Sol Gel Synthesis And Characterization Of Mesoporous Ceria Membranes

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Sol-gel Synthesis and Characterization of Mesoporous Ceria Membranes

Author : Neelesh J. Rane
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (52 download)

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Book Synopsis Sol-gel Synthesis and Characterization of Mesoporous Ceria Membranes by : Neelesh J. Rane

Download or read book Sol-gel Synthesis and Characterization of Mesoporous Ceria Membranes written by Neelesh J. Rane and published by . This book was released on 2002 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: CeO2, has numerous applications in industry including catalysts, electrolytes and in superconductors. One of the major area in which CeO2 research is lacking is in mesoporous inorganic membranes. The use of inorganic instead of organic membranes is advantageous if one is dealing with high temperatures, aggressive mixtures (chemical, mechanical, microbiological), high pressures (no compaction of inorganic membranes) or separation circumstances which make frequent cleaning of the membrane necessary. In addition to the ultrafiltration and gas separations, ceria is also most attractive as support for ultrathin dense ceramic or metallic membranes because of its thermal expansion coefficient, which match more closely with that of some dense membrane materials. Few researchers tried to prepare supported ceria membranes by the sol gel method. However they were unsuccessful to coat ceria layer directly on the support. So they coated ceria on top of alpha-alumina layer making a multilayer system. The ceria coating obtained had a very low surface area and consisted of some pinholes and cracks. Membranes with a narrow pore size distribution, in which especially large pores should be absent, are necessary to obtain a high degree of separation of mixtures. The present work is an attempt to prepare crack free and pinhole free supported and unsupported mesoporous ceria membranes by the sol gel method. A systematic study on microstructure and chemical evolution of ceria sols was done and the best available sol, which can give required ceria film thickness, was used for membrane preparation. Factors such as solid concentration, surface area and the organic impurities in the sols were considered. Ceria sol derived from cerium (IV) nitrate precursor having solid concentration of 172 g/L of CeO2 and whose particles showed a surface area of 101 m2/g was selected for fabrication of porous ceria membranes. Ceria was coated on chemically treated alpha-alumina support by dip-coating method. The pore structure and permeability properties of the supported membrane were studied by helium permeation experiments. SEM image shows ceria top-layer of thickness 28micron with an average pore diameter of 6.42 nm obtained by single dip coating of the ceria sol on the alumina support. XRD data reveal the fluorite type structure of ceria membranes. The permeability of ceria membrane is however low inspite of its high porosity, because of the thick top-layer obtained by the single dip-coating of ceria sol. The ionic conductivity of the ceria membranes is 0.06 - 8.5 S/cm in the temperature range of 600 - 900oC. These properties were compared with those of yttria-stabilized-zirconia (YSZ) membranes reported in the literature.

The Sol-Gel Handbook

Author : David Levy
Publisher : John Wiley & Sons
ISBN 13 : 352767084X
Total Pages : 1616 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis The Sol-Gel Handbook by : David Levy

Download or read book The Sol-Gel Handbook written by David Levy and published by John Wiley & Sons. This book was released on 2015-08-28 with total page 1616 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive three-volume handbook brings together a review of the current state together with the latest developments in sol-gel technology to put forward new ideas. The first volume, dedicated to synthesis and shaping, gives an in-depth overview of the wet-chemical processes that constitute the core of the sol-gel method and presents the various pathways for the successful synthesis of inorganic and hybrid organic-inorganic materials, bio- and bio-inspired materials, powders, particles and fibers as well as sol-gel derived thin films, coatings and surfaces. The second volume deals with the mechanical, optical, electrical and magnetic properties of sol-gel derived materials and the methods for their characterization such as diffraction methods and nuclear magnetic resonance, infrared and Raman spectroscopies. The third volume concentrates on the various applications in the fields of membrane science, catalysis, energy research, biomaterials science, biomedicine, photonics and electronics.

Handbook of Sol-Gel Science and Technology

Author : Lisa Klein
Publisher : Springer Nature
ISBN 13 : 3319321013
Total Pages : 3755 pages
Book Rating : 4.3/5 (193 download)

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Book Synopsis Handbook of Sol-Gel Science and Technology by : Lisa Klein

Download or read book Handbook of Sol-Gel Science and Technology written by Lisa Klein and published by Springer Nature. This book was released on 2018-05-31 with total page 3755 pages. Available in PDF, EPUB and Kindle. Book excerpt: This completely updated and expanded second edition stands as a comprehensive knowledgebase on both the fundamentals and applications of this important materials processing method. The diverse, international team of contributing authors of this reference clarify in extensive detail properties and applications of sol-gel science and technology as it pertains to the production of substances, active and non-active, including optical, electronic, chemical, sensor, bio- and structural materials. Essential to a wide range of manufacturing industries, the compilation divides into the three complementary sections: Sol-Gel Processing, devoted to general aspects of processing and recently developed materials such as organic-inorganic hybrids, photonic crystals, ferroelectric coatings, and photocatalysts; Characterization of Sol-Gel Materials and Products, presenting contributions that highlight the notion that useful materials are only produced when characterization is tied to processing, such as determination of structure by NMR, in-situ characterization of the sol-gel reaction process, determination of microstructure of oxide gels, characterization of porous structure of gels by the surface measurements, and characterization of organic-inorganic hybrid; and Applications of Sol-Gel Technology, covering applications such as the sol-gel method used in processing of bulk silica glasses, bulk porous gels prepared by sol-gel method, application of sol-gel method to fabrication of glass and ceramic fibers, reflective and antireflective coating films, application of sol-gel method to formation of photocatalytic coating films, and application of sol-gel method to bioactive coating films. The comprehensive scope and integrated treatment of topics make this reference volume ideal for R&D scientists and engineers across a wide range of disciplines and professional interests.

The Sol-Gel Handbook, 3 Volume Set

Author : David Levy
Publisher : John Wiley & Sons
ISBN 13 : 3527334866
Total Pages : 1604 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis The Sol-Gel Handbook, 3 Volume Set by : David Levy

Download or read book The Sol-Gel Handbook, 3 Volume Set written by David Levy and published by John Wiley & Sons. This book was released on 2015-11-02 with total page 1604 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive three-volume handbook brings together a review of the current state together with the latest developments in sol-gel technology to put forward new ideas. The first volume, dedicated to synthesis and shaping, gives an in-depth overview of the wet-chemical processes that constitute the core of the sol-gel method and presents the various pathways for the successful synthesis of inorganic and hybrid organic-inorganic materials, bio- and bio-inspired materials, powders, particles and fibers as well as sol-gel derived thin films, coatings and surfaces. The second volume deals with the mechanical, optical, electrical and magnetic properties of sol-gel derived materials and the methods for their characterization such as diffraction methods and nuclear magnetic resonance, infrared and Raman spectroscopies. The third volume concentrates on the various applications in the fields of membrane science, catalysis, energy research, biomaterials science, biomedicine, photonics and electronics.

Progress in Sol-Gel Production

Author : Luis Esquivias
Publisher : Trans Tech Publications Ltd
ISBN 13 : 3038132802
Total Pages : 194 pages
Book Rating : 4.0/5 (381 download)

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Book Synopsis Progress in Sol-Gel Production by : Luis Esquivias

Download or read book Progress in Sol-Gel Production written by Luis Esquivias and published by Trans Tech Publications Ltd. This book was released on 2008-10-21 with total page 194 pages. Available in PDF, EPUB and Kindle. Book excerpt: Volume is indexed by Thomson Reuters BCI (WoS). This book presents contributions covering the more recent applications of Sol-Gel science. Ceramics and films produced from gels were among the first applications developed by early sol-gel researchers. The possibility of tailoring the structure, and controlling particle growth, has permitted ever more advanced materials to be obtained. Several other potential applications were foreseen fifteen to twenty year ago, but their realization became possible only after extensive research on precursors had enabled progress towards the preparation of new pre-forms.

Advanced Nanomaterials for Catalysis and Energy

Author : Vladislav A. Sadykov
Publisher : Elsevier
ISBN 13 : 012814808X
Total Pages : 590 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Advanced Nanomaterials for Catalysis and Energy by : Vladislav A. Sadykov

Download or read book Advanced Nanomaterials for Catalysis and Energy written by Vladislav A. Sadykov and published by Elsevier. This book was released on 2018-08-27 with total page 590 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advanced Nanomaterials for Catalysis and Energy: Synthesis, Characterization and Applications outlines new approaches to the synthesis of nanomaterials (synthesis in flow conditions, laser electrodispersion of single metals or alloys on carbon or oxide supports, mechanochemistry, sol-gel routes, etc.) to provide systems with a narrow particle size distribution, controlled metal-support interaction and nanocomposites with uniform spatial distribution of domains of different phases, even in dense sintered materials. Methods for characterization of real structure and surface properties of nanomaterials are discussed, including synchrotron radiation diffraction and X-ray photoelectron spectroscopy studies, neutronography, transmission/scanning electron microscopy with elemental analysis, and more. The book covers the effect of nanosystems' composition, bulk and surface properties, metal-support interaction, particle size and morphology, deposition density, etc. on their functional properties (transport features, catalytic activity and reaction mechanism). Finally, it includes examples of various developed nanostructured solid electrolytes and mixed ionic-electronic conductors as materials in solid oxide fuel cells and asymmetric supported membranes for oxygen and hydrogen separation. Outlines synthetic and characterization methods for nanocatalysts Relates nanocatalysts' properties to their specific applications Proposes optimization methods aiming at specific applications

Handbook of sol-gel science and technology. 3. Applications of sol-gel technology

Author : Sumio Sakka
Publisher : Springer Science & Business Media
ISBN 13 : 9781402079689
Total Pages : 834 pages
Book Rating : 4.0/5 (796 download)

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Book Synopsis Handbook of sol-gel science and technology. 3. Applications of sol-gel technology by : Sumio Sakka

Download or read book Handbook of sol-gel science and technology. 3. Applications of sol-gel technology written by Sumio Sakka and published by Springer Science & Business Media. This book was released on 2005 with total page 834 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since Dr. Disiich of Germany prepared a glass lens by the sol-gel method around 1970, sol-gel science and technology has continued to develop. Since then this field has seen remarkable technical developments as well as a broadening of the applications of sol-gel science and technology. There is a growing need for a comprehensive reference that treats both the fundamentals and the applications, and this is the aim of "Handbook of Sol-Gel Science and Technology."The primary purpose of sol-gel science and technology is to produce materials, active and non-active including optical, electronic, chemical, sensor, bio- and structural materials. This means that sol-gel science and technology is related to all kinds of manufacturing industries. Thus Volume 1, "Sol-Gel Processing," is devoted to general aspects of processing. Newly developed materials such as organic-inorganic hybrids, photonic crystals, ferroelectric coatings, photocatalysts will be covered. Topics in this volume include: Volume 2, "Characterization of Sol-Gel Materials and Products, "highlights the important fact that useful materials are only produced when characterization is tied to processing. Furthermore, characterization is essential to the understanding of nanostructured materials, and sol-gel technology is a most important technology in this new field. Since nanomaterials display their functional property based on their nano- and micro-structure, "characterization" is very important. Topics found in Volume 2 include: Sol-gel technology is a versatile technology, making it possible to produce a wide variety of materials and to provide existing substances with novel properties. This technology was applied to producingnovel materials, for example organic-inorganic hybrids, which are quite difficult to make by other fabricating techniques, and it was also applied to producing materials based on high temperature superconducting oxides. "Applications of Sol-Gel Technology," (Volume 3), will cover applications such as:

Handbook of sol-gel science and technology. 1. Sol-gel processing

Author : Sumio Sakka
Publisher : Springer Science & Business Media
ISBN 13 : 9781402079665
Total Pages : 716 pages
Book Rating : 4.0/5 (796 download)

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Book Synopsis Handbook of sol-gel science and technology. 1. Sol-gel processing by : Sumio Sakka

Download or read book Handbook of sol-gel science and technology. 1. Sol-gel processing written by Sumio Sakka and published by Springer Science & Business Media. This book was released on 2005 with total page 716 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since Dr. Disiich of Germany prepared a glass lens by the sol-gel method around 1970, sol-gel science and technology has continued to develop. Since then this field has seen remarkable technical developments as well as a broadening of the applications of sol-gel science and technology. There is a growing need for a comprehensive reference that treats both the fundamentals and the applications, and this is the aim of "Handbook of Sol-Gel Science and Technology."The primary purpose of sol-gel science and technology is to produce materials, active and non-active including optical, electronic, chemical, sensor, bio- and structural materials. This means that sol-gel science and technology is related to all kinds of manufacturing industries. Thus Volume 1, "Sol-Gel Processing," is devoted to general aspects of processing. Newly developed materials such as organic-inorganic hybrids, photonic crystals, ferroelectric coatings, photocatalysts will be covered. Topics in this volume include: Volume 2, "Characterization of Sol-Gel Materials and Products, "highlights the important fact that useful materials are only produced when characterization is tied to processing. Furthermore, characterization is essential to the understanding of nanostructured materials, and sol-gel technology is a most important technology in this new field. Since nanomaterials display their functional property based on their nano- and micro-structure, "characterization" is very important. Topics found in Volume 2 include: Sol-gel technology is a versatile technology, making it possible to produce a wide variety of materials and to provide existing substances with novel properties. This technology was applied to producingnovel materials, for example organic-inorganic hybrids, which are quite difficult to make by other fabricating techniques, and it was also applied to producing materials based on high temperature superconducting oxides. "Applications of Sol-Gel Technology," (Volume 3), will cover applications such as:

SOL-gel Derived Ceramic Alumina Membranes for High Temperature Application

Author : Shahid Qayum Mohammad Qayum
Publisher :
ISBN 13 :
Total Pages : 119 pages
Book Rating : 4.:/5 (96 download)

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Book Synopsis SOL-gel Derived Ceramic Alumina Membranes for High Temperature Application by : Shahid Qayum Mohammad Qayum

Download or read book SOL-gel Derived Ceramic Alumina Membranes for High Temperature Application written by Shahid Qayum Mohammad Qayum and published by . This book was released on 1996 with total page 119 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Sol-Gel Method

Author : Guadalupe Valverde Aguilar
Publisher : BoD – Books on Demand
ISBN 13 : 1789853338
Total Pages : 108 pages
Book Rating : 4.7/5 (898 download)

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Book Synopsis Sol-Gel Method by : Guadalupe Valverde Aguilar

Download or read book Sol-Gel Method written by Guadalupe Valverde Aguilar and published by BoD – Books on Demand. This book was released on 2019-02-13 with total page 108 pages. Available in PDF, EPUB and Kindle. Book excerpt: The sol-gel method is a powerful route of synthesis used worldwide. It produces bulk, nano- and mesostructured sol-gel materials, which can encapsulate metallic and magnetic nanoparticles, non-linear azochromophores, perovskites, organic dyes, biological molecules, etc.. This can have interesting applications for catalysis, photocatalysis; drug delivery for treatment of neurodegenerative diseases such as cancer, Parkinson's and Azheimer's. In this book, valuable contributions related to novel materials synthesized by the sol-gel route are provided. The effect of the sol-gel method to synthesize these materials with potential properties is described, and how the variation of the parameters during the synthesis influences their design and allows to adjust their properties according to the desired application is discussed.

Sol-gel Synthesis and Characterization of MAI2O4 (M

Author : Motloung Setumo Victor
Publisher :
ISBN 13 :
Total Pages : 290 pages
Book Rating : 4.:/5 (919 download)

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Book Synopsis Sol-gel Synthesis and Characterization of MAI2O4 (M by : Motloung Setumo Victor

Download or read book Sol-gel Synthesis and Characterization of MAI2O4 (M written by Motloung Setumo Victor and published by . This book was released on 2014 with total page 290 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Emerging Fields in Sol-Gel Science and Technology

Author : Tessy Maria Lopez
Publisher : Springer Science & Business Media
ISBN 13 : 146150449X
Total Pages : 456 pages
Book Rating : 4.4/5 (615 download)

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Book Synopsis Emerging Fields in Sol-Gel Science and Technology by : Tessy Maria Lopez

Download or read book Emerging Fields in Sol-Gel Science and Technology written by Tessy Maria Lopez and published by Springer Science & Business Media. This book was released on 2013-11-27 with total page 456 pages. Available in PDF, EPUB and Kindle. Book excerpt: Emerging Fields in Sol-gel Science and Technology contains selected papers from the symposium on "Sol-Gel and Vitreous Materials and Applications" held during the International Materials Research Congress in Cancún, México in August 2002. One hundred and twenty researchers representing 10 countries attended this symposium. Some of the subjects covered in this symposium include 1.) synthesis of new materials endowed with outstanding and non-conventional optical, magnetic, electrical, thermal, catalytic, and mechanical properties; 2.) study of the sorption properties of model porous materials in order to test the validity of previous and recent theories; 3.) theoretical studies related to density functional theory, fractal and scaling law approaches, 4.) synthesis of biomaterials for use in medicine and pollution control; 5.) application of sol-gel colloids in the fine-chemistry industry in products such as fragrances and pharmaceuticals; 6.) development of special vitreous materials; 7.) implementation of inorganic thin films, and 8.) synthesis of materials for energy saving.

Sol-Gel Preparation and Characterization of Metal-Silica and Metal Oxide-Silica Nanocomposites

Author : G. Piccaluga
Publisher : Trans Tech Publications Ltd
ISBN 13 : 3035705941
Total Pages : 56 pages
Book Rating : 4.0/5 (357 download)

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Book Synopsis Sol-Gel Preparation and Characterization of Metal-Silica and Metal Oxide-Silica Nanocomposites by : G. Piccaluga

Download or read book Sol-Gel Preparation and Characterization of Metal-Silica and Metal Oxide-Silica Nanocomposites written by G. Piccaluga and published by Trans Tech Publications Ltd. This book was released on 2000-02-21 with total page 56 pages. Available in PDF, EPUB and Kindle. Book excerpt: Materials with nanometer size particles exhibit unique chemical and physical properties. In particular, nanocomposite materials, composed of nanometric metal and metal oxide particles embedded in vitreous matrices, present a variety of interesting magnetic, electric and catalytic properties, that are strongly size-dependent. Among the different preparation methods which can be used to obtain this kind of materials, the sol-gel process is particularly interesting because it is affected by several parameters which allow a versatile control of the structural, textural and chemical properties of the final products. The present volume focusses on the preparation of metal-silica and metal oxide-silica (Me=Ni, Fe, Zn) nanocomposites by the sol-gel method and the characterization of their structural and magnetic properties.

Sol-Gel Chemistry Applied to Materials Science

Author : Michelina Catauro
Publisher : MDPI
ISBN 13 : 3039213539
Total Pages : 216 pages
Book Rating : 4.0/5 (392 download)

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Book Synopsis Sol-Gel Chemistry Applied to Materials Science by : Michelina Catauro

Download or read book Sol-Gel Chemistry Applied to Materials Science written by Michelina Catauro and published by MDPI. This book was released on 2019-10-14 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt: Sol–gel technology is a contemporary advancement in science that requires taking a multidisciplinary approach with regard to its various applications. This book highlights some applications of the sol–gel technology, including protective coatings, catalysts, piezoelectric devices, wave guides, lenses, high-strength ceramics, superconductors, synthesis of nanoparticles, and insulating materials. In particular, for biotechnological applications, biomolecules or the incorporation of bioactive substances into the sol–gel matrix has been extensively studied and has been a challenge for many researchers. Some sol–gel materials are widely applied in light-emitting diodes, solar cells, sensing, catalysis, integration in photovoltaic devices, and more recently in biosensing, bioimaging, or medical diagnosis; others can be considered excellent drug delivery systems. The goal of an ideal drug delivery system is the prompt delivery of a therapeutic amount of the drug to the proper site in the body, where the desired drug concentration can be maintained. The interactions between drugs and the sol–gel system can affect the release rate. In conclusion, the sol–gel synthesis method offers mixing at the molecular level and is able to improve the chemical homogeneity of the resulting composite. This opens new doors not only regarding compositions of previously unattainable materials, but also to unique structures with different applications.

Sol-Gel Processing for Conventional and Alternative Energy

Author : Mario Aparicio
Publisher : Springer Science & Business Media
ISBN 13 : 1461419573
Total Pages : 399 pages
Book Rating : 4.4/5 (614 download)

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Book Synopsis Sol-Gel Processing for Conventional and Alternative Energy by : Mario Aparicio

Download or read book Sol-Gel Processing for Conventional and Alternative Energy written by Mario Aparicio and published by Springer Science & Business Media. This book was released on 2012-02-04 with total page 399 pages. Available in PDF, EPUB and Kindle. Book excerpt: Sol-Gel Processing for Conventional and Alternative Energy is a comprehensive source of information on the use of sol-gel processing in materials in energy systems, conversion, storage, and generation. The volume editors include numerous applications, primarily in nuclear fuel processing, electrolytes for fuel cells, and dye-sensitized solar cells (DSSC). In addition to examining contemporary processing, properties, and industrial applications, "Sol-Gel Processing for Conventional and Alternative Energy" identifies materials challenges presented by conventional and alternative energy generation that require new materials and innovative processing. Each chapter is written by an internationally respected researcher. The book provides a state-of-the-art treatment of different aspects of materials for energy production, with a focus on processing, and covers related topics such as carbon sequestration, clean energy, and biofuels.

Sol-Gel Materials for Energy, Environment and Electronic Applications

Author : Suresh C. Pillai
Publisher : Springer
ISBN 13 : 3319501445
Total Pages : 323 pages
Book Rating : 4.3/5 (195 download)

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Book Synopsis Sol-Gel Materials for Energy, Environment and Electronic Applications by : Suresh C. Pillai

Download or read book Sol-Gel Materials for Energy, Environment and Electronic Applications written by Suresh C. Pillai and published by Springer. This book was released on 2017-02-16 with total page 323 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume provides expert coverage of the state-of-the-art in sol-gel materials for functional applications in energy, environment and electronics. The use of sol-gel technology has become a hotbed for cutting edge developments in many fields due to the accessibility of advanced materials through low energy processes. The book offers a broad view of this growing research area from basic science through high-level applications with the potential for commercialization and industrial use. Taking an integrated approach, expert chapters present a wide range of topics, from photocatalysts, solar cells and optics, to thin films and materials for energy storage and conversion, demonstrating the combined use of chemistry, physics, materials science and engineering in the search for solutions to some of the most challenging problems of our time.

Synthesis and Characterization of Microporous Silica Membranes Fabricated Through Pore Size Reduction of Mesoporous Silica Membranes Using Catalyzed Atomic Layer Deposition

Download Synthesis and Characterization of Microporous Silica Membranes Fabricated Through Pore Size Reduction of Mesoporous Silica Membranes Using Catalyzed Atomic Layer Deposition PDF Online Free

Author : Benjamin A. McCool
Publisher :
ISBN 13 :
Total Pages : 246 pages
Book Rating : 4.:/5 (623 download)

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Book Synopsis Synthesis and Characterization of Microporous Silica Membranes Fabricated Through Pore Size Reduction of Mesoporous Silica Membranes Using Catalyzed Atomic Layer Deposition by : Benjamin A. McCool

Download or read book Synthesis and Characterization of Microporous Silica Membranes Fabricated Through Pore Size Reduction of Mesoporous Silica Membranes Using Catalyzed Atomic Layer Deposition written by Benjamin A. McCool and published by . This book was released on 2004 with total page 246 pages. Available in PDF, EPUB and Kindle. Book excerpt: