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Pretreatment Of Lignocellulosic Biomass Using Room Temperature Ionic Liquids Rtils
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Book Synopsis Pretreatment of Lignocellulosic Biomass Using Room Temperature Ionic Liquids (RTILs) by : Thomas Vincent Doherty
Download or read book Pretreatment of Lignocellulosic Biomass Using Room Temperature Ionic Liquids (RTILs) written by Thomas Vincent Doherty and published by . This book was released on 2010 with total page 270 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Pretreatment of Lignocellulosic Biomass with Acetic Acid, Salts, and Ionic Liquids by : Joan Goerss Lynam
Download or read book Pretreatment of Lignocellulosic Biomass with Acetic Acid, Salts, and Ionic Liquids written by Joan Goerss Lynam and published by . This book was released on 2011 with total page 264 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Bioenergy Research: Advances and Applications by : Vijai G. Gupta
Download or read book Bioenergy Research: Advances and Applications written by Vijai G. Gupta and published by Newnes. This book was released on 2013-12-05 with total page 513 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bioenergy Research: Advances and Applications brings biology and engineering together to address the challenges of future energy needs. The book consolidates the most recent research on current technologies, concepts, and commercial developments in various types of widely used biofuels and integrated biorefineries, across the disciplines of biochemistry, biotechnology, phytology, and microbiology. All the chapters in the book are derived from international scientific experts in their respective research areas. They provide you with clear and concise information on both standard and more recent bioenergy production methods, including hydrolysis and microbial fermentation. Chapters are also designed to facilitate early stage researchers, and enables you to easily grasp the concepts, methodologies and application of bioenergy technologies. Each chapter in the book describes the merits and drawbacks of each technology as well as its usefulness. The book provides information on recent approaches to graduates, post-graduates, researchers and practitioners studying and working in field of the bioenergy. It is an invaluable information resource on biomass-based biofuels for fundamental and applied research, catering to researchers in the areas of bio-hydrogen, bioethanol, bio-methane and biorefineries, and the use of microbial processes in the conversion of biomass into biofuels. Reviews all existing and promising technologies for production of advanced biofuels in addition to bioenergy policies and research funding Cutting-edge research concepts for biofuels production using biological and biochemical routes, including microbial fuel cells Includes production methods and conversion processes for all types of biofuels, including bioethanol and biohydrogen, and outlines the pros and cons of each
Book Synopsis Biochemical Saccharification of Ionic Liquid Pretreated Biomass by : Christopher James Barr
Download or read book Biochemical Saccharification of Ionic Liquid Pretreated Biomass written by Christopher James Barr and published by . This book was released on 2013 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: The goal of this dissertation research is to gain a deeper understanding of two major processes in the conversion of lignocellulosic biomass to monomeric sugars. These two core processes are the ionic liquid (IL) pretreatment step as well as biochemical (enzymatic) conversion of polysaccharides to monomeric sugars. Cellulose, one of the three primary components of lignocellulosic biomass, is recalcitrant to enzymatic deconstruction due, in part, to a predominantly crystalline structure. Enzymatic access to cellulose is restricted by hemicellulose and lignin. Pretreatment of lignocellulose by ionic liquids can result in a change in the cellulose structure as well as removal or redistribution of the hemicellulose and lignin. These changes result in a regenerated substrate that is more easily hydrolyzed compared to native substrates. Changes in cellulose structure as well as compositional changes within lignocellulosic biomass were examined as a response to changes in the IL incubation temperature. Maxima in 24 hour hydrolysis of glucan to glucose appears to be substrate dependent with maxima at incubation temperatures: 120°C for poplar, 110°C for switchgrass, and 100°C for corn stover. At these temperatures, native cellulose I was converted to a primarily amorphous substrate where the residual crystalline cellulose exhibits predominantly cellulose II features. This optimal incubation temperature occurred before dramatic xylan losses to the IL wash. In a substrate with minimal lignin and xylan (newspaper), a maximum in enzyme digestibility was seen at a considerably lower (60°C) pretreatment temperature. Differences in polysaccharide structure of IL pretreated poplar and switchgrass can impact hydrolysis of these polysaccharides to monomeric sugars and the formulation of the enzyme mixture needed for complete hydrolysis. These differences predicated studies with mono-component enzymes to determine critical enzyme activities and interactions. Endoglucanase, cellobiohydrolase, ß-glucosidase, endoxylanase, and ß-xylosidase were shown to be critical during hydrolysis for both poplar and switchgrass. Initial studies showed differences between poplar and switchgrass. Beneficial accessory enzymes necessary for hydrolysis of poplar were ferulic acid esterase and exopolygalacturonase while switchgrass required a-L-arabinofuranosidase and ferulic acid esterase. Further studies on switchgrass varying ß-glucosidase activity showed only a-L-arabinofuranosidase was necessary only for hydrolysis of IL pretreated switchgrass. Commercially available enzyme mixtures used for the digestion of lignocellulosic biomass contain many different types of enzymes. The composition of these enzyme mixtures are relatively unknown and are traditionally characterized by the amount of sugar released from the hydrolysis of filter paper in one hour (filter paper unit, FPU). This characterization does not quantitate the xylanolytic component within the mixture, especially accessory hemicellulases whose necessity may vary between substrates. Supplementation of the commercial mixture, Cellic CTec2, with a-L-arabinofuranosidase improved switchgrass xylose yields by 75% and resulted in complete conversion of switchgrass xylan at lower enzyme loadings than previous studies.
Book Synopsis Aspects Critical to Advancing Ionic Liquid Pretreatment Technique as a Viable Approach for Lignocellulosic Biomass Conversion by : Thehazhnan K. Ponnaiyan
Download or read book Aspects Critical to Advancing Ionic Liquid Pretreatment Technique as a Viable Approach for Lignocellulosic Biomass Conversion written by Thehazhnan K. Ponnaiyan and published by . This book was released on 2016 with total page 173 pages. Available in PDF, EPUB and Kindle. Book excerpt: Declining nonrenewable petroleum resources combined with political and environmental concerns over fossil fuels have necessitated the search for alternate energy sources. Plant (lignocellulosic) biomass, which includes the fibrous, woody, and generally inedible portion of plant matter, is an abundant, inexpensive, and sustainable source of organic carbon that can be processed to produce fuel ethanol and a variety of other chemicals. The biological conversion of cellulosic biomass to ethanol could offer high yields at low costs, but only if more improvement is seen in technology for releasing simple sugars from recalcitrant biomass. Lignocellulosic biomass is composed of three major components- cellulose, hemicellulose, and lignin. The cellulose and hemicellulose portions when hydrolyzed into glucose and pentose sugars, can be fermented to produce fuel. The pretreatment of biomass is a crucial step, and in recent years, ionic liquids (ILs) have been gaining recognition as environmentally benign solvents for biomass pretreatment, owing to their favorable properties. Although a promising route, IL pretreatment still harbors several critical aspects that require further investigation, and the goal of this dissertation is to address these concerns. A key aspect that influences the economic viability of the ionic liquid pretreatment technique is the recovery and reuse of ILs. The extent of recovery of the IL under investigation, 1-ethyl-3-methylimidazolium acetate (EMIM-Ac), is investigated and the results are presented in chapter 3. It is shown that the ionic liquid does not irreversibly adsorb onto the biomass and can be recovered in the displacement solvent (water is used as antisolvent for separating ionic liquid from the biomass after pretreatment) at different biomass loadings. Nearly complete recovery of IL in wash solutions is achieved and no appreciable loss in its effectiveness for subsequent pretreatment is observed for over 9 recycle stages. However, the water from the IL-water wash mix needs to be separated from the IL to facilitate its continued efficiency for further pretreatment. From a techno-economic point of view, when such separations are employed on an industrial scale, the energy aspects involved in the recovery of ionic liquids become important. A better understanding of the driving force for separation between the ionic liquid and the antisolvent requires the availability of vapor liquid equilibrium (VLE) for the binary mixture.This provides the motivation to develop a novel and rapid method for the generation of (VLE) data using thermogravimetric analysis, and the results are discussed in chapter 4. VLE data over almost the entire composition range of EMIMAc-water mixtures at five different temperatures (60.0, 70.0, 80.0, 90.0 and 100.0 °C) is generated. This method may be extended to other hydrophilic IL-water systems or to IL-ethanol binary mixtures as well. In the instance when ethanol is used as the antisolvent during the pretreatment step, again, it is necessary to separate the ethanol from the IL by suitable means before the IL can be reused. In light of this, it is of interest to quantify the amount of ethanol remaining in the IL, if any, after the separation. This motive led to the development of a simple and rapid method for the determination of residual ethanol content in hydrophilic ILs, and the results are presented in chapter 5. The method utilizes headspace solid-phase microextraction coupled with gas chromatography to quantify ethanol in ILs. In an integrated biorefinery, another key aspect that can reinforce economic viability is the complete utilization of all components of the biomass, including the lignin portion, to produce value added products. Lignin, given its interesting functionalities and properties owing to its complex aromatic nature, has ample potential to be converted in a wide array of value-added products ranging from adhesives and surfactants to flame retardant material and aromatic acids. Since the IL pretreatment technique is relatively new, the kind of lignin resulting from such a pretreatment needs to be better understood as it is important to assess its usability for further processing. This motive resulted in the characterization of lignin produced from IL pretreated biomass, as discussed in chapter 6. Techniques employed include Scanning Electron Microscopy (SEM), Elemental Analysis, Elemental CHN (Carbon Hydrogen Nitrogen) analysis, Nuclear Magnetic Resonance Spectroscopy (13NMR), Thermo-gravimetric Analysis (TGA), and MatrixAssisted Laser Desorption/Ionization Mass Spectroscopy (MALDI-MS). A better understanding of these key aspects mentioned above will help facilitate further advancement of the IL pretreatment technique as a viable approach for lignocellulosic biomass conversion.
Book Synopsis Deep Eutectic Solvents for Pretreatment of Lignocellulosic Biomass by : Pratima Bajpai
Download or read book Deep Eutectic Solvents for Pretreatment of Lignocellulosic Biomass written by Pratima Bajpai and published by Springer Nature. This book was released on 2021-08-20 with total page 98 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on the properties of deep eutectic solvents (DESs) and recent advances in their application in lignocellulosic biomass processing. Lignocellulosic biomass conversion to biofuels, biochemicals and other value-added products has attracted global attention because it is a readily available, inexpensive and renewable resource. However, in order for biomass technologies to be commercially viable, biomass recalcitrance needs to be cost-effectively reduced. Deep eutectic solvents (DESs) are new ‘green' solvents that have the high potential for biomass processing thanks to their low cost, low toxicity, biodegradability, and easy recycling and reuse. After an overview of the current lignocellulosic biomass pretreatment, the book discusses the synthesis and physiochemical properties of DESs, as well as key findings on the effects of DES on cellulose, hemicellulose and lignin solubilization, biomass pretreatment and biomass crystallinity. It then addresses the enzymatic hydrolysis performance of DES-pretreated solids, compatibility of DESs with enzymes and microorganisms, and the recycling potential of DESs. Lastly, it compares DESs with ionic liquids, and examines the challenges and opportunities relating to extending the use of DESs in lignocellulosic processing.
Book Synopsis From Biomass to Advanced Bio-Based Chemicals & Materials: A Multidisciplinary Perspective by : Gabriel Paës
Download or read book From Biomass to Advanced Bio-Based Chemicals & Materials: A Multidisciplinary Perspective written by Gabriel Paës and published by Frontiers Media SA. This book was released on 2020-04-01 with total page 210 pages. Available in PDF, EPUB and Kindle. Book excerpt: Lignocellulose is the only renewable carbon source that can help replace oil-based chemicals and materials, in the process fighting global warming. However, because of its chemical and structural complexity, lignocellulose transformation into advanced products requires a better understanding of its composition and of its architecture at different scales, as well as a combination of physical, biological, and chemical processes, in order to render this transformation efficient and economically competitive. Tremendous efforts continue to be made toward the production of ethanol as a biofuel from various lignocellulosic feedstocks. Furthermore, recent successes have been achieved in extracting fibers to prepare composite materials that can compete with plastic fabrics. Importantly, lignocellulose chemistry can bring to the market original and complex chemicals that can lead to new applications, in particular when exploiting aromatic molecules or oligosaccharides from lignocellulose to produce solvents, surfactants, plasticizers, functional additives for food/feed/cosmetics, drugs, monomers, and polymers. In addition to this broad range of molecular products, fibers and particles fractionated from the lignocellulosic biomass are increasingly used to elaborate bio-based composite materials.
Book Synopsis Exploring Pretreatment with Ionic Liquids for Enzymatic Cellulose Hydrolysis by : Philip Wolfram Engel
Download or read book Exploring Pretreatment with Ionic Liquids for Enzymatic Cellulose Hydrolysis written by Philip Wolfram Engel and published by . This book was released on 2012 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Green Chemistry for Sustainable Biofuel Production by : Veera Gnaneswar Gude
Download or read book Green Chemistry for Sustainable Biofuel Production written by Veera Gnaneswar Gude and published by CRC Press. This book was released on 2018-05-24 with total page 592 pages. Available in PDF, EPUB and Kindle. Book excerpt: Renewable fuel research and process development requires interdisciplinary approaches involving chemists and physicists from both scientific and engineering backgrounds. Here is an important volume that emphasizes green chemistry and green engineering principles for sustainable process development from an interdisciplinary point of view. It creates an enriching knowledge base on green chemistry of biofuel production, sustainable process development, and green engineering principles for renewable fuel production. This book includes chapters contributed by both research scientists and research engineers with significant experience in biofuel chemistry and processes. The book offers an abundance of scientific experimental methods and analytical procedures and interpretation of the results that capture the state-of-the-art knowledge in this field. The wide range of topics make this book a valuable resource for academicians, researchers, industrial practitioners and scientists, and engineers in various renewable energy fields. Key features: • Emphasizes green chemistry and green engineering principles for sustainable process development for biofuel production • Discusses a wide array of biofuels from algal biomass to waste-to-energy technologies and wastewater treatment and activated sludge processes • Presents advances and developments in biofuel green chemistry and green engineering, including process intensification (microwaves/ultrasound), ionic liquids, and green catalysis • Looks at environmental assessment and economic impact of biofuel production
Book Synopsis Enzymatic Hydrolysis of Ionic Liquid-pretreated Lignocellulose by : Kierston Ellen Shill
Download or read book Enzymatic Hydrolysis of Ionic Liquid-pretreated Lignocellulose written by Kierston Ellen Shill and published by . This book was released on 2013 with total page 91 pages. Available in PDF, EPUB and Kindle. Book excerpt: Cellulose is the most abundant organic compound on Earth, and is found in lignocellulosic biomass. In order to access this carbon source for biofuel production, a process must be developed that breaks down the natural barriers the plant has in place to protect itself from degradation. The natural breakdown of biomass by organisms involves a variety of enzymes that work together to make the carbon source available. Cellulose can be hydrolyzed in an acid-catalyzed process by cellulase enzymes to form glucose. The enzymatic hydrolysis of cellulose relies on the initial adsorption of cellulases to the solid lignocellulose surface, and thus the reaction can be limited by surface area. Additionally, hemicellulose and lignin combine to act as barriers to adsorption, both physically and through competitive binding that inactivates the enzymes. Cellulose crystallinity also inhibits enzymatic degradation by limiting surface area and decreasing the rate of enzymatic hydrolysis. All of these factors make enzymatic hydrolysis of cellulose slow for untreated biomass, and make pretreatment a necessary step for biofuel production. Several pretreatment methods have been developed to make biomass more amenable to enzymatic hydrolysis. A promising approach is biomass dissolution in ionic liquids (ILs) followed by the addition of an anti-solvent to precipitate the cellulosic fraction of the biomass prior to hydrolysis. A cellulase mixture can then quickly and efficiently hydrolyze the precipitated biomass. The enzymatic hydrolysis by a cellulase cocktail of Miscanthus x giganteus, a lignocellulosic biomass, pretreated with the IL 1-ethyl,3-methylimidazolium acetate ([Emim][OAc]) was studied. The IL pretreatment time and temperature parameters have been studied, and a kinetic model was developed to optimize the pretreatment conditions for improved cellulose and hemicellulose enzymatic conversion. This kinetic model indicated a wide range of optimal pretreatment conditions, from high temperatures / short times to lower temperatures / long times. Variables obtained from the kinetic model are within reported ranges of experimentally obtained values for other pretreatments, indicating that the model may be broadly applicable to a variety of lignocellulosic pretreatment processes. Since ionic liquid pretreatment provides a readily-hydrolysable substrate, other factors, such as enzyme loading, product inhibition, and solids loading, become important. For industrially-relevant processes, the enzymatic hydrolysis must produce and tolerate high levels of glucose. We have investigated the effects of glucose concentration on the enzymatic hydrolysis of Avicel, [Emim][OAc]-pretreated Avicel, and [Emim][OAc]-pretreated Miscanthus. Both cellobiose and glucose production were monitored over time, and cellobiose was found to be present at appreciable concentrations when high levels of glucose were present. This effect is more pronounced with [Emim][OAc]-pretreated substrates. A competitive inhibition model was fit to the hydrolysis data and found to fit moderately well. However, this model was unable to capture both the fast initial glucose production and prolonged cellobiose presence, highlighting the need for a more mechanistic kinetic model. By studying the enzymatic hydrolysis of pretreated lignocellulose, we will be able to better understand and direct the engineering of substrates, enzymes, and processes for more effective hydrolysis under industrially relevant conditions.
Book Synopsis Ionic Liquids by : Alexander Kokorin
Download or read book Ionic Liquids written by Alexander Kokorin and published by BoD – Books on Demand. This book was released on 2011-02-21 with total page 690 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is the second in the series of publications in this field by this publisher, and contains a number of latest research developments on ionic liquids (ILs). This promising new area has received a lot of attention during the last 20 years. Readers will find 30 chapters collected in 6 sections on recent applications of ILs in polymer sciences, material chemistry, catalysis, nanotechnology, biotechnology and electrochemical applications. The authors of each chapter are scientists and technologists from different countries with strong expertise in their respective fields. You will be able to perceive a trend analysis and examine recent developments in different areas of ILs chemistry and technologies. The book should help in systematization of knowledges in ILs science, creation of new approaches in this field and further promotion of ILs technologies for the future.
Book Synopsis Natural Polyphenols from Wood by : Kun Cheng
Download or read book Natural Polyphenols from Wood written by Kun Cheng and published by Elsevier. This book was released on 2021-03-24 with total page 340 pages. Available in PDF, EPUB and Kindle. Book excerpt: Natural Polyphenols from Wood: Tannin and Lignin – An Industrial Perspective is a detailed guide to the sourcing and processing of tannin and lignin for valuable advanced applications across areas such as fuels, chemicals, drugs, and food. Drawing on the latest academic research and patent literature, this book provides strong practical understanding of the use of these valuable materials in novel industrial applications. This book introduces natural polyphenols from wood and the fundamental aspects of carbon management within the tree. In-depth presentation of extraction and characterization methods is followed by an extensive coverage of practical and industrial applications of wood polyphenols. This is an essential resource for researchers and advanced students working with lignin or tannin, and across biopolymer science, biomass, wood chemistry, paper, wood adhesives, polymer materials, renewable resources, and biotechnology. It also supports industrial R&D and scientists working with wood polyphenols or bio-based polymers. This book re-evaluates wood polyphenols from an industrial perspective, revealing the latest techniques and drawing on patent literature. It addresses fundamental issues of wood polyphenols, such as carbon cycle, wood fractionation, structure, and properties. It offers a comprehensive review of practical applications, including lignin depolymerization, wood reconstruction, fuels, chemicals, drugs, and food.
Book Synopsis Fungi and Lignocellulosic Biomass by : Christian P. Kubicek
Download or read book Fungi and Lignocellulosic Biomass written by Christian P. Kubicek and published by John Wiley & Sons. This book was released on 2012-07-09 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: Harnessing fungi’s enzymatic ability to break down lignocellulolytic biomass to produce ethanol more efficiently and cost-effectively has become a significant research and industrial interest. Fungi and Lignocellulosic Biomass provides readers with a broad range of information on the uses and untapped potential of fungi in the production of bio-based fuels. With information on the molecular biological and genomic aspects of fungal degradation of plant cell walls to the industrial production and application of key fungal enzymes, chapters in the book cover topics such as enzymology of cellulose, hemicelluloses, and lignin degradation. Edited by a leading researcher in the field, Fungi and Lignocellulosic Biomass will be a valuable tool in advancing the development and production of biofuels and a comprehensive resource for fungal biologists, enzymologists, protein chemists, biofuels chemical engineers, and other research and industry professionals in the field of biomass research.
Book Synopsis The Oxford Handbook of Food Fermentations by : Charles W. Bamforth
Download or read book The Oxford Handbook of Food Fermentations written by Charles W. Bamforth and published by Oxford University Press. This book was released on 2014-07-17 with total page 864 pages. Available in PDF, EPUB and Kindle. Book excerpt: Fermentation, as a chemical and biological process, is everywhere. Countless societies throughout history have used it to form a vast array of foods and drinks, many of which were integral and essential to those cultures; it could be argued that the production of beer and bread formed the basis of many agriculture-based civilizations. Today, nearly every person on the planet consumes fermented products, from beer and wine, to bread and dairy products, to certain types of meat and fish. Fermentation is a nearly ubiquitous process in today's food science, and an aspect of chemistry truly worth understanding more fully. In The Oxford Handbook of Food Fermentations, Charles W. Bamforth and Robert E. Ward have collected and edited contributions from many of the world's experts on food fermentation, each focused on a different fermentation product. The volume contains authoritative accounts on fermented beverages, distilled beverages, and a diverse set of foods, as well as chapters on relevant biotechnology. Each chapter embraces the nature of the product, its production, and its final composition. The text also touches on the raw materials and processes involved in producing packaged foodstuff, and the likely future trends in each area. In the conclusion, Bamforth and Ward present a comparison between the various products and the diverse technologies employed to produce them. Fermentation is a multifaceted process that affects a wide variety of products we consume, and The Oxford Handbook of Food Fermentations is the definitive resource that captures the science behind fermentation, as well as its diverse applications.
Book Synopsis Green Chemistry by : Vinod K. Tiwari
Download or read book Green Chemistry written by Vinod K. Tiwari and published by Springer Nature. This book was released on 2022-09-02 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book summarizes fundamentals and advanced topics of green chemistry and highlights the importance and impact of green chemistry over traditional synthetic methods. It discusses about the importance and scope of the catalytic protocols in green chemistry and their application in daily life. Alternate green energy approaches discussed in this book underline the importance of efficiency enhancement with simultaneous energy demand reduction by replacing the dependence on non-renewable energy resources. Various topics covered in this book include green solvents, energy-efficient approach for organic synthesis, catalysis, biocatalysis, and green approach in pharmaceutically important molecules and drugs. The book will be a valuable reference for beginners, researchers, and professionals interested in sustainable green chemistry and their scope in allied fields.
Download or read book Ionic Liquids written by Scott Handy and published by BoD – Books on Demand. This book was released on 2015-05-21 with total page 694 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ionic liquids continue to attract a great deal of research attention in an even increasing number of areas, including more traditional areas such as synthesis (organic and materials) and physical properties studies and predictions, as well as less obvious areas such as lubrication and enzymatic transformations. In this volume, recent advances in a number of these different areas are reported and reviewed, thus granting some appreciation for the future that ionic liquids research holds, and affording inspiration for those who have not previously considered the application of ionic liquids in their area of interest.
Book Synopsis A Novel Ionic Liquid Pretreatment of Lignocellulosic Biomass for Production of Ethanol by : Anantharam P. Dadi
Download or read book A Novel Ionic Liquid Pretreatment of Lignocellulosic Biomass for Production of Ethanol written by Anantharam P. Dadi and published by . This book was released on 2008 with total page 402 pages. Available in PDF, EPUB and Kindle. Book excerpt:
