Pyrolysis - GC/MS Data Book of Synthetic Polymers

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Author :
Publisher : Elsevier
ISBN 13 : 0444538933
Total Pages : 405 pages
Book Rating : 4.4/5 (445 download)

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Book Synopsis Pyrolysis - GC/MS Data Book of Synthetic Polymers by : Shin Tsuge

Download or read book Pyrolysis - GC/MS Data Book of Synthetic Polymers written by Shin Tsuge and published by Elsevier. This book was released on 2011-08-02 with total page 405 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample

Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials

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Author :
Publisher : World Scientific
ISBN 13 : 1786345773
Total Pages : 267 pages
Book Rating : 4.7/5 (863 download)

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Book Synopsis Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials written by Peter Kusch and published by World Scientific. This book was released on 2018-10-08 with total page 267 pages. Available in PDF, EPUB and Kindle. Book excerpt: The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.

Emerging Energetic Materials: Synthesis, Physicochemical, and Detonation Properties

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Publisher : Springer
ISBN 13 : 9402412018
Total Pages : 477 pages
Book Rating : 4.4/5 (24 download)

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Book Synopsis Emerging Energetic Materials: Synthesis, Physicochemical, and Detonation Properties by : Dabir S. Viswanath

Download or read book Emerging Energetic Materials: Synthesis, Physicochemical, and Detonation Properties written by Dabir S. Viswanath and published by Springer. This book was released on 2018-01-02 with total page 477 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book summarizes science and technology of a new generation of high-energy andinsensitive explosives. The objective is to provide professionals with comprehensiveinformation on the synthesis and the physicochemical and detonation properties ofthe explosives. Potential technologies applicable for treatment of contaminated wastestreams from manufacturing facilities and environmental matrices are also be included.This book provides the reader an insight into the depth and breadth of theoreticaland empirical models and experimental techniques currently being developed in thefield of energetic materials. It presents the latest research by DoD engineers andscientists, and some of DoD’s academic and industrial researcher partners. The topicsexplored and the simulations developed or modified for the purposes of energetics mayfind application in other closely related fields, such as the pharmaceutical industry.One of the key features of the book is the treatment of wastewaters generated duringmanufacturing of these energetic materials.

Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition)

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Author :
Publisher : World Scientific
ISBN 13 : 1800613008
Total Pages : 383 pages
Book Rating : 4.8/5 (6 download)

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Book Synopsis Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) by : Peter Kusch

Download or read book Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) written by Peter Kusch and published by World Scientific. This book was released on 2023-08-28 with total page 383 pages. Available in PDF, EPUB and Kindle. Book excerpt: Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.

Sample Preparation in Chromatography

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Publisher : Elsevier
ISBN 13 : 0080540708
Total Pages : 949 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Sample Preparation in Chromatography by : S.C. Moldoveanu

Download or read book Sample Preparation in Chromatography written by S.C. Moldoveanu and published by Elsevier. This book was released on 2002-05-08 with total page 949 pages. Available in PDF, EPUB and Kindle. Book excerpt: Sample preparation is an essential step in many analyses. This book approaches the topic of sample preparation in chromatography in a methodical way, viewing it as a logical connection between sample collection and analytical chromatography. Providing a guide for choosing the appropriate sample preparation for a given analysis, this book describes various ways to process the sample, explaining the principle, discussing the advantages and disadvantages, describing the applicability to different types of samples, and showing the fitness to specific chromatographic determinations. The first part of the book contains an overview of sample preparation showing its relation to sample collection and to the core chromatographic analysis. The second part covers procedures that do not use chemical modifications of the analyte and includes methods for sample dissolution, concentration and cleanup designed mainly for modifying the initial matrix of the sample. This part starts with conventional separations such as filtration and distillation and finishes with more advanced techniques such as solid phase extraction and electroseparations. The third part gives a description of the chemical modifications that can be performed on a sample either for fractionation purposes or to improve a specific property of the analyte. This part includes derivatizations, polymer chemical degradations, and pyrolysis.

Analytical Pyrolysis

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Author :
Publisher : BoD – Books on Demand
ISBN 13 : 1789849586
Total Pages : 104 pages
Book Rating : 4.7/5 (898 download)

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Book Synopsis Analytical Pyrolysis by : Peter Kusch

Download or read book Analytical Pyrolysis written by Peter Kusch and published by BoD – Books on Demand. This book was released on 2019-02-13 with total page 104 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical pyrolysis deals with the structural identification and quantitation of pyrolysis products with the ultimate aim of establishing the identity of the original material and the mechanisms of its thermal decomposition. The pyrolytic process is carried out in a pyrolyzer interfaced with analytical instrumentation such as gas chromatography (GC), mass spectrometry (MS), gas chromatography coupled with mass spectrometry (GC/MS), or with Fourier-transform infrared spectroscopy (GC/FTIR). By measurement and identification of pyrolysis products, the molecular composition of the original sample can often be reconstructed.This book is the outcome of contributions by experts in the field of pyrolysis and includes applications of the analytical pyrolysis-GC/MS to characterize the structure of synthetic organic polymers and lignocellulosic materials as well as cellulosic pulps and isolated lignins, solid wood, waste particle board, and bio-oil. The thermal degradation of cellulose and biomass is examined by scanning electron micrography, FTIR spectroscopy, thermogravimetry (TG), differential thermal analysis, and TG/MS. The calorimetric determination of high heating values of different raw biomass, plastic waste, and biomass/plastic waste mixtures and their by-products resulting from pyrolysis is described.

Principles and Practice of Modern Chromatographic Methods

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Publisher : Academic Press
ISBN 13 : 012822097X
Total Pages : 532 pages
Book Rating : 4.1/5 (282 download)

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Book Synopsis Principles and Practice of Modern Chromatographic Methods by : Kevin Robards

Download or read book Principles and Practice of Modern Chromatographic Methods written by Kevin Robards and published by Academic Press. This book was released on 2021-12-03 with total page 532 pages. Available in PDF, EPUB and Kindle. Book excerpt: Principles and Practice of Modern Chromatographic Methods, Second Edition takes a comprehensive, unified approach in its presentation of chromatographic techniques. Like the first edition, the book provides a scientifically rigid, but easy-to-follow presentation of chromatography concepts that begins with the purpose and intent of chromatographic theory - the "what and why that are left out of other books attempting to cover these principles. This fully revised second edition brings the content up-to-date, covering recent developments in several new sections and an additional chapter on composite methods. New topics include sample profiling, sample preparation, sustainable green chemistry, 2D chromatography, miniaturization/nano-LC, HILIC, and more. - Contains thorough chapters that begin with an updated schematic overview and a visual representation of the content - Avoids the obfuscation of different terminologies and classification systems that are prevalent in the area, such as the relationship between liquid chromatography and column chromatography - Provides integrated and comprehensive topic coverage based on chromatographic bibliometrics and survey reports on the relative usage of chromatographic techniques

The Analysis and Comparison of Adhesives by Pyrolysis Gas Chromatography/mass Spectrometry

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Publisher :
ISBN 13 :
Total Pages : 192 pages
Book Rating : 4.3/5 (129 download)

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Book Synopsis The Analysis and Comparison of Adhesives by Pyrolysis Gas Chromatography/mass Spectrometry by : Kirsten Renee James

Download or read book The Analysis and Comparison of Adhesives by Pyrolysis Gas Chromatography/mass Spectrometry written by Kirsten Renee James and published by . This book was released on 2003 with total page 192 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Monthly Catalog of United States Government Publications

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Publisher :
ISBN 13 :
Total Pages : 658 pages
Book Rating : 4.3/5 (243 download)

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Book Synopsis Monthly Catalog of United States Government Publications by :

Download or read book Monthly Catalog of United States Government Publications written by and published by . This book was released on 2000 with total page 658 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Methods in Lignin Chemistry

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Publisher : Springer Science & Business Media
ISBN 13 : 3642740650
Total Pages : 595 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Methods in Lignin Chemistry by : Stephen Y. Lin

Download or read book Methods in Lignin Chemistry written by Stephen Y. Lin and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 595 pages. Available in PDF, EPUB and Kindle. Book excerpt: An up-to-date compilation of the theoretical background and practical procedures involved in lignin characterization. Whenever possible, the procedures are presented in sufficient detail to enable the reader to perform the analysis solely by following the step-by-step description. The advantages and limitations of individual methods are discussed and, more importantly, illustrated by typical analytical data in comparison to results obtained from other methods. This handbook serves the need of researchers and other professionals in academia, the pulp and paper industry as well as allied industries. It is equally useful for those with no previous experience in lignin or lignocellulosics.

Analytical Methods for Biomass Characterization and Conversion

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Publisher : Elsevier
ISBN 13 : 0128156066
Total Pages : 262 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Analytical Methods for Biomass Characterization and Conversion by : David C. Dayton

Download or read book Analytical Methods for Biomass Characterization and Conversion written by David C. Dayton and published by Elsevier. This book was released on 2019-11-05 with total page 262 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Methods for Biomass Characterization and Conversion is a thorough resource for researchers, students and professors who investigate the use of biomass for fuels, chemicals and products. Advanced analytical chemistry methods and techniques can now provide detailed compositional and chemical measurements of biomass, biomass conversion process streams, intermediates and products. This volume from the Emerging Issues in Analytical Chemistry series brings together the current knowledge on each of these methods, including spectroscopic methods (Fourier Transform Infrared Spectroscopy, Near-infrared Spectroscopy, Solid State Nuclear Magnetic Resonance), pyrolysis (Gas Chromatography/Mass Spectrometry), Liquid Chromatography/High Performance Liquid Chromatography, Liquid Chromatography/Mass Spectrometry, and so on. Authors David C. Dayton and Thomas D. Foust show how these can be used for measuring biomass composition and for determining the composition of intermediates with regard to subsequent processing for biofuels, bio-chemicals and bio-based products. - Covers the broad range of techniques and applications that have been developed and perfected in the last decade - Highlights specific analyses required for understanding biomass conversion to select intermediates - Provides references to seminal books, review articles and technical articles that go into greater depth, serving as a basis for further study

Evaluation of a Computer Program for GC-MS Specific Ion Monitoring

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Publisher :
ISBN 13 :
Total Pages : 348 pages
Book Rating : 4.:/5 (2 download)

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Book Synopsis Evaluation of a Computer Program for GC-MS Specific Ion Monitoring by : Ann Alford-Stevens

Download or read book Evaluation of a Computer Program for GC-MS Specific Ion Monitoring written by Ann Alford-Stevens and published by . This book was released on 1974 with total page 348 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Solar Energy Update

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Publisher :
ISBN 13 :
Total Pages : 370 pages
Book Rating : 4.3/5 ( download)

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Book Synopsis Solar Energy Update by :

Download or read book Solar Energy Update written by and published by . This book was released on 1983-03 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Plastics to Energy

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Publisher : William Andrew
ISBN 13 : 0128131411
Total Pages : 560 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Plastics to Energy by : Sultan Al-Salem

Download or read book Plastics to Energy written by Sultan Al-Salem and published by William Andrew. This book was released on 2018-11-05 with total page 560 pages. Available in PDF, EPUB and Kindle. Book excerpt: Plastics to Energy: Fuel, Chemicals, and Sustainability Implications covers important trends in the science and technology of polymer recovery, such as the thermo-chemical treatment of plastics, the impact of environmental degradation on mechanical recycling, incineration and thermal unit design, and new options in biodegradable plastics. The book also introduces product development opportunities from waste materials and discusses the main processes and pathways of the conversion of polymeric materials to energy, fuel and chemicals. A particular focus is placed on industrial case studies and academic reviews, providing a practical emphasis that enables plastics practitioners involved in end-of-life aspects to employ these processes. Final sections examine lifecycle and cost analysis of different plastic waste management processes, exploring the potential of various techniques in modelling, optimization and simulation of waste management options. - Introduces new pathways for the end-of-life treatment of plastics and polymers, including conversion to energy, fuel and other chemicals - Compares different options to assist materials scientists, engineers and waste management practitioners to choose the most effective and sustainable option - Covers the latest trends in the science and technology of polymer energy recovery

Fossil Energy Update

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Publisher :
ISBN 13 :
Total Pages : 748 pages
Book Rating : 4.:/5 (31 download)

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Book Synopsis Fossil Energy Update by :

Download or read book Fossil Energy Update written by and published by . This book was released on 1977 with total page 748 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Energy Research Abstracts

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Publisher :
ISBN 13 :
Total Pages : 474 pages
Book Rating : 4.0/5 ( download)

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Book Synopsis Energy Research Abstracts by :

Download or read book Energy Research Abstracts written by and published by . This book was released on 1992-12 with total page 474 pages. Available in PDF, EPUB and Kindle. Book excerpt:

NBS Special Publication

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Publisher :
ISBN 13 :
Total Pages : 684 pages
Book Rating : 4.F/5 ( download)

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Book Synopsis NBS Special Publication by :

Download or read book NBS Special Publication written by and published by . This book was released on 1968 with total page 684 pages. Available in PDF, EPUB and Kindle. Book excerpt: