Time Weighted Average Solid Phase Microextraction (TWA-SPME) for In-planta Detection of Chlorinated Solvents

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ISBN 13 :
Total Pages : 134 pages
Book Rating : 4.:/5 (436 download)

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Book Synopsis Time Weighted Average Solid Phase Microextraction (TWA-SPME) for In-planta Detection of Chlorinated Solvents by : Emily Moore Sheehan

Download or read book Time Weighted Average Solid Phase Microextraction (TWA-SPME) for In-planta Detection of Chlorinated Solvents written by Emily Moore Sheehan and published by . This book was released on 2009 with total page 134 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Recent interest in the use of phyto-mapping for plume delineation at contaminated sites has promoted a need for new and innovative sampling techniques. Solid-phase micro-extraction (SPME) methods have been developed as a chemical analysis tool offering fast, simple, non-invasive sampling without the use of solvents. In this study SPME devices were tested for applicability for in-planta detection of chlorinated solvents. To evaluate the use of SPME for VOCs in-planta a number of integrated studies were undertaken. Uptake profiles were developed for nine chlorinated solvents in a liquid polydimethylsiloxane (PDMS) matrix with 100 [mu]m Carboxene SPME fibers. Timeweighted average (TWA) sampling was conducted by exposing the SPME fiber to the chemical mixtures using three retraction lengths. Linear uptake profiles were demonstrated for 25 of the 27 of the sampling conditions. A storage experiment was conducted to determine sample retention on the SPME fiber for transport prior to analysis. It was demonstrated that all chemicals except dichloromethane are retained on the fiber for up to 24 hours. Field sampling with SPME devices was conducted at a known chlorinated solvent contaminated site using a newly designed in-planta sampler. Sampling with SPME fibers produced detections ranging from 5 to 234 times higher than tree core sampling"--Abstract, leaf iii.

Solid Phase Microextraction

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Publisher : CRC Press
ISBN 13 : 9781439832387
Total Pages : 274 pages
Book Rating : 4.8/5 (323 download)

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Book Synopsis Solid Phase Microextraction by : Sue Ann Wercinski

Download or read book Solid Phase Microextraction written by Sue Ann Wercinski and published by CRC Press. This book was released on 1999-07-09 with total page 274 pages. Available in PDF, EPUB and Kindle. Book excerpt: An explanation of proven methods of chemical analysis, focusing on the myriad applications of solid phase microextraction (SPME) to laboratories performing high-sample throughput, quick sample turnaround time, low detection levels, and dirty sample matrices. It supplies commentary on developments in SPME technology from its inventor, Janusz Pawliszyn.

Solid Phase Microextraction

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Publisher : Springer
ISBN 13 : 366253598X
Total Pages : 313 pages
Book Rating : 4.6/5 (625 download)

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Book Synopsis Solid Phase Microextraction by : Gangfeng Ouyang

Download or read book Solid Phase Microextraction written by Gangfeng Ouyang and published by Springer. This book was released on 2016-11-24 with total page 313 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book offers comprehensive information on the developments and applications of the solid phase microextraction (SPME) technique. The first part of the book briefly introduces readers to the fundamentals of SPME, while subsequent sections describe the applications of SPME technique in detail, including environmental analysis (air, water, soil/sediments), food analysis (volatile/nonvolatile compounds), and bioanalysis (plants, animal tissues, body fluids). The advantages and future challenges of the SPME technique are also discussed. Including recent research advances and further developments of SPME, the book offers a practical reference guide and a valuable resource for researchers and users of SPME techniques. The target audience includes analytical chemists, environmental scientists, biological scientists, material scientists, and analysts, as well as students at universities/institutes in related fields. Dr. Gangfeng Ouyang is a Professor at the School of Chemistry and Chemical Engineering, Sun Yat-sen University, China. Dr. Ruifen Jiang is an Associate Professor at the School of Environment, Jinan University, China.

Handbook of Solid Phase Microextraction

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Publisher : Elsevier
ISBN 13 : 0124160174
Total Pages : 497 pages
Book Rating : 4.1/5 (241 download)

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Book Synopsis Handbook of Solid Phase Microextraction by : Janusz Pawliszyn

Download or read book Handbook of Solid Phase Microextraction written by Janusz Pawliszyn and published by Elsevier. This book was released on 2011 with total page 497 pages. Available in PDF, EPUB and Kindle. Book excerpt: The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner.

Evolution of Solid Phase Microextraction Technology

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Publisher : Royal Society of Chemistry
ISBN 13 : 1839166800
Total Pages : 663 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Evolution of Solid Phase Microextraction Technology by : Janusz Pawliszyn

Download or read book Evolution of Solid Phase Microextraction Technology written by Janusz Pawliszyn and published by Royal Society of Chemistry. This book was released on 2023-03-24 with total page 663 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid Phase Microextraction (SPME) is a flexible and convenient sampling and sample preparation technique that extracts different kinds of analytes, including both volatile and non-volatile, without the use of a solvent. The technique facilitates fast, simple and automated determination of target analytes in a range of matrices. As it offers a green methodology, it is growing in popularity as an alternative tool in analytical chemistry to traditional methods. This book follows on in spirit from the editors' previous title, Applications of Solid Phase Microextraction and will introduce the reader to breakthrough methodologies and cutting edge applications. Although it assumes a good degree of SPME knowledge, an overview of the fundamentals is given before taking the reader through an update of the field. The reader will learn the basic principles and advantages of different SPME formats including the stir bar extraction techniques, thin film SPME, Bio-SPME, and new trends in different coatings. Applications in complex media, including food analysis, drug residues and bioanalysis are covered. Bringing together leading sample preparation academics from around the world, the editor has put together an informative new book, suitable for analytical chemists and practitioners utilising SPME tools in their research.

Solid-Phase Microextraction

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Publisher : MDPI
ISBN 13 : 303928262X
Total Pages : 266 pages
Book Rating : 4.0/5 (392 download)

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Book Synopsis Solid-Phase Microextraction by : Constantinos K. Zacharis

Download or read book Solid-Phase Microextraction written by Constantinos K. Zacharis and published by MDPI. This book was released on 2020-02-07 with total page 266 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers the most recent research activities and achievements regarding to the solid phase microextraction (SPME) technique. It is a powerful sample preparation tool that addresses the new challenges of analytical laboratories. Among others, its fundamental applications involved the sampling of volatile compounds from various matrixes. The demonstrated topics ranged from aroma characterization of various fruits, essential oils to the utilization of SPME for in-tube extraction and isolation of selected compounds from complex samples followed by state-of-the-art analytical techniques.

Solid Phase Microextraction

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Publisher : John Wiley & Sons
ISBN 13 : 9780471190349
Total Pages : 266 pages
Book Rating : 4.1/5 (93 download)

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Book Synopsis Solid Phase Microextraction by : Janusz Pawliszyn

Download or read book Solid Phase Microextraction written by Janusz Pawliszyn and published by John Wiley & Sons. This book was released on 1997-04-21 with total page 266 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gesetzliche Auflagen und ökonomische Erwägungen steigern den Bedarf an Propenpräparations- und -extraktionstechniken, die ohne toxische organische Lösungsmittel auskommen. Die hier erstmals in Buchform veröffentlichte Festphasen-Mikroextraktion (SPME) ist ein neuartiges Verfahren, das diesen Anforderungen entspricht und gegenwärtig apparativ umgesetzt wird. Der Erfinder selbst, ein international anerkannter Pionier auf dem Gebiet der lösungsmittelfreien Extraktion, erklärt theoretische Hintergründe und praktische Anwendungsmöglichkeiten. SPME ist einfach, kostengünstig, automatisierbar, zeit- und analytsparend. Interessant für Analytiker in Industrie und Forschung, für Spurenanalytik, Umwelt- und pharmazeutische Chemie.

Solid Phase Microextraction in Aqueous Sample Analysis

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Publisher :
ISBN 13 : 9780494433942
Total Pages : 165 pages
Book Rating : 4.4/5 (339 download)

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Book Synopsis Solid Phase Microextraction in Aqueous Sample Analysis by : Wennan Zhao

Download or read book Solid Phase Microextraction in Aqueous Sample Analysis written by Wennan Zhao and published by . This book was released on 2008 with total page 165 pages. Available in PDF, EPUB and Kindle. Book excerpt: This thesis presents enhanced analytical methods developed for complex aqueous sample analysis based on solid phase microextraction (SPME).

Applications of Solid Phase Microextraction

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Publisher : Royal Society of Chemistry
ISBN 13 : 9780854045259
Total Pages : 680 pages
Book Rating : 4.0/5 (452 download)

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Book Synopsis Applications of Solid Phase Microextraction by : Janusz Pawliszyn

Download or read book Applications of Solid Phase Microextraction written by Janusz Pawliszyn and published by Royal Society of Chemistry. This book was released on 1999 with total page 680 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid Phase Microextraction (SPME) has been introduced as a modern alternative to current sample preparation technology, and has a wide range of applications. Focusing on quantitative aspects of analysis, Applications of Solid Phase Microextraction aims to describe these applications. In industry, practical uses of SPME can be found in environmental, food, pharmaceutical, clinical and forensic applications, all of which are described in this book. Important scientific applications such as reaction monitoring, characterization of coatings and distributions of analytes in natural multiphase systems are also discussed. Throughout there are descriptions of new technologies, including new coatings and interfaces for analytical instrumentation (SPME/LC and SPME/CE), automation and calibration processes. Written by internationally recognised experts, edited by the scientist involved in the research since its infancy, and encompassing a wide range of applications, this book will be ideal for anyone wishing to explore the feasibility of using SPME technology.

Solid-phase Microextraction

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ISBN 13 :
Total Pages : 56 pages
Book Rating : 4.:/5 (47 download)

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Book Synopsis Solid-phase Microextraction by :

Download or read book Solid-phase Microextraction written by and published by . This book was released on 2000 with total page 56 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Analytical Techniques in Biosciences

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Publisher : Academic Press
ISBN 13 : 0128227990
Total Pages : 302 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Analytical Techniques in Biosciences by : Chukwuebuka Egbuna

Download or read book Analytical Techniques in Biosciences written by Chukwuebuka Egbuna and published by Academic Press. This book was released on 2021-10-21 with total page 302 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Techniques in Biosciences: From Basics to Applications presents comprehensive and up-to-date information on the various analytical techniques obtainable in bioscience research laboratories across the world. This book contains chapters that discuss the basic bioanalytical protocols and sample preparation guidelines. Commonly encountered analytical techniques, their working principles, and applications were presented. Techniques, considered in this book, include centrifugation techniques, electrophoretic techniques, chromatography, titrimetry, spectrometry, and hyphenated techniques. Subsequent chapters emphasize molecular weight determination and electroanalytical techniques, biosensors, and enzyme assay protocols. Other chapters detail microbial techniques, statistical methods, computational modeling, and immunology and immunochemistry. The book draws from experts from key institutions around the globe, who have simplified the chapters in a way that will be useful to early-stage researchers as well as advanced scientists. It is also carefully structured and integrated sequentially to aid flow, consistency, and continuity. This is a must-have reference for graduate students and researchers in the field of biosciences. Presents basic analytical protocols and sample-preparation guidelines Details the various analytical techniques, including centrifugation, spectrometry, chromatography, and titrimetry Describes advanced techniques such as hyphenated techniques, electroanalytical techniques, and the application of biosensors in biomedical research Presents biostatistical tools and methods and basic computational models in biosciences

Coal Tar Creosote

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Publisher : WHO
ISBN 13 :
Total Pages : 154 pages
Book Rating : 4.:/5 (319 download)

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Book Synopsis Coal Tar Creosote by : C. Melber

Download or read book Coal Tar Creosote written by C. Melber and published by WHO. This book was released on 2004 with total page 154 pages. Available in PDF, EPUB and Kindle. Book excerpt: On cover: IPCS International Programme on Chemical Safety. Published under the joint sponsorship of the United Nations Environment Programme, the International Labour Organization and the World Health Organization, and produced within the framework of the Inter-organization Programme for the Sound Management of Chemicals (IOMC)

Passive Sampling Techniques in Environmental Monitoring

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Publisher : Elsevier
ISBN 13 : 0080489508
Total Pages : 487 pages
Book Rating : 4.0/5 (84 download)

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Book Synopsis Passive Sampling Techniques in Environmental Monitoring by : Richard Greenwood

Download or read book Passive Sampling Techniques in Environmental Monitoring written by Richard Greenwood and published by Elsevier. This book was released on 2007-07-03 with total page 487 pages. Available in PDF, EPUB and Kindle. Book excerpt: Monitoring pollutants in air, soil and water is a routine requirement in the workplace, and in the wider environment. Passive samplers can provide a representative picture of levels of pollutants over a period of time from days to months by measuring the average concentrations to which they have been exposed. Air monitors are widely used, for instance to measure the exposure of workers to volatile compounds, but also for monitoring the fate of pollutants in the atmosphere. Passive sampling devices are now becomining increasingly used to monitor pollutants in rivers, coastal waters and ground water where contamination results from sources such as domestic and industrial discharges, and the use of agrochemicals. Passive Sampling Techniques in Environmental Monitoring provides a timely collection of information on a set of techniques that help monitor the quality of air, surface and ground waters. Passive sampling can provide an inexpensive means of obtaining a representative picture of quality over a period of time, even where levels of pollutants fluctuate due to discontinuous discharges or seasonal application of chemicals such as pesticides. Recent changes in legislation have increased the pressure to obtain better information than that provided by classical infrequent spot sampling.Brought together in one source, this book looks at the performance of a range of devices for the passive sampling of metals, and of non-polar and polar organic chemicals in air and in water. The strengths and weaknesses and the range of applicability of the technology are considered.* Comprehensive review of passive sampling - covering air, water and majority of available technologies in one volume* Chapters written by international specialist experts * Covers theory and applications, providing background information and guidelines for use in the field

Toxicological Profile for Tetrachloroethylene

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Publisher :
ISBN 13 :
Total Pages : 324 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Toxicological Profile for Tetrachloroethylene by :

Download or read book Toxicological Profile for Tetrachloroethylene written by and published by . This book was released on 1997 with total page 324 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Draft Toxicological Profile for Ethylbenzene

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Publisher :
ISBN 13 :
Total Pages : 324 pages
Book Rating : 4.:/5 (318 download)

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Book Synopsis Draft Toxicological Profile for Ethylbenzene by :

Download or read book Draft Toxicological Profile for Ethylbenzene written by and published by . This book was released on 2007 with total page 324 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Toxicological Profile for Styrene

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Publisher :
ISBN 13 :
Total Pages : 176 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Toxicological Profile for Styrene by :

Download or read book Toxicological Profile for Styrene written by and published by . This book was released on 1992 with total page 176 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Toxicological Profile for Methylene Chloride

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Publisher :
ISBN 13 :
Total Pages : 244 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Toxicological Profile for Methylene Chloride by :

Download or read book Toxicological Profile for Methylene Chloride written by and published by . This book was released on 1998 with total page 244 pages. Available in PDF, EPUB and Kindle. Book excerpt: