New Concepts and Techniques for Quantification and Trace Analysis by Gas Chromatography

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Publisher :
ISBN 13 : 9789172838277
Total Pages : 77 pages
Book Rating : 4.8/5 (382 download)

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Book Synopsis New Concepts and Techniques for Quantification and Trace Analysis by Gas Chromatography by : Johan Pettersson

Download or read book New Concepts and Techniques for Quantification and Trace Analysis by Gas Chromatography written by Johan Pettersson and published by . This book was released on 2004 with total page 77 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Advances in Gas Chromatography

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Publisher : BoD – Books on Demand
ISBN 13 : 9535112279
Total Pages : 226 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Advances in Gas Chromatography by : Xinghua Guo

Download or read book Advances in Gas Chromatography written by Xinghua Guo and published by BoD – Books on Demand. This book was released on 2014-02-26 with total page 226 pages. Available in PDF, EPUB and Kindle. Book excerpt: For decades gas chromatography has been and will remain an irreplaceable analytical technique in many research areas for both quantitative analysis and qualitative characterization/identification, which is still supplementary with HPLC. This book highlights a few areas where significant advances have been reported recently and/or a revisit of basic concepts is deserved. It provides an overview of instrumental developments, frontline and modern research as well as practical industrial applications. The topics include GC-based metabolomics in biomedical, plant and microbial research, natural products as well as characterization of aging of synthetic materials and industrial monitoring, which are contributions of several experts from different disciplines. It also contains best hand-on practices of sample preparation (derivatization) and data processing in daily research. This book is recommended to both basic and experienced researchers in gas chromatography.

Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control

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Publisher : Elsevier
ISBN 13 : 0080858473
Total Pages : 811 pages
Book Rating : 4.0/5 (88 download)

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Book Synopsis Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control by : G. Guiochon

Download or read book Quantitative Gas Chromatography for Laboratory Analyses and On-Line Process Control written by G. Guiochon and published by Elsevier. This book was released on 1988-06-01 with total page 811 pages. Available in PDF, EPUB and Kindle. Book excerpt: Here is an invaluable new book on quantitative gas chromatography which explains how the method can - or should - be used for accurate and precise analysis. Gas chromatography is firmly established as one of the few major methods for the quantitative analysis of complex mixtures. It is fast, accurate and inexpensive, with a broad range of applications. It has however become very complex and involved: over 200 stationary phases, more than 10 detector principles and several very different column types are available from among the catalogs of over 100 manufacturers and major retailers. The progressive changes in the nature of gas chromatography have created new needs for information which are not satisfied by the literature presently available.This book provides a complete discussion of all the problems involved in the achievement of quantitative analysis by gas chromatography, whether in the research laboratory, in the routine analysis laboratory or in process control. For this reason the presentation of theoretical concepts has been limited to the essential, while extensive explanations have been devoted to the various steps involved in the derivation of precise and accurate data. This starts with the selection of the instrumentation and column, continues with the choice of optimum experimental conditions, then calibration and ends with the use of correct procedures for data acquisition and calculations. Finally, there is almost always a way to reduce errors and an entire chapter deals with this single issue. Numerous relevant examples are presented.The first part of the book presents the theoretical background, simple enough to be understood by all analytical chemists, but still complete and up-to-date. It discusses the problems of flow dynamics, retention and band broadening. The changes in band profile associated with column overloading are explained without much recourse to mathematics. The second part describes the gas chromatograph and discusses the properties of each of its parts: gas flow and pressure controller sampling system, oven, column switching valves, detectors. The different implementations, their advantages and drawbacks are discussed and compared. In addition, three chapters present packed column technology, open tubular column technology and some sophisticated new phase systems, respectively. The new phase systems described use adsorbents, modified by coating or grafting organic phase, and carrier gases containing vapors which are sorbed by the stationary phase and modify it, such as steam. The third part discusses the applications in qualitative and quantitative analysis. Calibration, peak integration, sources of errors arising from the various parts of the instrument as well as from the measurement process itself are carefully described in four detailed chapters. Methods to carry out accurate and precise analysis are presented. A last chapter is devoted to process control analysis and gives a number of detailed examples of applications. A lexicon explaining the most important chromatographic terms and a detailed index complete the book.This is a book which no chemical analyst should be without. It should be on the library shelf of all universities, instrument companies and any laboratory and plant where gas chromatography is used.

Analytical Quality Assurance for Trace Organics Analysis by Gas Chromatography/mass Spectrometry

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Publisher :
ISBN 13 :
Total Pages : 26 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Analytical Quality Assurance for Trace Organics Analysis by Gas Chromatography/mass Spectrometry by : James W. Eichelberger

Download or read book Analytical Quality Assurance for Trace Organics Analysis by Gas Chromatography/mass Spectrometry written by James W. Eichelberger and published by . This book was released on 1975 with total page 26 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Modern Practice of Gas Chromatography

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Publisher : John Wiley & Sons
ISBN 13 : 047165115X
Total Pages : 1059 pages
Book Rating : 4.4/5 (716 download)

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Book Synopsis Modern Practice of Gas Chromatography by : Robert L. Grob, PhD

Download or read book Modern Practice of Gas Chromatography written by Robert L. Grob, PhD and published by John Wiley & Sons. This book was released on 2004-08-04 with total page 1059 pages. Available in PDF, EPUB and Kindle. Book excerpt: The bible of gas chromatography-offering everything the professional and the novice need to know about running, maintaining, and interpreting the results from GC Analytical chemists, technicians, and scientists in allied disciplines have come to regard Modern Practice of Gas Chomatography as the standard reference in gas chromatography. In addition to serving as an invaluable reference for the experienced practitioner, this bestselling work provides the beginner with a solid understanding of gas chromatographic theory and basic techniques. This new Fourth Edition incorporates the most recent developments in the field, including entirely new chapters on gas chromatography/mass spectrometry (GC/MS); optimization of separations and computer assistance; high speed or fast gas chromatography; mobile phase requirements: gas system requirements and sample preparation techniques; qualitative and quantitative analysis by GC; updated information on detectors; validation and QA/QC of chromatographic methods; and useful hints for good gas chromatography. As in previous editions, contributing authors have been chosen for their expertise and active participation in their respective areas. Modern Practice of Gas Chromatography, Fourth Edition presents a well-rounded and comprehensive overview of the current state of this important technology, providing a practical reference that will greatly appeal to both experienced chomatographers and novices.

Comprehensive Two Dimensional Gas Chromatography

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Publisher : Elsevier Science
ISBN 13 : 9780444532374
Total Pages : 328 pages
Book Rating : 4.5/5 (323 download)

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Book Synopsis Comprehensive Two Dimensional Gas Chromatography by : Lourdes Ramos

Download or read book Comprehensive Two Dimensional Gas Chromatography written by Lourdes Ramos and published by Elsevier Science. This book was released on 2009-09-09 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book reviews the basic concepts and highlights the most relevant advances and developments that have taken place in the field of comprehensive two dimensional gas chromatography (GC x GC) since its introduction in 1991. The several instrumental and technical approaches assayed and developed during these seventeen years and that have contributed to the development of this powerful separation technique and to its increasing application in many areas is explained and comprehensively illustrated through a number of chapters devoted these specific topics. More specialized aspects of the technique, including theoretical aspects, modelization of the chromatographic process, software developments, and alternative couplings is also covered. Finally, special attention is paid to data treatment, for both qualitative and quantitative analysis. This book will be a practical resource that will explain from basic to specialized concepts of GC x GC and will show the current state-of-the-art and discuss future trends of this technique. Outlines basic concepts and principles of GCxGC technique for non-specialists to apply the technique to their research Provides detailed descriptions of recent technical advances and serves as an instructional guide in latest applications in GCxGC Sets the scene for possible future development and alternative new applications of technique

Qualitative and Quantitative Aspects of Trace Analysis by Capillary Gas Chromatography

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Publisher :
ISBN 13 :
Total Pages : 183 pages
Book Rating : 4.:/5 (248 download)

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Book Synopsis Qualitative and Quantitative Aspects of Trace Analysis by Capillary Gas Chromatography by : Joseph Matias Peter Marie Curvers

Download or read book Qualitative and Quantitative Aspects of Trace Analysis by Capillary Gas Chromatography written by Joseph Matias Peter Marie Curvers and published by . This book was released on 1985 with total page 183 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Practical Gas Chromatography

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Publisher : Springer
ISBN 13 : 3642546404
Total Pages : 904 pages
Book Rating : 4.6/5 (425 download)

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Book Synopsis Practical Gas Chromatography by : Katja Dettmer-Wilde

Download or read book Practical Gas Chromatography written by Katja Dettmer-Wilde and published by Springer. This book was released on 2014-11-05 with total page 904 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Quantitative Chromatographic Analysis

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Publisher : CRC Press
ISBN 13 : 9780203910788
Total Pages : 398 pages
Book Rating : 4.9/5 (17 download)

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Book Synopsis Quantitative Chromatographic Analysis by : Thomas Beesley

Download or read book Quantitative Chromatographic Analysis written by Thomas Beesley and published by CRC Press. This book was released on 2000-12-06 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt: Highlights critical factors involved in successful chromatographic analysis. Details analytical procedures; outlining sample preparation, collection, transportation, and storage. Provides step-by-step guidelines for producing analytical reports.

Quantification in LC and GC

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Publisher : John Wiley & Sons
ISBN 13 : 3527323015
Total Pages : 377 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Quantification in LC and GC by : Stavros Kromidas

Download or read book Quantification in LC and GC written by Stavros Kromidas and published by John Wiley & Sons. This book was released on 2009-10-12 with total page 377 pages. Available in PDF, EPUB and Kindle. Book excerpt: Closing a gap in the current literature by addressing the evaluation and quality assessment of raw data, this practice-oriented guide is clearly divided into three parts. The first describes basic considerations of chromatographic data quality, common errors and potential pitfalls in reading out and quantifying the data. Part two systematically covers the most important chromatographic methods as well as the specific requirements for obtaining good chromatographic data. The final part looks at data quality from the perspective of those regulatory authorities demanding certain standards in data quality, describing in detail best practices. Written with the practitioner in mind, the text not only teaches the mathematical basics but also provides invaluable advice.

Gas Chromatography

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Publisher : BoD – Books on Demand
ISBN 13 : 1838818650
Total Pages : 144 pages
Book Rating : 4.8/5 (388 download)

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Book Synopsis Gas Chromatography by : Peter Kusch

Download or read book Gas Chromatography written by Peter Kusch and published by BoD – Books on Demand. This book was released on 2019-09-04 with total page 144 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography (GC) is one of the most important types of chromatography used in analytical chemistry for separating and analyzing chemical organic compounds. Today, gas chromatography is one of the most widespread investigation methods of instrumental analysis. This technique is used in the laboratories of chemical, petrochemical, and pharmaceutical industries, in research institutes, and also in clinical, environmental, and food and beverage analysis. This book is the outcome of contributions by experts in the field of gas chromatography and includes a short history of gas chromatography, an overview of derivatization methods and sample preparation techniques, a comprehensive study on pyrazole mass spectrometric fragmentation, and a GC/MS/MS method for the determination and quantification of pesticide residues in grape samples.

The Analysis of Gases by Chromatography

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Publisher : Elsevier
ISBN 13 : 1483285634
Total Pages : 160 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis The Analysis of Gases by Chromatography by : C. J. Cowper

Download or read book The Analysis of Gases by Chromatography written by C. J. Cowper and published by Elsevier. This book was released on 2013-10-22 with total page 160 pages. Available in PDF, EPUB and Kindle. Book excerpt: Intended to enable trained scientists to equip themselves to successfully perform analyses of complex gas mixtures. The equipment and the considerations governing the choice of carrier gas are described in detail. Selection of methods for use on complex mixtures often involves the choice of more than one column; the separating capabilities of column packing and how they can be used in combinations are described and numerous examples are given. The handling of samples prior to separation and the calculation of results after separation, including calibration, are described. Throughout, special emphasis is given to the differences between gas analysis and the better documented liquid analysis.

Basic Gas Chromatography

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Publisher : Wiley-Interscience
ISBN 13 :
Total Pages : 232 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Basic Gas Chromatography by : Harold Monroe McNair

Download or read book Basic Gas Chromatography written by Harold Monroe McNair and published by Wiley-Interscience. This book was released on 1998 with total page 232 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gets you Quickly up to Speed on the Principles and Practice of Modern Gas Chromatography Gas Chromatography (GC) is undoubtedly the most widely used technique for the separation and analysis of volatile compounds. Yet comprehensive guides to contemporary GC theory and practice are surprisingly hard to find. Basic Gas Chromatography fills this significant void in the GC literature. Written by two well-known practitioners and educators in GC, it offers thorough coverage of the basic principles and techniques of modern gas chromatography. Designed to serve as a primer/working reference for bench chemists and as a textbook for upper-level undergraduate and graduate students, it presents the fundamentals in a straightforward and logical fashion. Theoretical issues are explained without complicated equations and derivations and always in terms of how they relate to practical operating principles. Timely, comprehensive, and accessible, Basic Gas Chromatography: * Provides a balanced presentation of theory and practice * Includes both capillary column and packed column chromatography * Uses the new IUPAC terms throughout, cross-referenced to traditional terms and symbols * Offers a wealth of helpful hints, step-by-step guidelines, and trouble - shooting tips * Briefly covers GC-MS, headspace analysis, chiral analysis, solid phase microextraction, and other cutting-edge topics

Gas Chromatography and Mass Spectrometry: A Practical Guide

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Publisher : Academic Press
ISBN 13 : 0080920152
Total Pages : 633 pages
Book Rating : 4.0/5 (89 download)

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Book Synopsis Gas Chromatography and Mass Spectrometry: A Practical Guide by : O. David Sparkman

Download or read book Gas Chromatography and Mass Spectrometry: A Practical Guide written by O. David Sparkman and published by Academic Press. This book was released on 2011-05-17 with total page 633 pages. Available in PDF, EPUB and Kindle. Book excerpt: The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensible resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on chromatographic peak deconvolution has been added along with a more in-depth understanding of the use of mass spectral databases in the identification of unknowns. Since the last edition, a number of advances in GC inlet systems and sample introduction techniques have occurred, and they are included in the new edition. Other updates include a discussion on fast GC and options for combining GC detectors with mass spectrometry. The section regarding GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types has the same number of compound types as the original edition, but the information in each section has been expanded to not only explain some of the spectra but to also explain why certain fragmentations take place. The number of Appendices has been increased from 12 to 17. The Appendix on Atomic Masses and Isotope Abundances has been expanded to provide tools to aid in determination of elemental composition from isotope peak intensity ratios. An appendix with examples on "Steps to follow in the determination of elemental compositions based on isotope peak intensities" has been added. Appendices on whether to use GC/MS or LC/MS, third-party software for use in data analysis, list of information required in reporting GC/MS data, X+1 and X+2 peak relative intensities based on the number of atoms of carbon in an ion, and list of available EI mass spectral databases have been added. Others such as the ones on derivatization, isotope peak patterns for ions with Cl and/or Br, terms used in GC and in mass spectrometry, and tips on setting up, maintaining and troubleshooting a GC/MS system have all been expanded and updated. Covers the practical instruction necessary for successful operation of GC/MS equipment Reviews the latest advances in instrumentation, ionization methods, and quantitation Includes troubleshooting techniques and a variety of additional information useful for the GC/MS practitioner A true benchtop reference A guide to a basic understanding of the components of a Gas Chromatograph-Mass Spectrometer (GC-MS) Quick References to data interpretation Ready source for information on new analyses

Trace Analysis by Capillary Gas Chromatography

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Publisher :
ISBN 13 :
Total Pages : 194 pages
Book Rating : 4.:/5 (312 download)

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Book Synopsis Trace Analysis by Capillary Gas Chromatography by : Theodorus Henricus Maria Noij

Download or read book Trace Analysis by Capillary Gas Chromatography written by Theodorus Henricus Maria Noij and published by . This book was released on 1988 with total page 194 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Advanced Gas Chromatography

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Publisher : BoD – Books on Demand
ISBN 13 : 9535102982
Total Pages : 474 pages
Book Rating : 4.5/5 (351 download)

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Book Synopsis Advanced Gas Chromatography by : Mustafa Ali Mohd

Download or read book Advanced Gas Chromatography written by Mustafa Ali Mohd and published by BoD – Books on Demand. This book was released on 2012-03-21 with total page 474 pages. Available in PDF, EPUB and Kindle. Book excerpt: Progress in agricultural, biomedical and industrial applications' is a compilation of recent advances and developments in gas chromatography and its applications. The chapters cover various aspects of applications ranging from basic biological, biomedical applications to industrial applications. Book chapters analyze new developments in chromatographic columns, microextraction techniques, derivatisation techniques and pyrolysis techniques. The book also includes several aspects of basic chromatography techniques and is suitable for both young and advanced chromatographers. It includes some new developments in chromatography such as multidimensional chromatography, inverse chromatography and some discussions on two-dimensional chromatography. The topics covered include analysis of volatiles, toxicants, indoor air, petroleum hydrocarbons, organometallic compounds and natural products. The chapters were written by experts from various fields and clearly assisted by simple diagrams and tables. This book is highly recommended for chemists as well as non-chemists working in gas chromatography.

Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues

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Publisher : Elsevier
ISBN 13 : 0080454402
Total Pages : 509 pages
Book Rating : 4.0/5 (84 download)

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Book Synopsis Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues by : A.R. Fernandez Alba

Download or read book Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues written by A.R. Fernandez Alba and published by Elsevier. This book was released on 2004-12-11 with total page 509 pages. Available in PDF, EPUB and Kindle. Book excerpt: The trace determination of pesticides continues to be a topic for analytical chemists working in research centres, government and universities. With four chapters devoted to chromatography-mass spectrometry methods, readers are able to understand the analytical basis, technical characteristics and possibilities to evaluate pesticides in food by gas chromatography (GC) and liquid chromatography (LC) mass spectrometry. The book also provides a well-defined and critical compilation of the sample treatment and clean-up procedures, as well as injection techniques applied in GC and LC food analysis. Finally the book deals with aspects related to analytical quality control requirements for pesticide residues, in addition to pesticide regulation aspects. * Contains specific chapters devoted to chromatography-mass spectrometry methods* Provides a well-defined and critical compilation of the sample treatment and clean-up procedures* Contains aspects related to analytical quality control requirements for pesticide residues