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Multidimensional Nmr In Liquids
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Book Synopsis Multidimensional NMR in Liquids by : Frank J. M. van de Ven
Download or read book Multidimensional NMR in Liquids written by Frank J. M. van de Ven and published by Wiley-VCH. This book was released on 1995 with total page 432 pages. Available in PDF, EPUB and Kindle. Book excerpt: Multidimensional NMR in Liquids offers a lucid treatment of basic NMR phenomena, building up to today's most sophisticated NMR experiments from first principles. Using easy-to-grasp product-operator formalism, diagrams, and practical examples, one-, two-, and N-dimensional NMR experiments are explained with minimal recourse to quantum mechanics.
Book Synopsis Multidimensional NMR Methods for the Solution State by : Gareth A. Morris
Download or read book Multidimensional NMR Methods for the Solution State written by Gareth A. Morris and published by John Wiley & Sons. This book was released on 2012-12-19 with total page 877 pages. Available in PDF, EPUB and Kindle. Book excerpt: The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established scientist with a solid foundation for the understanding of multidimensional NMR, a representative if inevitably limited survey of its applications, an authoritative account of classic techniques such as COSY, NOESY and TOSCY, and an account of the latest progress in the development of multidimensional techniques. This handbook is structured in four parts. The first opens with an historical introduction to, and a brief account of, the practicalities and applications of multidimensional NMR methods, followed by a definitive survey of their conceptual basis and a series of articles setting out the generic principles of methods for acquiring and processing multidimensional NMR data. In the second part, the main families of multidimensional techniques, arranged in approximate order of increasing complexity, are described in detail, from simple J-resolved spectroscopy through to the powerful heteronuclear 3D and 4D methods that now dominate the study of structural biology in solution. The third part offers and illustrative selection from the very wide range of applications of multidimensional NMR methods, including some of the most recent developments in protein NMR. Finally, the fourth part introduces the idea of multidimensional spectra containing non-frequency dimensions, in which properties such as diffusion and relaxation are correlated. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here
Book Synopsis Scaling in One and Two Dimensional NMR Spectroscopy in Liquids by : R. V. Hosur
Download or read book Scaling in One and Two Dimensional NMR Spectroscopy in Liquids written by R. V. Hosur and published by . This book was released on 1990 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Multidimensional Solid-State NMR and Polymers by : Klaus Schmidt-Rohr
Download or read book Multidimensional Solid-State NMR and Polymers written by Klaus Schmidt-Rohr and published by Elsevier. This book was released on 2012-12-02 with total page 501 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR spectroscopy is the most valuable and versatile analytical tool in chemistry. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better understanding of materials properties on the molecular level.Dramatic progress-much of it pioneered by the authors-has been achieved in this area, especially in synthetic polymers. Solid-state NMR now favorably competes with well-established techniques, such as light, x-ray, or neutron scattering, electron microscopy, and dielectric and mechanical relaxation.The application of multidimensional solid-state NMR inevitably involves use of concepts from different fields of science. This book also provides the first comprehensive treatment of both the new experimental techniques and the theoretical concepts needed in more complex data analysis. The text addresses spectroscopists and polymer scientists by treating the subject on different levels; descriptive, technical, and mathematical approaches are used when appropriate. It presents an overview of new developments with numerous experimental examples and illustrations, which will appeal to readers interested in both the information content as well as the potential of solid-state NMR. The book also contains many previously unpublished details that will be appreciated by those who want to perform the experiments. The techniques described are applicable not only to the study of synthetic polymers but to numerous problems in solid-state physics, chemistry, materials science, and biophysics. - Presents original theories and new perspectives on scattering techniques - Provides a systematic treatment of the whole subject - Gives readers access to previously unpublished material - Includes extensive illustrations
Book Synopsis Multidimensional NMR Studies on the Structure, Dynamics, and Function of the Human Oncoprotein MDM2 and the Human Melanoma Inhibitory Activity (MIA) Protein by : Raphael Stoll
Download or read book Multidimensional NMR Studies on the Structure, Dynamics, and Function of the Human Oncoprotein MDM2 and the Human Melanoma Inhibitory Activity (MIA) Protein written by Raphael Stoll and published by Herbert Utz Verlag. This book was released on 2000 with total page 130 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Nuclear Magnetic Resonance Spectroscopy by : Joseph B. Lambert
Download or read book Nuclear Magnetic Resonance Spectroscopy written by Joseph B. Lambert and published by John Wiley & Sons. This book was released on 2019-01-04 with total page 485 pages. Available in PDF, EPUB and Kindle. Book excerpt: Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
Book Synopsis Multinuclear and Multidimensional NMR Methodology for Studying Individual Water Molecules Bound to Peptides and Proteins in Solution by : Ioannis P. Gerothanassis
Download or read book Multinuclear and Multidimensional NMR Methodology for Studying Individual Water Molecules Bound to Peptides and Proteins in Solution written by Ioannis P. Gerothanassis and published by . This book was released on 1994 with total page 67 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book NMR of Polymers written by Frank A. Bovey and published by Academic Press. This book was released on 1996-11-19 with total page 471 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR has made important contributions to our understanding of structure–property relationships in polymers. This book provides an up-to-date and comprehensive overview of the fundamentals of NMR, with applications of multidimensional NMR and the new solution and solid-state methods in polymer science. NMR of Polymers is written by leading authorities for graduate students and professionals in academia and industry. Provides comprehensive overview of NMR in Polymer Science Covers multidimensional NMR Includes new solution and solid state methods Addresses chain conformation and dynamics
Book Synopsis Understanding NMR Spectroscopy by : James Keeler
Download or read book Understanding NMR Spectroscopy written by James Keeler and published by John Wiley & Sons. This book was released on 2011-09-19 with total page 533 pages. Available in PDF, EPUB and Kindle. Book excerpt: This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually ‘work’. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal with the emphasis on obtaining a good understanding of how the experiments actually work. The use of two-colour printing and a new larger format improves the readability of the text. In addition, a number of new topics have been introduced: How product operators can be extended to describe experiments in AX2 and AX3 spin systems, thus making it possible to discuss the important APT, INEPT and DEPT experiments often used in carbon-13 NMR. Spin system analysis i.e. how shifts and couplings can be extracted from strongly-coupled (second-order) spectra. How the presence of chemically equivalent spins leads to spectral features which are somewhat unusual and possibly misleading, even at high magnetic fields. A discussion of chemical exchange effects has been introduced in order to help with the explanation of transverse relaxation. The double-quantum spectroscopy of a three-spin system is now considered in more detail. Reviews of the First Edition “For anyone wishing to know what really goes on in their NMR experiments, I would highly recommend this book” – Chemistry World “...I warmly recommend for budding NMR spectroscopists, or others who wish to deepen their understanding of elementary NMR theory or theoretical tools” – Magnetic Resonance in Chemistry
Book Synopsis Fast 2D Solution-state NMR by : Dr Jean-Nicolas Dumez
Download or read book Fast 2D Solution-state NMR written by Dr Jean-Nicolas Dumez and published by Royal Society of Chemistry. This book was released on 2023-05-17 with total page 560 pages. Available in PDF, EPUB and Kindle. Book excerpt: Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.
Book Synopsis NMR Spectroscopy and its Application to Biomedical Research by : S.K. Sarkar
Download or read book NMR Spectroscopy and its Application to Biomedical Research written by S.K. Sarkar and published by Elsevier. This book was released on 1996-12-04 with total page 407 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR has become the most diverse spectroscopic tool available to date in biomedical research. It is now routinely used to study biomolecular structure and dynamics particularly as a result of recent developments of a cascade of highly sophisticated multidimensional NMR pulse sequences, and of advances in genetic engineering to produce biomolecules, uniformly or selectively enriched with 13C, 15N and 2H.Features of this book:• Provides an up-to-date treatment of NMR techniques and their application to problems of biomedical interest• Most refined multidimensional pulse sequences including the basic aspects are covered by leading NMR spectroscopists.The book will be useful to NMR spectroscopists, biochemists, and to molecular biologists interested in the use of NMR techniques for solving biological problems.
Book Synopsis Two Dimensional NMR of Liquids and Oriented Molecules by : Miriam Gochin
Download or read book Two Dimensional NMR of Liquids and Oriented Molecules written by Miriam Gochin and published by . This book was released on 1987 with total page 554 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Relaxation Matrix Analysis of 2D NMR Data by : R. V. Hosur
Download or read book Relaxation Matrix Analysis of 2D NMR Data written by R. V. Hosur and published by . This book was released on 1990 with total page 100 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Basic One- and Two-dimensional NMR Spectroscopy by : Horst Friebolin
Download or read book Basic One- and Two-dimensional NMR Spectroscopy written by Horst Friebolin and published by . This book was released on 1993 with total page 402 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis NMR of Ordered Liquids by : Elliott Burnell
Download or read book NMR of Ordered Liquids written by Elliott Burnell and published by Springer Science & Business Media. This book was released on 2003-07-31 with total page 494 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR of Ordered Liquids gives a unique overview of the scope and limitations of the NMR of oriented liquids, based on contributions from acknowledged experts in the field. The book consists of four sections: -detailed general introduction which covers the basic principles and sophisticated experimental techniques; -wide variety of applications ranging from NMR studies of small atoms and molecules in anisotropic liquids to the utilization of residual dipolar couplings for structure determination of biological molecules; -summary of the sophisticated theoretical treatments, computer simulations, and phenomenological models for anisotropic intermolecular interactions that are widely used in the analysis of experimental results; -overview of the dynamical aspects and relaxation processes relevant for orientationally ordered molecules.
Book Synopsis Multidimensional NMR Studies of the Polymers by : Silapong Baiagern
Download or read book Multidimensional NMR Studies of the Polymers written by Silapong Baiagern and published by . This book was released on 2008 with total page 144 pages. Available in PDF, EPUB and Kindle. Book excerpt: "The purpose of this work was to apply multinuclear and multidimensional nuclear magnetic resonance (NMR) spectroscopy techniques to determine the characteristics of the structure and intermolecular interactions of dendrimers supramolecular assemblies, polyalkylsilane oligomer and Nafion® fluoropolymer. In the one of the studies, a mixture of alkylpolysilane oligomers was characterized by one-dimensional (1D) and two-dimensional (2D) NMR spectroscopy. The oligomeric products were observed to have chains of up to 5-6 silicons. Complete unambiguous resonance assignments were obtained with the help of 1D 1H, 13C, 29Si and 2D 1H{29Si}gHSQC/gHSQC-TOCSY/gHMBC experiments. Finally, the discovery of the quarternary Si atoms by using HMBC technique provides evidence for branching in the structures. In a separate study, multidimensional NMR spectroscopy was used to analyze the supramolecular chemistry of poly(propylene imine) dendrimers that have urea-adamantane as end groups with numerous acidic guest molecules. Data about the close proximity of the host and guest molecules was determined by two-dimensional (2D) nuclear Overhauser enhancement spectroscopy (NOESY). These interactions support a specific binding model for the formation of a stable host-guest complex. Diffusion studies concerning a ratio of host and guest molecule helped to support the data collected. Finally, the Nafion® fluoropolymer, used for proton exchange membranes, was investigated using regional or band selective excitation to perform selective nD NMR experiments. The microstructure of the Nafion® prepolymer with the sulfonyl fluoride functional group was characterized by homonuclear band-selective 19F-19F COSY. When compared with signals in a standard COSY spectrum, the cross-peaks in the selective homonuclear 19F-19F COSY give more intense and cleaner signals. To further simplify the complex cross-peak patterns, a q3 and Gaussian 180° inversion pulse was introduced to remove fluorine homonuclear coupling during the t1 evolution time."--Abstract.
Book Synopsis Multinuclear and Multidimensional NMR Methodology for Studying Individual Water Molecules Bound to Peptides and Proteins in Solution by : I. P. Gerothanassis
Download or read book Multinuclear and Multidimensional NMR Methodology for Studying Individual Water Molecules Bound to Peptides and Proteins in Solution written by I. P. Gerothanassis and published by . This book was released on 1994 with total page 122 pages. Available in PDF, EPUB and Kindle. Book excerpt:
