmaier
Publisher : CRC Press
ISBN 13 : 9783718604739
Total Pages : 378 pages
Book Rating : 4.6/5 (47 download)
Download or read book 13C NMR Spectroscopy written by Eberhard Breitmaier and published by CRC Press. This book was released on 1984 with total page 378 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : J. A. Whitesell
Publisher : Springer Science & Business Media
ISBN 13 : 9400931611
Total Pages : 231 pages
Book Rating : 4.4/5 (9 download)
Download or read book Stereochemical Analysis of Alicyclic Compounds by C-13 NMR Spectroscopy written by J. A. Whitesell and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 231 pages. Available in PDF, EPUB and Kindle. Book excerpt: Through numerous conversations with other synthetic chemists it became apparent that the great power of carbon nuclear magnetic resonance was being significantly underutilized. In our own work we have found that 13C spectroscopy is a more powerful tool than IH NMR spectroscopy, especially for probing subtle stereochemical questions in complicated systems. This is especially true in five membered ring compounds where IH NMR is at a particular disadvantage. The two techniques can be used independently to solve the same question-that of stereochemistry - but they do so in different ways. Advantage can be taken in IH NMR of a relatively consistent relationship between stereochemical orientation and coupling constants between vicinal protons, while in 13C NMR it is the correlation between spatial relationships of non-hydrogen, y substituents and their effect on chemical shift that can be used to assign stereochemistry. It was also clear that the use of 13C NMR required a different approach to problem solving than that typically used with IH NMR. While the latter technique could be employed with a very general approach (e.g., the Karplus equation), 13C NMR would, at least for the immediate future, require a relatively extensive set of model systems from which the consequences of stereochemical changes could be derived for any given carbon framework.
Author : William W. Paudler
Publisher :
ISBN 13 :
Total Pages : 280 pages
Book Rating : 4.4/5 (91 download)
Download or read book Nuclear Magnetic Resonance written by William W. Paudler and published by . This book was released on 1971 with total page 280 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Author : T.I. Atta-Ur-Rahman
Publisher : Springer Science & Business Media
ISBN 13 : 1461248949
Total Pages : 366 pages
Book Rating : 4.4/5 (612 download)
Download or read book Nuclear Magnetic Resonance written by T.I. Atta-Ur-Rahman and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 366 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear magnetic resonance spectroscopy is presently going through an explosive phase of development. This has been brought about largely on account of the advent of Fourier transform NMR spectrometers linked to powerful microcomputers which have opened up a whole new world for structural chemists and biochemists. This is exemplified by a host of publications, especially on new pulse sequences, which continue to provide new exciting modifications for recording two-dimensional NMR. Moreover, NMR is no longer confined to structural chemists but has moved firmly into the area of medicine as a powerful nondestructive body scanning technique. With this background, I felt that there was need for a text which would provide a fairly comprehensive account of the important features of 1 H- and 13C-NMR spectroscopy in one book, as well as make available an up-to-date account of recent developments of new pulse sequences, with particular reference to 2D-NMR spectroscopy. Since this book is written for students of chemistry and biochemistry as well as for biology students who have chemistry as a subsidiary, it was decided to avoid a complex mathematical treatment and to present, as far as possible without oversimplification, a qualitative account of 1 H- and 13C-NMR spectroscopy as it is today. I hope that the book satisfactorily meets these objectives.
Author : Charlotte Stagg
Publisher : Academic Press
ISBN 13 : 0124016979
Total Pages : 398 pages
Book Rating : 4.1/5 (24 download)
Download or read book Magnetic Resonance Spectroscopy written by Charlotte Stagg and published by Academic Press. This book was released on 2013-11-11 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt: Magnetic Resonance Spectroscopy: Tools for Neuroscience Research and Emerging Clinical Applications is the first comprehensive book for non-physicists that addresses the emerging and exciting technique of magnetic resonance spectroscopy. Divided into three sections, this book provides coverage of the key areas of concern for researchers. The first, on how MRS is acquired, provides a comprehensive overview of the techniques, analysis, and pitfalls encountered in MRS; the second, on what can be seen by MRS, provides essential background physiology and biochemistry on the major metabolites studied; the final sections, on why MRS is used, constitutes a detailed guide to the major clinical and scientific uses of MRS, the current state of teh art, and recent innovations. Magnetic Resonance Spectroscopy will become the essential guide for people new to the technique and give those more familiar with MRS a new perspective. Chapters written by world-leading experts in the field Fully illustrated Covers both proton and non-proton MRS Includes the background to novel MRS imaging approaches
