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Microwave Assisted Chemistry Experiments
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Book Synopsis Laboratory Experiments Using Microwave Heating by : Nicholas E. Leadbeater
Download or read book Laboratory Experiments Using Microwave Heating written by Nicholas E. Leadbeater and published by CRC Press. This book was released on 2013-04-24 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: Allowing many chemical reactions to be completed within minutes, microwave heating has revolutionized preparative chemistry. As a result, this technology has been widely adopted in both academic and industrial laboratories. Integrating microwave-assisted chemistry into undergraduate laboratory courses enables students to perform a broader range of
Book Synopsis Synthetic Applications by : Rajender S. Varma
Download or read book Synthetic Applications written by Rajender S. Varma and published by Walter de Gruyter GmbH & Co KG. This book was released on 2022-05-09 with total page 454 pages. Available in PDF, EPUB and Kindle. Book excerpt: Magnetic nanocatalysts are an important tool for greener catalytic processes due to the ease of their removal from a reaction medium. This book explores different magnetic nanocatalysts, their use in synthesis, and their recyclability. Topics covered include magnetic nanocatalysts for S-S bond formation, N-hetercycle formation, C-heteroatom bond formation, silica-supported catalysts, multicomponent reactions, and their recyclability.
Book Synopsis Aqueous Microwave Assisted Chemistry by : Vivek Polshettiwar
Download or read book Aqueous Microwave Assisted Chemistry written by Vivek Polshettiwar and published by Royal Society of Chemistry. This book was released on 2010-05-20 with total page 243 pages. Available in PDF, EPUB and Kindle. Book excerpt: The demands for green and sustainable synthetic methods in the fields of healthcare and fine chemicals, combined with the pressure to produce these substances expeditiously and in an environmentally benign fashion, pose significant challenges to the synthetic chemical community. Green chemistry can avoid pollution by utilizing techniques that are environmentally friendly by design and one of the best green techniques is the use of microwave (MW) assisted aqueous synthetic protocols. Fusing MW technique with water (as a benign reaction medium) can offer an extraordinary synergistic effect with greater potential than these two individual components in isolation. Selective microwave heating can be exploited to develop a high yield protocol and the use of water expedites the MW-protocol with more energy efficiency. This book provides an overview of the various processes developed using aqueous microwave chemistry and is written for chemists, chemical engineers and researchers in the early stages who want to develop sustainable and green processes. Written by well known microwave experts, the book is a comprehensive examination of the field and is the first book that deals strictly with aqueous microwave chemistry and represents a significant effort towards green chemistry. It covers all the microwave-assisted aqueous reactions in depth, including heterocycle synthesis, metal catalysis, enzyme catalysis, polymer synthesis, nanomaterials synthesis and nano-catalysis. Each chapter contains representative experimental procedures, helping the reader quickly replicate some of the experiments to gain hands-on experience.
Download or read book Catalysis written by James J Spivey and published by Royal Society of Chemistry. This book was released on 2021-06-14 with total page 494 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume looks at modern approaches to catalysis and reviews the extensive literature. Chapters highlight application of 2D materials in biomass conversion catalysis, plasmonic photocatalysis, catalytic demonstration of mesoporosity in the hierarchical zeolite and the effect of surface phase oxides on supported metals and catalysis. Looking to the future a chapter on ab initio machine learning for accelerating catalytic materials discovery is included. Appealing broadly to researchers in academia and industry, these illustrative chapters bridge the gap from academic studies in the laboratory to practical applications in industry not only for catalysis field but also for environmental protection. Other chapters with an industrial perspective include heterogeneous and homogeneous catalytic routes for vinyl acetate synthesis, catalysis for production of jet fuel from renewable sources by HDO/HDC and microwave-assisted catalysis for fuel conversion. Chemical reactions in ball mills is also explored. The book will be of great benefit to any researcher wanting a succinct reference on developments in this area now and looking to the future.
Book Synopsis Microwave Assisted Organic Synthesis by : Jason Tierney
Download or read book Microwave Assisted Organic Synthesis written by Jason Tierney and published by John Wiley & Sons. This book was released on 2009-02-12 with total page 296 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first reports on the application of microwaves in organicsynthesis date back to 1986, but it was not until the recentintroduction of specifically designed and constructed equipment,which countered the safety and reproducibility concerns, thatsynthetic application of microwaves has become established as alaboratory technique. Microwave assisted synthesis is now beingadopted in many industrial and academic laboratories to takeadvantage of the novel chemistry that can be carried out using avariety of organic reaction types. This book demonstrates the underlying principles of microwavedielectric heating and, by reference to a range of organic reactiontypes, it's effective use in synthetic organic chemistry. Toillustrate the impact microwave assisted organic synthesis can haveon chemical research, case studies drawn mainly from thepharmaceutical industry are presented.
Book Synopsis Microwave Methods in Organic Synthesis by : Mats Larhed
Download or read book Microwave Methods in Organic Synthesis written by Mats Larhed and published by Springer. This book was released on 2006-09-21 with total page 297 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents critical reviews of the present position and future trends in modern chemical research. It contains short and concise reports on chemistry, each written by the world renowned experts. The book is still valid and useful after 5 or 10 years. More information as well as the electronic version of the whole content is available at: springerlink.com. The book will interest scientists and practitioners in the mentioned fields and in industry.
Book Synopsis Elementary Pharmacoinformatics by : t Durai Ananda Kumar
Download or read book Elementary Pharmacoinformatics written by t Durai Ananda Kumar and published by Pharmamed Press. This book was released on 2015-06-28 with total page 362 pages. Available in PDF, EPUB and Kindle. Book excerpt: Pharmacoinformatics is an informatics based discipline, concerned with the information, design, discovery and development of drugs using high performance computing and graphic tools. This material covers principles and applications of health informatics, cheminformatics and bioinformatics. It comprehensively covers the current advances and in silico strategies used in drug information and drug design. Each of 29 chapters reviews the concepts of pharmacy automation, mechanistic drug design and bioinformatics. The book avoids the use of high level descriptions to convert the subject interesting. This concise source of information will be of immense benefit to the learning community of pharmacy, bio-technology, biomedical engineering and other interdisciplinary fields. Explanations for the entry level student are the important feature of this material - Neat and self explanatory diagrams are incorporated wherever possible to bring user-friendly material Four major parts with 29 chapters proceeds in very systematic and with lucid language - Each chapter is provided with practical application part, which ensures the better understanding Comprehensive overview on in silico methods of drug information and drug design - Emphasis on molecular level approach of drug design strategies The application section of this material provides opportunity to have hands-on-experience Distinct features of this book Descriptions followed systematic approach with very simple language - Neat and self explanatory reaction mechanisms given for all the chemical reactions Role of reagents, alternative reagents and hazards associated are highlighted - Pharmaceutical relevance is given wherever possible Limit tests, qualitative analysis of inorganic, natural and synthetic organic compounds are given in very lucid manner - Estimations of natural and organic-medicinal compounds are given along with isolation of active principles from natural resources
Book Synopsis Practical Microwave Synthesis for Organic Chemists by : C. Oliver Kappe
Download or read book Practical Microwave Synthesis for Organic Chemists written by C. Oliver Kappe and published by John Wiley & Sons. This book was released on 2008-11-21 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the novice user in mind, this beginner's guide explains thebasics behind microwave technology, evaluates available instrumentsand reaction modes, and provides practical hints for everyeventuality. Includes 27 detailed protocols for often-usedreactions. From the contents: 1 Microwave Synthesis - An Introduction 2 Microwave Theory 3 Equipment Review 4 Microwave Processing Techniques 5 Starting With Microwave Chemistry 6 Experimental Protocols 6.1 General Small-Scale Sealed-Vessel Microwave Processing 6.2 Reaction Optimization 6.3 Library Generation 6.4 Reaction Scale-Up 6.5 Special Processing Techniques
Book Synopsis Microwave-assisted Extraction for Bioactive Compounds by : Farid Chemat
Download or read book Microwave-assisted Extraction for Bioactive Compounds written by Farid Chemat and published by Springer Science & Business Media. This book was released on 2012-12-12 with total page 248 pages. Available in PDF, EPUB and Kindle. Book excerpt: With increasing energy prices and the drive to reduce CO2 emissions, food industries are challenged to find new technologies in order to reduce energy consumption, to meet legal requirements on emissions, product/process safety and control, and for cost reduction and increased quality as well as functionality. Extraction is one of the promising innovation themes that could contribute to sustainable growth in the chemical and food industries. For example, existing extraction technologies have considerable technological and scientific bottlenecks to overcome, such as often requiring up to 50% of investments in a new plant and more than 70% of total process energy used in food, fine chemicals and pharmaceutical industries. These shortcomings have led to the consideration of the use of new "green" techniques in extraction, which typically use less solvent and energy, such as microwave extraction. Extraction under extreme or non-classical conditions is currently a dynamically developing area in applied research and industry. Using microwaves, extraction and distillation can now be completed in minutes instead of hours with high reproducibility, reducing the consumption of solvent, simplifying manipulation and work-up, giving higher purity of the final product, eliminating post-treatment of waste water and consuming only a fraction of the energy normally needed for a conventional extraction method. Several classes of compounds such as essential oils, aromas, anti-oxidants, pigments, colours, fats and oils, carbohydrates, and other bioactive compounds have been extracted efficiently from a variety of matrices (mainly animal tissues, food, and plant materials). The advantages of using microwave energy, which is a non-contact heat source, includes more effective heating, faster energy transfer, reduced thermal gradients, selective heating, reduced equipment size, faster response to process heating control, faster start-up, increased production, and elimination of process steps. This book will present a complete picture of the current knowledge on microwave-assisted extraction (MAE) of bioactive compounds from food and natural products. It will provide the necessary theoretical background and details about extraction by microwaves, including information on the technique, the mechanism, protocols, industrial applications, safety precautions, and environmental impacts.
Book Synopsis Comprehensive Organic Chemistry Experiments for the Laboratory Classroom by : Carlos A. M. Afonso
Download or read book Comprehensive Organic Chemistry Experiments for the Laboratory Classroom written by Carlos A. M. Afonso and published by Royal Society of Chemistry. This book was released on 2016-12-16 with total page 976 pages. Available in PDF, EPUB and Kindle. Book excerpt: This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.
Book Synopsis Green Chemistry Experiments in Undergraduate Laboratories by : Jodie T. Fahey
Download or read book Green Chemistry Experiments in Undergraduate Laboratories written by Jodie T. Fahey and published by ACS Symposium. This book was released on 2018-02-02 with total page 184 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the introduction of green chemistry principles in industrial processes, interest has continued to grow and green chemistry has started to take roots in educational laboratories of all disciplines of chemistry. Entire courses centered around green chemistry are becoming more prevalent. By introducing students to green chemistry at a collegiate level, they will better be prepared for industry, graduate schools, and also have a better appreciation for the environment. This book includes experiments that cover a range of green chemistry principles, particularly in the field of organic chemistry. Green chemistry, as we know it today, revolves around a set of twelve principles that were outlined 1998. The experiments presented in this text utilize many of the 12 Principles of Green Chemistry. Each chapter presents an experiment that utilizes at least one, if not more, of these principles. This book is targeted for any professor who would like to introduce green or "greener" laboratory experiments for their students in any chemistry course regardless of level. The book is designed to introduce students to the ideas, principles, and benefits of green chemistry and inspire educators to adopt more green chemistry principles in their course.
Book Synopsis Microwave-assisted Polymer Synthesis by : Richard Hoogenboom
Download or read book Microwave-assisted Polymer Synthesis written by Richard Hoogenboom and published by Springer. This book was released on 2016-09-02 with total page 357 pages. Available in PDF, EPUB and Kindle. Book excerpt: The series Advances in Polymer Science presents critical reviews of the present and future trends in polymer and biopolymer science. It covers all areas of research in polymer and biopolymer science including chemistry, physical chemistry, physics, material science.The thematic volumes are addressed to scientists, whether at universities or in industry, who wish to keep abreast of the important advances in the covered topics.Advances in Polymer Science enjoys a longstanding tradition and good reputation in its community. Each volume is dedicated to a current topic, and each review critically surveys one aspect of that topic, to place it within the context of the volume. The volumes typically summarize the significant developments of the last 5 to 10 years and discuss them critically, presenting selected examples, explaining and illustrating the important principles, and bringing together many important references of primary literature. On that basis, future research directions in the area can be discussed. Advances in Polymer Science volumes thus are important references for every polymer scientist, as well as for other scientists interested in polymer science - as an introduction to a neighboring field, or as a compilation of detailed information for the specialist.Review articles for the individual volumes are invited by the volume editors. Single contributions can be specially commissioned.Readership: Polymer scientists, or scientists in related fields interested in polymer and biopolymer science, at universities or in industry, graduate students
Book Synopsis Microwaves in Organic Synthesis by : Antonio de la Hoz
Download or read book Microwaves in Organic Synthesis written by Antonio de la Hoz and published by John Wiley & Sons. This book was released on 2013-02-26 with total page 1354 pages. Available in PDF, EPUB and Kindle. Book excerpt: The third edition of the bestselling two-volume reference covers everything you need to know about microwave technology for synthesis - from the best equipment to nonthermal effects, from solid-support reactions to catalysis. Completely revised and updated with half of the authors completely new to the project, this comprehensive work is clearly divided into two parts on the fundamentals of microwave irradiation, and application of microwaves and synergies with other enabling techniques. Also new to this edition are chapters on on-line monitoring, flow chemistry, combination with ultrasounds and natural products, including multicomponent reactions. An indispensable source for organic, catalytic, physical, and medicinal chemists.
Book Synopsis Microwaves in Catalysis by : Satoshi Horikoshi
Download or read book Microwaves in Catalysis written by Satoshi Horikoshi and published by John Wiley & Sons. This book was released on 2015-12-14 with total page 426 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive overview covering the principles and preparation of catalysts, as well as reactor technology and applications in the field of organic synthesis, energy production, and environmental catalysis. Edited and authored by renowned and experienced scientists, this reference focuses on successful reaction procedures for applications in industry. Topics include catalyst preparation, the treatment of waste water and air, biomass and waste valorisation, hydrogen production, oil refining as well as organic synthesis in the presence of heterogeneous and homogeneous catalysts and continuous-flow reactions. With its practical relevance and successful methodologies, this is a valuable guide for chemists at universities working in the field of catalysis, organic synthesis, pharmaceutical or green chemistry, as well as researchers and engineers in the chemical industry.
Book Synopsis Comprehensive Organic Chemistry Experiments for the Laboratory Classroom by : Carlos A M Afonso
Download or read book Comprehensive Organic Chemistry Experiments for the Laboratory Classroom written by Carlos A M Afonso and published by Royal Society of Chemistry. This book was released on 2020-08-28 with total page 976 pages. Available in PDF, EPUB and Kindle. Book excerpt: This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.
Book Synopsis Microwave Synthesis by : Brittany L. Hayes
Download or read book Microwave Synthesis written by Brittany L. Hayes and published by . This book was released on 2002 with total page 300 pages. Available in PDF, EPUB and Kindle. Book excerpt: 1. Introduction to microwave chemistry 11; 2. Solvents 29; 3. Chemical reactions in the presence and absence of solvent 77; 4. Synthetic applications 95; 5. Getting started with microwave synthesis 157; 6. Microwave safety considerations 175; 7. Microwave hardware 181.
Book Synopsis Aqueous Microwave Assisted Chemistry by : Vivek Polshettiwar
Download or read book Aqueous Microwave Assisted Chemistry written by Vivek Polshettiwar and published by Royal Society of Chemistry. This book was released on 2010 with total page 243 pages. Available in PDF, EPUB and Kindle. Book excerpt: The demands for green and sustainable synthetic methods in the fields of healthcare and fine chemicals, combined with the pressure to produce these substances expeditiously and in an environmentally benign fashion, pose significant challenges to the synthetic chemical community. Green chemistry can avoid pollution by utilizing techniques that are environmentally friendly by design and one of the best green techniques is the use of microwave (MW) assisted aqueous synthetic protocols. Fusing MW technique with water (as a benign reaction medium) can offer an extraordinary synergistic effect with greater potential than these two individual components in isolation. Selective microwave heating can be exploited to develop a high yield protocol and the use of water expedites the MW-protocol with more energy efficiency. This book provides an overview of the various processes developed using aqueous microwave chemistry and is written for chemists, chemical engineers and researchers in the early stages who want to develop sustainable and green processes. Written by well known microwave experts, the book is a comprehensive examination of the field and is the first book that deals strictly with aqueous microwave chemistry and represents a significant effort towards green chemistry. It covers all the microwave-assisted aqueous reactions in depth, including heterocycle synthesis, metal catalysis, enzyme catalysis, polymer synthesis, nanomaterials synthesis and nano-catalysis. Each chapter contains representative experimental procedures, helping the reader quickly replicate some of the experiments to gain hands-on experience.
