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Practical Nmr Spectroscopy Laboratory Guide Using Bruker Spectrometers
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Book Synopsis Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers by : John S. Harwood
Download or read book Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers written by John S. Harwood and published by Academic Press. This book was released on 2015-10-28 with total page 137 pages. Available in PDF, EPUB and Kindle. Book excerpt: Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge's High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009). - Written by experts in solution-state NMR spectroscopy - Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer - Includes detailed appendices and sample questions for lab reports
Book Synopsis 50 and More Essential NMR Experiments by : Matthias Findeisen
Download or read book 50 and More Essential NMR Experiments written by Matthias Findeisen and published by John Wiley & Sons. This book was released on 2013-07-30 with total page 322 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.
Book Synopsis NMR-Spectroscopy: Data Acquisition by : Christian Schorn
Download or read book NMR-Spectroscopy: Data Acquisition written by Christian Schorn and published by John Wiley & Sons. This book was released on 2004-09-03 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume enables the newcomer to become familiar with the basic data acquisition procedures, modular pulse sequence units and complete sequences in NMR spectroscopy.
Book Synopsis Essential Practical NMR for Organic Chemistry by : S. A. Richards
Download or read book Essential Practical NMR for Organic Chemistry written by S. A. Richards and published by John Wiley & Sons. This book was released on 2023-05-01 with total page 293 pages. Available in PDF, EPUB and Kindle. Book excerpt: A hands-on resource advocating an ordered approach to gathering and interpreting NMR data The second edition of Essential Practical NMR for Organic Chemistry delivers a pragmatic and accessible text demonstrating an ordered approach to gathering and interpreting NMR data. In this informal guide, you’ll learn to make sense of the high density of NMR information through the authors’ problem-solving strategies and interpretations. The book also discusses critical aspects of NMR theory, as well as data acquisition and processing strategy. It explains the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation and includes a brand-new chapter on Nitrogen-15 NMR. Readers will also find: Strategies for preparing a sample, spectrum acquisition, processing, and interpreting your spectrum Fulsome discussions of Carbon-13 NMR spectroscopy Practical treatments of quantification, safety procedures, and relevant software An ideal handbook for anyone involved in using NMR to solve structural problems, this latest edition of Essential Practical NMR for Organic Chemistry will be particularly useful for chemists running and looking at their own NMR spectra, as well as those who work in small molecule NMR. It will also earn a place in the libraries of undergraduate and post-graduate organic chemistry students.
Book Synopsis Handbook of Spectroscopy by : Tuan Vo-Dinh
Download or read book Handbook of Spectroscopy written by Tuan Vo-Dinh and published by Wiley-VCH. This book was released on 2003-10-17 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: Research scientists, analytical scientists, industrial engineers, astronomers, and others who utilize the ever-increasing power of spectroscopic methods need an accessible, authoritative guidance on how best to apply current available techniques to their particular fields of interest and to their specific applications. Based on a survey of spectroscopists in universities, research, and industry, this is the first handbook to fulfill their needs. (Midwest).
Book Synopsis NMR Spectroscopy Explained by : Neil E. Jacobsen
Download or read book NMR Spectroscopy Explained written by Neil E. Jacobsen and published by John Wiley & Sons. This book was released on 2007-09-10 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.
Download or read book Hands on NMR written by William S. Price and published by . This book was released on 2021-05-17 with total page 500 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presenting important practical aspects of NMR spectroscopy, this book will be useful for explaining and facilitating the successful set up of a wide variety of NMR experiments. It will enlighten readers with the relevant information on the basic concepts in NMR, how it works, and how to trouble-shoot artefacts that may be encountered. A short introductory chapter on some basic theory and key concepts will precede chapters on more practical aspects e.g. instrumentation, sample preparation, experimentation and data processing. Several practical case experiments covering various fields and including details on the pitfalls, tips and recommendations are presented next. Lastly, detailed chapters on other important practical aspects such as artefacts, spectral prediction, databases and safety are included. Bringing books that present practical NMR up to date, this book fills a gap in the literature and provides a new comprehensive practical NMR book for teaching and research at all levels - graduates, postgraduates, industry and research.
Book Synopsis Practical NMR Spectroscopy by : Maryvonne L. Martin
Download or read book Practical NMR Spectroscopy written by Maryvonne L. Martin and published by . This book was released on 1980 with total page 460 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis NMR-Spectroscopy: Data Acquisition by : Christian Schorn
Download or read book NMR-Spectroscopy: Data Acquisition written by Christian Schorn and published by John Wiley & Sons. This book was released on 2001 with total page 376 pages. Available in PDF, EPUB and Kindle. Book excerpt: The key to correct structure analysis. This volume of the successful "Spectroscopic Techniques" series familiarizes newcomers with the basic data acquisition procedures, modular pulse sequence units and complete sequences in NMR spectroscopy. It applies the numerous possibilities of Bruker's simulation program NMR-SIM to provide a guided introduction to the world of pulse sequences. The effectiveness of particular NMR experiments is demonstrated by the section "Check Its" and that of data processing by the accompanying CD-ROM with the Bruker processing software 1D and 2D WIN-NMR. This interactive approach to simulate spectra based on a reduced spin system and the processing of the accomplished NMR raw data is closely related to everyday work at the spectrometer. In this way, the author encourages beginners to use high resolution NMR, and also experts on NMR spectroscopy to evaluate new experiments using the easy-manageable simulation program.
Book Synopsis NMR — From Spectra to Structures by : Terence N. Mitchell
Download or read book NMR — From Spectra to Structures written by Terence N. Mitchell and published by Springer Science & Business Media. This book was released on 2013-04-17 with total page 144 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy is one of the most important analytical methods available today. This practice-oriented textbook shows how NMR spectra is used in the education of organic structures. The emphasis is on practical rather than on theoretical aspects, which are treated only briefly. NMR- From Spectra to Strucures is a textbook providing an ideal practical guide to today ́s standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only the 1D NMR spectra (proton, carbon, DEPT/APT) but, for the first time in a textbook, also the most important 2D spectra (H,H and C,H correlation).
Book Synopsis Practical NMR Spectroscopy by : Maryvonne L. Martin
Download or read book Practical NMR Spectroscopy written by Maryvonne L. Martin and published by . This book was released on 1980 with total page 460 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Laboratory Guide to Proton NMR Spectroscopy by : S. A. Richards
Download or read book Laboratory Guide to Proton NMR Spectroscopy written by S. A. Richards and published by Wiley-Blackwell. This book was released on 1988-01-01 with total page 229 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis NMR Spectroscopy Techniques, Second Edition, by : Martha Bruch
Download or read book NMR Spectroscopy Techniques, Second Edition, written by Martha Bruch and published by CRC Press. This book was released on 1996-03-05 with total page 634 pages. Available in PDF, EPUB and Kindle. Book excerpt: This work elucidates the power of modern nuclear magnetic resonance (NMR) techniques to solve a wide range of practical problems that arise in both academic and industrial settings. This edition provides current information regarding the implementation and interpretation of NMR experiments, and contains material on: three- and four-dimensional NMR; the NMR analysis of peptides, proteins, carbohydrates and oligonucleotides; and more.
Download or read book NMR and Chemistry written by J.W. Akitt and published by CRC Press. This book was released on 2017-12-21 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt: Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.
Book Synopsis NMR-Spectroscopy: Processing Strategies by : Peter Bigler
Download or read book NMR-Spectroscopy: Processing Strategies written by Peter Bigler and published by Wiley-VCH. This book was released on 1997-05-15 with total page 280 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Entrance to Practical NMR Spectroscopy This interactive tutorial is designed to introduce newcomers to the crucial and central step of NMR data processing. It enables and encourages you to process measured data according to your own special needs and ideas, rather than having to rely on automatic processing or specialist help. You are shown how to transform NMR data into 1D or 2D spectra in easy steps. Various processing strategies are explained, the necessary theoretical background presented, and practical hints, examples, exercises and problems are all included. The accompanying CD-ROM provides a comprehensive NMR data base and powerful software tools, based on WIN-NMR software designed by Bruker, which enable you to make best use of your NMR data. It is the interactive approach of using text, software and the appropriate sets of data that makes this a unique book on NMR spectroscopy.
Book Synopsis NMR Spectroscopy in Drug Development and Analysis by : Ulrike Holzgrabe
Download or read book NMR Spectroscopy in Drug Development and Analysis written by Ulrike Holzgrabe and published by John Wiley & Sons. This book was released on 2008-07-11 with total page 312 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the development of the NMR spectrometer in the 1950s, NMR spectra have been widely used for the elucidation of the 2D structure of newly synthesized and natural compounds. In the 1980s, the high-resolution NMR spectrometer (> 300 Mhz) and 2D experiments were introduced, which opens up the possibility to determine the 3D structure of large molecules, especially biomolecules. However, NMR spectroscopy has been rarely applied to drug analysis. This book illustrates the power and versatility of NMR spectroscopy in the determination of impurities in and the content of drugs, the composition of polymer excipients, the characterization of isomeric drug mixtures, the complexity of drugs with small-size components or ions, and the behavior of drugs in acid and basic solution. In addition, NMR spectroscopy and especially the hyphenated technique with HPLC is shown to be a powerful tool to measure a drug and its metabolites in various body fluids. The solid state NMR technique can give information on the structure, especially the conformation of drugs and excipients in drug formulations. Recently, SAR by NMR, introduced by Fesik, impressively demonstrated the potential of NMR spectroscopy in drug development and in the characterization of the interaction between large molecules and ligands. The complexation between proteins, lipids and cyclodextrins with drugs is described. Finally, NMR imaging (MRI and MRS) can be used to characterize the liberation of drugs from a drug formulation. Furthermore, the distribution of substances in plants, in animals, in tissues and in humans can be visualized by imaging. In short, this book covers all aspects of drug analysis.
Book Synopsis Fundamentals of Protein NMR Spectroscopy by : Gordon S. Rule
Download or read book Fundamentals of Protein NMR Spectroscopy written by Gordon S. Rule and published by Springer Science & Business Media. This book was released on 2005-10-28 with total page 543 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy has proven to be a powerful technique to study the structure and dynamics of biological macromolecules. Fundamentals of Protein NMR Spectroscopy is a comprehensive textbook that guides the reader from a basic understanding of the phenomenological properties of magnetic resonance to the application and interpretation of modern multi-dimensional NMR experiments on 15N/13C-labeled proteins. Beginning with elementary quantum mechanics, a set of practical rules is presented and used to describe many commonly employed multi-dimensional, multi-nuclear NMR pulse sequences. A modular analysis of NMR pulse sequence building blocks also provides a basis for understanding and developing novel pulse programs. This text not only covers topics from chemical shift assignment to protein structure refinement, as well as the analysis of protein dynamics and chemical kinetics, but also provides a practical guide to many aspects of modern spectrometer hardware, sample preparation, experimental set-up, and data processing. End of chapter exercises are included to emphasize important concepts. Fundamentals of Protein NMR Spectroscopy not only offer students a systematic, in-depth, understanding of modern NMR spectroscopy and its application to biomolecular systems, but will also be a useful reference for the experienced investigator.
