Modern Techniques In High Resolution Ft Nmr

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Modern Techniques in High-Resolution FT-NMR

Author : Narayanan Chandrakumar
Publisher : Springer Science & Business Media
ISBN 13 : 1461246261
Total Pages : 396 pages
Book Rating : 4.4/5 (612 download)

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Book Synopsis Modern Techniques in High-Resolution FT-NMR by : Narayanan Chandrakumar

Download or read book Modern Techniques in High-Resolution FT-NMR written by Narayanan Chandrakumar and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 396 pages. Available in PDF, EPUB and Kindle. Book excerpt: The magnetism of nuclear spin systems has proved an amazingly fertile ground for the creativity of researchers. This happy circumstance results from the triple benediction that nature appears to have bestowed on nuclear spins: they are sporting spies-being infinitely manipulable (one is even tempted to say malleable), not unduly coy in revealing their secrets, and having a whole treasure house of secrets to reveal in the first place. researcher with Since spin dynamics are now orchestrated by the NMR ever more subtle scores, it is important to be able to tune into the pro ceedings with precision, if one is to make sense of it at all. Fortunately, it is not terribly difficult to do so, since in many ways spin dynamics are the theoretician's dream come true: they are often finite dimensional and quite tractable with basic quantum mechanics, frequently allowing near exact treatments and readily testable predictions. This book was conceived two years ago, with the objective of providing a simple, consistent introduction to the description of the spin dynamics that one encounters in modern NMR experiments. We believed it was a good time to attempt this, since it was possible by then to give sufficiently general descriptions of powelful classes of new NMR experiments. The choice of experiments we discuss in detail is necessarily subjective, al though we hope to have given a flavor of most of the important classes of pulse sequences, including some surface coil imaging applications.

Modern Techniques in High-Resolution FT-NMR

Author : Narayanan Chandrakumar
Publisher :
ISBN 13 : 9781461246275
Total Pages : 400 pages
Book Rating : 4.2/5 (462 download)

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Book Synopsis Modern Techniques in High-Resolution FT-NMR by : Narayanan Chandrakumar

Download or read book Modern Techniques in High-Resolution FT-NMR written by Narayanan Chandrakumar and published by . This book was released on 1986-11-01 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt:

High Resolution NMR

Author : Edwin D. Becker
Publisher : Elsevier
ISBN 13 : 9780080508061
Total Pages : 424 pages
Book Rating : 4.5/5 (8 download)

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Book Synopsis High Resolution NMR by : Edwin D. Becker

Download or read book High Resolution NMR written by Edwin D. Becker and published by Elsevier. This book was released on 1999-10-08 with total page 424 pages. Available in PDF, EPUB and Kindle. Book excerpt: High Resolution NMR provides a broad treatment of the principles and theory of nuclear magnetic resonance (NMR) as it is used in the chemical sciences. It is written at an "intermediate" level, with mathematics used to augment, rather than replace, clear verbal descriptions of the phenomena. The book is intended to allow a graduate student, advanced undergraduate, or researcher to understand NMR at a fundamental level, and to see illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins. Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. Careful attention is given to developing and interrelating four approaches - steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The presentation is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. Likewise, no previous background in NMR is assumed, since the book begins with a description of the basic physics, together with a brief account of the historical development of the field. This third edition of High Resolution NMR preserves the "conversational" approach of the previous editions that has been well accepted as a teaching tool. However, more than half the material is new, and the remainder has been revised extensively. Problems are included to reinforce concepts in the book. Uses mathematics to augment, not replace, verbal explanations Written in a clear and conversational style Follows the successful format and approach of two previous editions Revised and updated extensively--about 70 percent of the text is new Includes problems and references to additional reading at the end of each chapter

NMR in Biological Systems

Author : K.V.R. Chary
Publisher : Springer Science & Business Media
ISBN 13 : 1402066791
Total Pages : 551 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis NMR in Biological Systems by : K.V.R. Chary

Download or read book NMR in Biological Systems written by K.V.R. Chary and published by Springer Science & Business Media. This book was released on 2008-04-08 with total page 551 pages. Available in PDF, EPUB and Kindle. Book excerpt: During teaching NMR to students and researchers, we felt the need for a text-book which can cover modern trends in the application of NMR to biological systems. This book covers the entire area of NMR in Biological Sciences (Biomolecules, cells and tissues, animals, plants and drug design). As well as being useful to researchers, this is an excellent book for teaching a course on NMR in Biological Systems.

High-Resolution NMR Techniques in Organic Chemistry

Author : Timothy D.W. Claridge
Publisher : Newnes
ISBN 13 : 0080546285
Total Pages : 400 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis High-Resolution NMR Techniques in Organic Chemistry by : Timothy D.W. Claridge

Download or read book High-Resolution NMR Techniques in Organic Chemistry written by Timothy D.W. Claridge and published by Newnes. This book was released on 2009 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Nuclear Magnetic Resonance (NMR) Spectroscopy remains the foremost analytical technique for the structure elucidation of organic molecules and an indispensable tool for the synthetic, medicinal and natural product chemist. New techniques continue to emerge and the application of NMR methods continues to expand. High-Resolution NMR Techniques in Organic Chemistry is designed for use in academic and industrial NMR facilities, as a text for graduate-level NMR courses, and as an accessible reference for the chemist's or spectroscopist's desk."--BOOK JACKET.

Structure Elucidation by Modern NMR

Author : Helmut Duddeck
Publisher : Springer Science & Business Media
ISBN 13 : 3642977871
Total Pages : 273 pages
Book Rating : 4.6/5 (429 download)

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Book Synopsis Structure Elucidation by Modern NMR by : Helmut Duddeck

Download or read book Structure Elucidation by Modern NMR written by Helmut Duddeck and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 273 pages. Available in PDF, EPUB and Kindle. Book excerpt: For several years, we have been organizing seminars and workshops on the application of modem one and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry. In 1987, we wrote a workbook (StrukturaufkUirung mit modemer NMR-Spektroskopie, Steinkopff, Darmstadt, FRG, 1988) in German language based on our experience in these courses. Many of the exercises described therein have been used in such courses and some of them have been shaped by the participants to a great extent. The response of readers and discussions with colleagues from many countries encouraged us two years later to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in English version. Now, after the rapid development of basic multipulse NMR me thods in the early 1980s, the avantgarde in modem NMR is concentrating on the invention and optimi zation of advanced techniques, e. g. , three-dimensional experiments. For the beginners, however, the situation has not changed markedly since the appearence of the first edition of this book. Therefore, we decided not to add new techniques to this second edition, but rather to increase the number of exerci ses from 23 to 33, the new ones being basically single-spectrum-problems.

Pulse and Fourier Transform NMR

Author : Thomas C. Farrar
Publisher : Elsevier
ISBN 13 : 0080918123
Total Pages : 118 pages
Book Rating : 4.0/5 (89 download)

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Book Synopsis Pulse and Fourier Transform NMR by : Thomas C. Farrar

Download or read book Pulse and Fourier Transform NMR written by Thomas C. Farrar and published by Elsevier. This book was released on 2012-12-02 with total page 118 pages. Available in PDF, EPUB and Kindle. Book excerpt: Pulse and Fourier Transform NMR: Introduction to Theory and Methods presents the different types of pulse experiments that are commonly used and provides the theoretical background necessary for understanding these techniques. This book evaluates the practical application of pulse methods and the necessary instrumentation. Organized into seven chapters, this book begins with an overview of the NMR fundamentals and the basic pulse methods. This text then summarizes the important features of pulse spectrometers. Other chapters consider the rationale, the advantages, and the limitations of Fourier transform NMR methods. This book discusses as well how the idea of the rotating frame can be utilized to understand certain experiments that extend the range of application of pulse methods. The final chapter deals with a few significant special uses of pulse techniques. This book is a valuable resource for chemists and readers who are familiar with high resolution NMR but with no background in pulse methods.

Perspectives in Modern Chemical Spectroscopy

Author : David L. Andrews
Publisher : Springer Science & Business Media
ISBN 13 : 3642754562
Total Pages : 333 pages
Book Rating : 4.6/5 (427 download)

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Book Synopsis Perspectives in Modern Chemical Spectroscopy by : David L. Andrews

Download or read book Perspectives in Modern Chemical Spectroscopy written by David L. Andrews and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 333 pages. Available in PDF, EPUB and Kindle. Book excerpt: "An interesting and enlightening book well worth the time for someone who is grounded in the basics of spectroscopy, yet interested in newer techniques and applications... particularly useful in providing breadth for those whose work has caused them to narrow their appreciation of spectroscopy to one area." (Spectroscopy) "This book should be on the bookshelves of all chemists whose daily work involves the practical application of spectroscopy to chemical analysis." (Fresenius' J. of Analytical Chem.) "...stands in style between an introduction to the various topics covered and near monographic treatments...meets a real need." (Faraday Transactions) "It covers an enormous amount of spectral theory and methodology in a condensed and readable format." (SIM News)

Pulsed Magnetic Resonance

Author : A. Abragam
Publisher : Oxford University Press
ISBN 13 : 9780198539629
Total Pages : 586 pages
Book Rating : 4.5/5 (396 download)

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Book Synopsis Pulsed Magnetic Resonance by : A. Abragam

Download or read book Pulsed Magnetic Resonance written by A. Abragam and published by Oxford University Press. This book was released on 1992 with total page 586 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a tribute to E.L. Hahn, an outstanding physicist whose discovery of spin echoes and demonstration of nuclear free induction decay led to the most important methods of modern nuclear magnetic resonance. The wide impact of these methods in physics, chemistry, biology, and medicine is fully acknowledged. In addition, Hahn's fundamental contributions in nuclear quadrupole echo phenomena, level crossing techniques, self-induced transparency and laser physics have been of paramount importance. Reflecting the diversity of these key discoveries and their vital influence, the articles presented here offer a stimulating and challenging contribution to the scientific literature which will be read by students and research workers from the wide range of disciplines using NMR techniques.

Polymorphism in Pharmaceutical Solids

Author : Harry G. Brittain
Publisher : CRC Press
ISBN 13 : 1420073222
Total Pages : 656 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Polymorphism in Pharmaceutical Solids by : Harry G. Brittain

Download or read book Polymorphism in Pharmaceutical Solids written by Harry G. Brittain and published by CRC Press. This book was released on 2018-11-12 with total page 656 pages. Available in PDF, EPUB and Kindle. Book excerpt: Using clear and practical examples, Polymorphism of Pharmaceutical Solids, Second Edition presents a comprehensive examination of polymorphic behavior in pharmaceutical development that is ideal for pharmaceutical development scientists and graduate students in pharmaceutical science. This edition focuses on pharmaceutical aspects of polymorphism a

Multidimensional NMR Methods for the Solution State

Author : Gareth A. Morris
Publisher : John Wiley & Sons
ISBN 13 : 1118589084
Total Pages : 877 pages
Book Rating : 4.1/5 (185 download)

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Book Synopsis Multidimensional NMR Methods for the Solution State by : Gareth A. Morris

Download or read book Multidimensional NMR Methods for the Solution State written by Gareth A. Morris and published by John Wiley & Sons. This book was released on 2012-12-19 with total page 877 pages. Available in PDF, EPUB and Kindle. Book excerpt: The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established scientist with a solid foundation for the understanding of multidimensional NMR, a representative if inevitably limited survey of its applications, an authoritative account of classic techniques such as COSY, NOESY and TOSCY, and an account of the latest progress in the development of multidimensional techniques. This handbook is structured in four parts. The first opens with an historical introduction to, and a brief account of, the practicalities and applications of multidimensional NMR methods, followed by a definitive survey of their conceptual basis and a series of articles setting out the generic principles of methods for acquiring and processing multidimensional NMR data. In the second part, the main families of multidimensional techniques, arranged in approximate order of increasing complexity, are described in detail, from simple J-resolved spectroscopy through to the powerful heteronuclear 3D and 4D methods that now dominate the study of structural biology in solution. The third part offers and illustrative selection from the very wide range of applications of multidimensional NMR methods, including some of the most recent developments in protein NMR. Finally, the fourth part introduces the idea of multidimensional spectra containing non-frequency dimensions, in which properties such as diffusion and relaxation are correlated. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here

High-resolution NMR Techniques in Organic Chemistry

Author : T. Claridge
Publisher : Elsevier
ISBN 13 : 9780080427980
Total Pages : 414 pages
Book Rating : 4.4/5 (279 download)

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Book Synopsis High-resolution NMR Techniques in Organic Chemistry by : T. Claridge

Download or read book High-resolution NMR Techniques in Organic Chemistry written by T. Claridge and published by Elsevier. This book was released on 1999-12-24 with total page 414 pages. Available in PDF, EPUB and Kindle. Book excerpt: From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.

Spectroscopic Methods in Mineralogy

Author : A. Beran
Publisher : The Mineralogical Society of Great Britain and Ireland
ISBN 13 : 9634636624
Total Pages : 676 pages
Book Rating : 4.6/5 (346 download)

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Book Synopsis Spectroscopic Methods in Mineralogy by : A. Beran

Download or read book Spectroscopic Methods in Mineralogy written by A. Beran and published by The Mineralogical Society of Great Britain and Ireland. This book was released on 2004 with total page 676 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Pharmacognosy

Author : Simone Badal McCreath
Publisher : Elsevier
ISBN 13 : 0443186588
Total Pages : 847 pages
Book Rating : 4.4/5 (431 download)

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Book Synopsis Pharmacognosy by : Simone Badal McCreath

Download or read book Pharmacognosy written by Simone Badal McCreath and published by Elsevier. This book was released on 2023-10-13 with total page 847 pages. Available in PDF, EPUB and Kindle. Book excerpt: Pharmacognosy: Fundamentals, Applications and Strategies, Second Edition represents a comprehensive compilation of the philosophical, scientific and technological aspects of contemporary pharmacognosy. The book examines the impact of the advanced techniques of pharmacognosy on improving the quality, safety and effectiveness of traditional medicines, and how pharmacokinetics and pharmacodynamics have a crucial role to play in discerning the relationships of active metabolites to bioavailability and function at the active sites, as well as the metabolism of plant constituents. Structured in seven parts, the book covers the foundational aspects of Pharmacognosy, the chemistry of plant metabolites, their effects, other sources of metabolites, crude drugs from animals, basic animal anatomy and physiology, technological applications and biotechnology, and the current trends in research. New to this edition is a chapter on plant metabolites and SARS-Cov-2, extensive updates on existing chapters and the development of a Laboratory Guide to support instructors execute practical activities on the laboratory setting. Covers the main sources of natural bioactive substances Contains practice questions and laboratory exercises at the end of every chapter to test learning and retention Describes how pharmacokinetics and pharmacodynamics play a crucial role in discerning the relationships of active metabolites to bioavailability and function at active sites Includes a dedicated chapter on the effect of plant metabolites on SARS-CoV-2

Solving Problems with NMR Spectroscopy

Author : Atta-ur Rahman
Publisher : Academic Press
ISBN 13 : 0124116132
Total Pages : 535 pages
Book Rating : 4.1/5 (241 download)

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Book Synopsis Solving Problems with NMR Spectroscopy by : Atta-ur Rahman

Download or read book Solving Problems with NMR Spectroscopy written by Atta-ur Rahman and published by Academic Press. This book was released on 2015-08-18 with total page 535 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solving Problems with NMR Spectroscopy, Second Edition, is a fully updated and revised version of the best-selling book. This new edition still clearly presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving many new, clear examples for readers to understand and try, with new solutions provided in the text. It also explains new developments and concepts in NMR spectroscopy, including sensitivity problems (hardware and software solutions) and an extension of the multidimensional coverage to 3D NMR. The book also includes a series of applications showing how NMR is used in real life to solve advanced problems beyond simple small-molecule chemical analysis. This new text enables organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems provided by the authors help readers understand the discussion more clearly and the solution and interpretation of spectra help readers become proficient in the application of important, modern 1D, 2D, and 3D NMR techniques to structural studies. Explains and presents the most important NMR techniques used for structural determinations Offers a unique problem-solving approach for readers to understand how to solve structure problems Uses questions and problems, including discussions of their solutions and interpretations, to help readers understand the fundamentals and applications of NMR Avoids use of extensive mathematical formulas and clearly explains how to implement NMR structure analysis Foreword by Nobel Prize winner Richard R. Ernst New to This Edition Key developments in the field of NMR spectroscopy since the First Edition in 1996 New chapter on sensitivity enhancement, a key driver of development in NMR spectroscopy New concepts such as Pulse Field Gradients, shaped pulses, and DOSY (Diffusion Order Spectroscopy) in relevant chapters More emphasis on practical aspects of NMR spectroscopy, such as the use of Shigemi tubes and various types of cryogenic probes Over 100 new problems and questions addressing the key concepts in NMR spectroscopy Improved figures and diagrams More than 180 example problems to solve, with detailed solutions provided at the end of each chapter

Aspects of Organic Chemistry

Author : Gerhard Quinkert
Publisher : John Wiley & Sons
ISBN 13 : 9783906390154
Total Pages : 530 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Aspects of Organic Chemistry by : Gerhard Quinkert

Download or read book Aspects of Organic Chemistry written by Gerhard Quinkert and published by John Wiley & Sons. This book was released on 1996 with total page 530 pages. Available in PDF, EPUB and Kindle. Book excerpt: Modeling molecular structures is a useful tool for the description, classification and understanding of molecules – species, which have already been synthesized, and others existing only in the imagination of the chemist. The first part of the four–volume series ′Aspects of Organic Chemistry′ focuses on molecular structure, especially that of nucleid acids and proteins. The authors, a team of internationally recognized specialists, present a modern interdisciplinary concept between chemistry – and biology – an approach, which proved to be useful in university education. A unique book, important for both lecturers and students. Subjects of the three remaining volumes are ′Reactivity′, ′Synthesis′ and ′Methods of Structure Elucidation′.

Experimental Pulse NMR

Author : Eiichi Fukushima
Publisher : CRC Press
ISBN 13 : 0429973497
Total Pages : 305 pages
Book Rating : 4.4/5 (299 download)

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Book Synopsis Experimental Pulse NMR by : Eiichi Fukushima

Download or read book Experimental Pulse NMR written by Eiichi Fukushima and published by CRC Press. This book was released on 2018-03-08 with total page 305 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is about pulse nuclear magnetic resonance (NMR), with its techniques, the information to be obtained, and practical advice on performing experiments. The emphasis is on the motivation and physical ideas underlying NMR experiments and the actual techniques, including the hardware used. The level is generally suitable for those to whom pulse NMR is a new technique, be they students in chemistry or physics on the one hand and research workers in biology, geology, or agriculture, on the other. The book can be used for a senior or first year graduate course where it could supplement the standard NMR texts.