Solid State Nmr Spectroscopy For Biopolymers

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Solid State NMR Spectroscopy for Biopolymers

Author : Hazime Saitô
Publisher : Springer Science & Business Media
ISBN 13 : 1402043031
Total Pages : 455 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Solid State NMR Spectroscopy for Biopolymers by : Hazime Saitô

Download or read book Solid State NMR Spectroscopy for Biopolymers written by Hazime Saitô and published by Springer Science & Business Media. This book was released on 2006-08-05 with total page 455 pages. Available in PDF, EPUB and Kindle. Book excerpt: ‘‘Biopolymers’’ are polymeric materials of biological origin, including globular, membrane, and fibrous proteins, polypeptides, nucleic acids, po- saccharides, lipids, etc. and their assembly, although preference to respe- ive subjects may be different among readers who are more interested in their biological significance or industrial and/or medical applications. Nevert- less, characterizing or revealing their secondary structure and dynamics may be an equally very important and useful issue for both kinds of readers. Special interest in revealing the 3D structure of globular proteins, nucleic acids, and peptides was aroused in relation to the currently active Structural Biology. X-ray crystallography and multidimensional solution NMR sp- troscopy have proved to be the standard and indispensable means for this purpose. There remain, however, several limitations to this end, if one intends to expand its scope further. This is because these approaches are not always straightforward to characterize fibrous or membrane proteins owing to extreme difficulty in crystallization in the former, and insufficient spectral resolution due to sparing solubility or increased effective molecular mass in the presence of surrounding lipid bilayers in the latter.

Solid State NMR Studies of Biopolymers

Author : Anne E. McDermott
Publisher : John Wiley & Sons
ISBN 13 : 1118588886
Total Pages : 596 pages
Book Rating : 4.1/5 (185 download)

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Book Synopsis Solid State NMR Studies of Biopolymers by : Anne E. McDermott

Download or read book Solid State NMR Studies of Biopolymers written by Anne E. McDermott and published by John Wiley & Sons. This book was released on 2012-12-19 with total page 596 pages. Available in PDF, EPUB and Kindle. Book excerpt: The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The field of solid state NMR of biological samples [ssNMR] has blossomed in the past 5-10 years, and a cohesive overview of the technology is needed for new practitioners in industry and academia. This title provides an overview of Solid State NMR methods for studying structure dynamics and ligand-binding in biopolymers, and offers an overview of RF pulse sequences for various applications, including not only a systematic catalog but also a discussion of theoretical tools for analysis of pulse sequences. Practical examples of biochemical applications are included, along with a detailed discussion of the many aspects of sample preparation and handling that make spectroscopy on solid proteins successful. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here

NMR Applications in Biopolymers

Author : John W. Finley
Publisher : Springer Science & Business Media
ISBN 13 : 146845868X
Total Pages : 512 pages
Book Rating : 4.4/5 (684 download)

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Book Synopsis NMR Applications in Biopolymers by : John W. Finley

Download or read book NMR Applications in Biopolymers written by John W. Finley and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 512 pages. Available in PDF, EPUB and Kindle. Book excerpt: Elucidating the structures of biopolymers as they exist in nature has long been a goal of biochemists and biologists. Understanding how these substances interact with themselves, other solutes, and solvents can provide useful insights into many areas of biochemistry, agriculture, food science and medicine. Knowledge of the structure of a protein or complex carbohydrate in its native form provides guidelines for the chemical or genetic modifications often desired to optimize these compounds to specific needs and applications. For example, in the pharmaceutical industry, structure-function relationships involving biopolymers are studied rou tinely as a means to design new drugs and improve their efficacies. The tools to conduct structure investigations of biopolymers at the molecular level are limited in number. Historically X-ray crystallography has been the most attractive method to conduct studies of this type. How ever, X-ray methods can only be applied to highly ordered, crystalline materials, thus obviating studies of solution dynamics that are often critical to attaining a global understanding of biopolymer behavior. In recent years, nuclear magnetic resonance (NMR) spectroscopy has evolved to become a powerful tool to probe the structures of biopolymers in solution and in the solid state. NMR provides a means to study the dynamics of polymers in solution, and to examine the effects of solute, solvent and' other factors~n polymer behavior. With the development of 2D and 3D forms of NMR spectroscopy, it is now possible to assess the solution conforma tions of small proteins, oligonucleotides and oligosaccharides.

NMR Methods for Characterization of Synthetic and Natural Polymers

Author : Rongchun Zhang
Publisher : Royal Society of Chemistry
ISBN 13 : 178801863X
Total Pages : 590 pages
Book Rating : 4.7/5 (88 download)

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Book Synopsis NMR Methods for Characterization of Synthetic and Natural Polymers by : Rongchun Zhang

Download or read book NMR Methods for Characterization of Synthetic and Natural Polymers written by Rongchun Zhang and published by Royal Society of Chemistry. This book was released on 2019-07-29 with total page 590 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.

Biological NMR Spectroscopy

Author : John L. Markley
Publisher : Oxford University Press
ISBN 13 : 0195094689
Total Pages : 375 pages
Book Rating : 4.1/5 (95 download)

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Book Synopsis Biological NMR Spectroscopy by : John L. Markley

Download or read book Biological NMR Spectroscopy written by John L. Markley and published by Oxford University Press. This book was released on 1997-01-30 with total page 375 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents a critical assessment of progress on the use of nuclear magnetic resonance spectroscopy to determine the structure of proteins, including brief reviews of the history of the field along with coverage of current clinical and in vivo applications. The book, in honor of Oleg Jardetsky, one of the pioneers of the field, is edited by two of the most highly respected investigators using NMR, and features contributions by most of the leading workers in the field. It will be valued as a landmark publication that presents the state-of-the-art perspectives regarding one of today's most important technologies.

Handbook of Biopolymer-Based Materials

Author : Sabu Thomas
Publisher : John Wiley & Sons
ISBN 13 : 3527652477
Total Pages : 880 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Handbook of Biopolymer-Based Materials by : Sabu Thomas

Download or read book Handbook of Biopolymer-Based Materials written by Sabu Thomas and published by John Wiley & Sons. This book was released on 2013-04-16 with total page 880 pages. Available in PDF, EPUB and Kindle. Book excerpt: This first systematic scientific reference in the area of micro- and nanostructured biopolymer systems discusses in two volumes the morphology, structure, dynamics, properties and applications of all important biopolymers, as well as their blends, composites, interpenetrating networks and gels. Selected leading researchers from industry, academia, government and private research institutions around the globe comprehensively review recent accomplishments in the field. They examine the current state of the art, new challenges, and opportunities, discussing all the synthetic routes to the generation of both micro- and nano-morphologies, as well as the synthesis, characterization and application of porous biopolymers. An outstanding resource for anyone involved in the fi eld of eco-friendly biomaterials for advanced technologies.

Biopolymer Membranes and Films

Author : Mariana Agostini De Moraes
Publisher : Elsevier
ISBN 13 : 0128181354
Total Pages : 658 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Biopolymer Membranes and Films by : Mariana Agostini De Moraes

Download or read book Biopolymer Membranes and Films written by Mariana Agostini De Moraes and published by Elsevier. This book was released on 2020-06-19 with total page 658 pages. Available in PDF, EPUB and Kindle. Book excerpt: Biopolymer Membranes and Films: Health, Food, Environment, and Energy Applications presents the latest techniques for the design and preparation of biopolymer-based membranes and films, leading to a range of cutting-edge applications. The first part of the book introduces the fundamentals of biopolymers, two-dimensional systems, and the characterization of biopolymer membranes and films, considering physicochemical, mechanical and barrier properties. Subsequent sections are organized by application area, with each chapter explaining how biopolymer-based membranes or films can be developed for specific innovative uses across the health, food, environmental and energy sectors. This book is a valuable resource for researchers, scientists and advanced students involved in biopolymer science, polymer membranes and films, polymer chemistry and materials science, as well as for those in industry and academia who are looking to develop materials for advanced applications in the health, food science, environment or energy industries. - Presents detailed coverage of a range of novel applications in key strategic areas across health, food, environment and energy - Considers the difficulties associated with two-dimensional materials - Assists the reader in selecting the best materials and properties for specific applications - Helps researchers, scientists and engineers combine the enhanced properties of membranes and films with the sustainable characteristics of biopolymer-based materials

Annual Reports on NMR Spectroscopy

Author : Graham A. Webb
Publisher : Academic Press
ISBN 13 : 0080921817
Total Pages : 225 pages
Book Rating : 4.0/5 (89 download)

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Book Synopsis Annual Reports on NMR Spectroscopy by : Graham A. Webb

Download or read book Annual Reports on NMR Spectroscopy written by Graham A. Webb and published by Academic Press. This book was released on 2008-10-13 with total page 225 pages. Available in PDF, EPUB and Kindle. Book excerpt: The great importance of NMR in many areas of scientific research is once again highlighted in this volume of Annual Reports on NMR Spectroscopy. Provides updates on the latest developments in NMR spectroscopy Includes comprehensive review articles Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

Applications of NMR Spectroscopy

Author : Atta-ur-Rahman
Publisher : Bentham Science Publishers
ISBN 13 : 168108287X
Total Pages : 289 pages
Book Rating : 4.6/5 (81 download)

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Book Synopsis Applications of NMR Spectroscopy by : Atta-ur-Rahman

Download or read book Applications of NMR Spectroscopy written by Atta-ur-Rahman and published by Bentham Science Publishers. This book was released on 2016-11-22 with total page 289 pages. Available in PDF, EPUB and Kindle. Book excerpt: Applications of NMR Spectroscopy is a book series devoted to publishing the latest advances in the applications of nuclear magnetic resonance (NMR) spectroscopy in various fields of organic chemistry, biochemistry, health and agriculture. The fifth volume of the series features several reviews focusing on NMR spectroscopic techniques for identifying natural and synthetic compounds (polymer and peptide characterization, GABA in tinnitus affected mice), medical diagnosis and therapy (gliomas) and food analysis. The spectroscopic methods highlighted in this volume include high resolution proton magnetic resonance spectroscopy and solid state NMR.

Solid State NMR Spectroscopy

Author : Melinda J. Duer
Publisher : John Wiley & Sons
ISBN 13 : 0470999381
Total Pages : 592 pages
Book Rating : 4.4/5 (79 download)

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Book Synopsis Solid State NMR Spectroscopy by : Melinda J. Duer

Download or read book Solid State NMR Spectroscopy written by Melinda J. Duer and published by John Wiley & Sons. This book was released on 2008-04-15 with total page 592 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time. It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. This dual requirement is met through careful construction of the material within each chapter. The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR. The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter. The basic techniques that all chapters rely on are collected into a second chapter to avoid unnecessary repetition later. Remaining chapters in the "Fundamentals" part deal with the major areas of solid-state NMR which all solid-state NMR spectroscopists should know about. Each begins with an overview of the topic that puts the chapter in context. The basic principles upon which the techniques in the chapter rely are explained in a separate section. Each of these chapters exemplifies the principles and techniques with the applications most commonly found in current practice. The "Further Applications" section contains a series of shorter chapters which describe the NMR techniques used in other, more specific areas. The basic principles upon which these techniques rely will be expounded only if not already in the Fundamentals part.

Nuclear Magnetic Resonance

Author :
Publisher : Royal Society of Chemistry
ISBN 13 : 1849738122
Total Pages : 569 pages
Book Rating : 4.8/5 (497 download)

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Book Synopsis Nuclear Magnetic Resonance by :

Download or read book Nuclear Magnetic Resonance written by and published by Royal Society of Chemistry. This book was released on 2014-05-21 with total page 569 pages. Available in PDF, EPUB and Kindle. Book excerpt: Now in its 43rd volume, the Specialist Periodical Report in Nuclear Magnetic Resonance presents comprehensive and critical reviews of the recent literature, providing the reader with an informed summary of the field from invited authors. Several chapters in this volume are devoted to biochemistry, focussing on carbohydrates, lipids, and proteins and nucleic acids; Malcolm Prior also presents a chapter examining the recent literature of NMR in living systems and Cynthia Jameson reviews the theoretical and physical aspects of nuclear shielding, while Jaroslaw Jazwinski examines the theoretical aspects of spin-spin couplings. The lead volume editor, Krystyna Kamienska-Trela, presents a chapter on the applications of spin-spin couplings. Anyone wishing to update themselves on the recent and hottest developments in NMR will benefit from this volume, which deserves a place in any library or NMR facility. Purchasers of the print edition can register for free access to the electronic edition by returning the enclosed registration card.

NMR Spectroscopy

Author : Harald Günther
Publisher : John Wiley & Sons
ISBN 13 : 3527674772
Total Pages : 842 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis NMR Spectroscopy by : Harald Günther

Download or read book NMR Spectroscopy written by Harald Günther and published by John Wiley & Sons. This book was released on 2013-12-13 with total page 842 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is important for determining the 3D-structure of molecules. This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.

Characterization of Polymeric Biomaterials

Author : Maria Cristina Tanzi
Publisher : Woodhead Publishing
ISBN 13 : 0081007434
Total Pages : 503 pages
Book Rating : 4.0/5 (81 download)

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Book Synopsis Characterization of Polymeric Biomaterials by : Maria Cristina Tanzi

Download or read book Characterization of Polymeric Biomaterials written by Maria Cristina Tanzi and published by Woodhead Publishing. This book was released on 2017-06-20 with total page 503 pages. Available in PDF, EPUB and Kindle. Book excerpt: Characterization of Polymeric Biomaterials presents a comprehensive introduction on the topic before discussing the morphology and surface characterization of biomedical polymers. The structural, mechanical, and biological characterization is described in detail, followed by invaluable case studies of polymer biomaterial implants. With comprehensive coverage of both theoretical and experimental information, this title will provide scientists with an essential guide on the topic of these materials which are regularly used for clinical applications, such as implants and drug delivery devices. However, a range of novel polymers and the development and modification of existing medical polymers means that there is an ongoing need to satisfy particular design requirements. This book explains the critical and fundamentals methods to characterize polymer materials for biomedical applications. - Presents a self-contained reference on the characterization of polymeric biomaterials - Provides comprehensive information on how to characterize biomedical polymers in order to improve design and synthesis - Includes useful case studies that demonstrate the characterization of biomaterial implants

Polysaccharide Hydrogels

Author : Pietro Matricardi
Publisher : CRC Press
ISBN 13 : 9814613622
Total Pages : 527 pages
Book Rating : 4.8/5 (146 download)

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Book Synopsis Polysaccharide Hydrogels by : Pietro Matricardi

Download or read book Polysaccharide Hydrogels written by Pietro Matricardi and published by CRC Press. This book was released on 2016-01-05 with total page 527 pages. Available in PDF, EPUB and Kindle. Book excerpt: Hydrogels are an emerging area of interest in medicine as well as pharmaceutics, and their physico-chemical characterization is fundamental to their practical applications. Compared with synthetic polymers, polysaccharides that are widely present in living organisms and come from renewable sources are extremely advantageous for hydrogel formation.

Spin Dynamics

Author : Malcolm H. Levitt
Publisher : Wiley
ISBN 13 : 0470517123
Total Pages : 744 pages
Book Rating : 4.4/5 (75 download)

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Book Synopsis Spin Dynamics by : Malcolm H. Levitt

Download or read book Spin Dynamics written by Malcolm H. Levitt and published by Wiley. This book was released on 2008-07-31 with total page 744 pages. Available in PDF, EPUB and Kindle. Book excerpt: Spin Dynamics: Basics of Nuclear Magnetic Resonance, Second Edition is a comprehensive and modern introduction which focuses on those essential principles and concepts needed for a thorough understanding of the subject, rather than the practical aspects. The quantum theory of nuclear magnets is presented within a strong physical framework, supported by figures. The book assumes only a basic knowledge of complex numbers and matrices, and provides the reader with numerous worked examples and exercises to encourage understanding. With the explicit aim of carefully developing the subject from the beginning, the text starts with coverage of quarks and nucleons and progresses through to a detailed explanation of several important NMR experiments, including NMR imaging, COSY, NOESY and TROSY. Completely revised and updated, the Second Edition features new material on the properties and distributions of isotopes, chemical shift anisotropy and quadrupolar interactions, Pake patterns, spin echoes, slice selection in NMR imaging, and a complete new chapter on the NMR spectroscopy of quadrupolar nuclei. New appendices have been included on Euler angles, and coherence selection by field gradients. As in the first edition, all material is heavily supported by graphics, much of which is new to this edition. Written for undergraduates and postgraduate students taking a first course in NMR spectroscopy and for those needing an up-to-date account of the subject, this multi-disciplinary book will appeal to chemical, physical, material, life, medical, earth and environmental scientists. The detailed physical insights will also make the book of interest for experienced spectroscopists and NMR researchers. • An accessible and carefully written introduction, designed to help students to fully understand this complex and dynamic subject • Takes a multi-disciplinary approach, focusing on basic principles and concepts rather than the more practical aspects • Presents a strong pedagogical approach throughout, with emphasis placed on individual spins to aid understanding • Includes numerous worked examples, problems, further reading and additional notes Praise from the reviews of the First Edition: "This is an excellent book... that many teachers of NMR spectroscopy will cherish... It deserves to be a ‘classic’ among NMR spectroscopy texts." NMR IN BIOMEDICINE "I strongly recommend this book to everyone…it is probably the best modern comprehensive description of the subject." ANGEWANDTE CHEMIE, INTERNATIONAL EDITION

Experimental Approaches of NMR Spectroscopy

Author : The Nuclear Magnetic Resonance Society of Japan
Publisher : Springer
ISBN 13 : 9811059667
Total Pages : 634 pages
Book Rating : 4.8/5 (11 download)

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Book Synopsis Experimental Approaches of NMR Spectroscopy by : The Nuclear Magnetic Resonance Society of Japan

Download or read book Experimental Approaches of NMR Spectroscopy written by The Nuclear Magnetic Resonance Society of Japan and published by Springer. This book was released on 2017-11-23 with total page 634 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book describes the advanced developments in methodology and applications of NMR spectroscopy to life science and materials science. Experts who are leaders in the development of new methods and applications of life and material sciences have contributed an exciting range of topics that cover recent advances in structural determination of biological and material molecules, dynamic aspects of biological and material molecules, and development of novel NMR techniques, including resolution and sensitivity enhancement. First, this book particularly emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of NMR spectroscopy. Second, the book is designed for those who are involved in either developing the technique or expanding the NMR application fields by applying them to specific samples. Third, the Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.

NMR Spectroscopy of Biological Solids

Author : A. Ramamoorthy
Publisher : CRC Press
ISBN 13 : 1420027611
Total Pages : 368 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis NMR Spectroscopy of Biological Solids by : A. Ramamoorthy

Download or read book NMR Spectroscopy of Biological Solids written by A. Ramamoorthy and published by CRC Press. This book was released on 2005-09-22 with total page 368 pages. Available in PDF, EPUB and Kindle. Book excerpt: Over the past decade, a myriad of techniques have shown that solid-state nuclear magnetic resonance (NMR) can be used in a broad spectrum of applications with exceptionally impressive results. Solid-state NMR results can yield high-resolution details on the structure and function of many important biological solids, including viruses, fibril-formin