Mass Spectrometry For The Analysis Of Pesticide Residues And Their Metabolites

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Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites

Author : Despina Tsipi
Publisher : John Wiley & Sons
ISBN 13 : 1119070007
Total Pages : 288 pages
Book Rating : 4.1/5 (19 download)

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Book Synopsis Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites by : Despina Tsipi

Download or read book Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites written by Despina Tsipi and published by John Wiley & Sons. This book was released on 2015-05-12 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new ionization techniques as well as the main MS platforms, software tools and mass spectral libraries

Multiresidue Methods for the Analysis of Pesticide Residues in Food

Author : Horacio Heinzen
Publisher : CRC Press
ISBN 13 : 1482235102
Total Pages : 452 pages
Book Rating : 4.4/5 (822 download)

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Book Synopsis Multiresidue Methods for the Analysis of Pesticide Residues in Food by : Horacio Heinzen

Download or read book Multiresidue Methods for the Analysis of Pesticide Residues in Food written by Horacio Heinzen and published by CRC Press. This book was released on 2017-10-10 with total page 452 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.

Liquid Chromatography

Author : F. Hernández
Publisher : Elsevier Inc. Chapters
ISBN 13 : 0128071176
Total Pages : 28 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Liquid Chromatography by : F. Hernández

Download or read book Liquid Chromatography written by F. Hernández and published by Elsevier Inc. Chapters. This book was released on 2013-01-08 with total page 28 pages. Available in PDF, EPUB and Kindle. Book excerpt: Pesticide residue analysis is a specialized field of modern analytical chemistry, where the role of LC–MS is of great importance. A highly reliable determination, including both quantification and identification, of pesticide residues in food is required nowadays because of the strict international regulations on maximum residue Limits. The increasing interest of including metabolites in analyses comes from the inclusion of pesticide-related compounds within the residue definition. The polar character of most pesticides used at present and their metabolites make LC coupled to tandem MS the technique of choice for the great majority of compounds. Thus, LC–MS/MS with a triple-quadrupole (QqQ) analyzer is highly appropriate for developing multiresidue methods, where up to 200–300 analytes can be simultaneously determined. It can also be efficiently applied to solve analytical problems associated with some problematic pesticides, such as those present as ionic compounds in the samples, which have to be determined with more specific LC–MS/MS methods. High-resolution MS using modern analyzers like time of flight or Orbitrap offers interesting features for wide-scope screening of pesticides and metabolites in food, due to their mass accuracy capabilities, with the advantage that a retrospective analysis is feasible at any time to search for other compounds that were not included in the first analysis.

Applications in High Resolution Mass Spectrometry

Author : Roberto Romero-González
Publisher : Elsevier
ISBN 13 : 0128096489
Total Pages : 362 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Applications in High Resolution Mass Spectrometry by : Roberto Romero-González

Download or read book Applications in High Resolution Mass Spectrometry written by Roberto Romero-González and published by Elsevier. This book was released on 2017-03-07 with total page 362 pages. Available in PDF, EPUB and Kindle. Book excerpt: Applications of High Resolution Mass Spectrometry: Food Safety and Pesticide Residue Analysis is the first book to offer complete coverage of all aspects of high resolution mass spectrometry (HRMS) used for the analysis of pesticide residue in food. Aimed at researchers and graduate students in food safety, toxicology, and analytical chemistry, the book equips readers with foundational knowledge of HRMS, including established and state-of-the-art principles and analysis strategies. Additionally, it provides a roadmap for implementation, including discussions of the latest instrumentation and software available. Detailed coverage is given to the application of HRMS coupled to ultra high-performance liquid chromatography (UHPLC-HRMS) in the analysis of pesticide residue in fruits and vegetables and food from animal origin. The book also discusses extraction procedures and the challenges of sample preparation, gas chromatography coupled to high resolution mass spectrometry, flow injection-HRMS, ambient ionization, and identification of pesticide transformation products in food. Responding to the fast development and application of these new procedures, this book is an essential resource in the food safety field. Arms researchers with an in-depth resource devoted to the rapid advances in HRMS tools and strategies for pesticide residue analysis in food Provides a complete overview of analytical methodologies and applications of HRMS, including UHPLC-HRMS, HRMS coupled with time of flight (TOF) and/or GC-Orbitrap, and flow injection-HRMS Discusses the current international regulations and legislation related to the use of HRMS in pesticide residue analysis Features a chapter on the hardware and software available for HRMS implementation Offers separate chapters on HRMS applied to pesticide residue analysis in fruits and vegetables and in food from animal origin

Analysis of Pesticides in Food and Environmental Samples, Second Edition

Author : Jose L. Tadeo
Publisher : CRC Press
ISBN 13 : 135104706X
Total Pages : 380 pages
Book Rating : 4.3/5 (51 download)

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Book Synopsis Analysis of Pesticides in Food and Environmental Samples, Second Edition by : Jose L. Tadeo

Download or read book Analysis of Pesticides in Food and Environmental Samples, Second Edition written by Jose L. Tadeo and published by CRC Press. This book was released on 2019-03-04 with total page 380 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a critical overview of analytical methods used for the determination of pesticide residues and other contaminants in food and environmental samples by modern instrumental analysis. It contains up-to-date material including recent trends in sample preparation, general methods used for pesticide analysis and quality assurance aspects, and chromatographic and immunoassay methods. The rest of the book describes particular analytical methods used for the determination of pesticides in food and soil, water and air. In addition, the levels of these chemicals found in food, their regulatory aspects and the monitoring of pesticides in the environment are described.

Pesticide Residues in Foods

Author : W. George Fong
Publisher : John Wiley & Sons
ISBN 13 : 0471574007
Total Pages : 389 pages
Book Rating : 4.4/5 (715 download)

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Book Synopsis Pesticide Residues in Foods by : W. George Fong

Download or read book Pesticide Residues in Foods written by W. George Fong and published by John Wiley & Sons. This book was released on 1999-01-29 with total page 389 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in analytical chemistry methodology now allow us to detect the most minute trace amounts of pesticides. As this capacity grows, so does public concern about toxic contamination, resulting in stricter government regulations and a growing demand for even more sensitive, precise, and reliable analysis. Addressing the interplay between regulations and the development of analytical technology, this volume presents the first unified treatment of the regulatory and analytical aspects of pesticide residues. Current regulations, existing and emerging methodologies, state-of-the-art instrumentation, and the basic science of analyzing for pesticides in food and other environmental media are all covered. The book provides step-by-step guidelines to analytical techniques, along with real-world examples from the latest research-showing the reader how to analyze minute traces of pesticides quickly and accurately, using both highly sophisticated and basic, less sensitive techniques. Many safety issues are explored in depth, as are the regulatory aspects of pesticide registration, residue analysis, exposure monitoring, risk assessment, and tolerance enforcement. Timely, authoritative, and practical throughout, Pesticide Residues in Foods is an invaluable reference for analytical chemists and laboratory managers everywhere-in industry, agriculture, environmental sciences, research, and instrument manufacturing-and for anyone with an interest in the broader environmental, agricultural, and consumer-related implications of pesticide use. An invaluable resource for analytical chemists and laboratory managers, Pesticide Residues in Foods provides a complete overview of the theory, practice, and regulatory aspects of pesticide residue analysis today, including: * All regulatory issues, from risk assessment and tolerance to data-quality requirements to laboratory accreditation standards * State-of-the-art methodologies and instrumentation, including high- performance liquid chromatography and mass spectrometry * The application of analytical technology to "green chemistry," such as the reduction of solvents and toxic reagents in the laboratory * Novel solutions to the old problem of keeping the food supply safe from harmful levels of pesticides * Ample examples to help analytical chemists select the most appropriate method for a given residue analysis * Easy-to-use tables and figures throughout the text

Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues

Author : A.R. Fernandez Alba
Publisher : Elsevier
ISBN 13 : 0080454402
Total Pages : 509 pages
Book Rating : 4.0/5 (84 download)

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Book Synopsis Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues by : A.R. Fernandez Alba

Download or read book Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues written by A.R. Fernandez Alba and published by Elsevier. This book was released on 2004-12-11 with total page 509 pages. Available in PDF, EPUB and Kindle. Book excerpt: The trace determination of pesticides continues to be a topic for analytical chemists working in research centres, government and universities. With four chapters devoted to chromatography-mass spectrometry methods, readers are able to understand the analytical basis, technical characteristics and possibilities to evaluate pesticides in food by gas chromatography (GC) and liquid chromatography (LC) mass spectrometry. The book also provides a well-defined and critical compilation of the sample treatment and clean-up procedures, as well as injection techniques applied in GC and LC food analysis. Finally the book deals with aspects related to analytical quality control requirements for pesticide residues, in addition to pesticide regulation aspects. * Contains specific chapters devoted to chromatography-mass spectrometry methods* Provides a well-defined and critical compilation of the sample treatment and clean-up procedures* Contains aspects related to analytical quality control requirements for pesticide residues

Pesticide Protocols

Author : José L. Martínez Vidal
Publisher : Springer Science & Business Media
ISBN 13 : 159259929X
Total Pages : 491 pages
Book Rating : 4.5/5 (925 download)

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Book Synopsis Pesticide Protocols by : José L. Martínez Vidal

Download or read book Pesticide Protocols written by José L. Martínez Vidal and published by Springer Science & Business Media. This book was released on 2007-10-26 with total page 491 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive collection of robust methods for the detection of pesticide compounds or their metabolites useful in food, environmental, and biological monitoring, and in studies of exposure via food, water, air, and the skin or lungs. The readily reproducible methods range from gas and liquid chromatography coupled to mass spectrometry detection and other classic detectors, to capillary electrophoresis and immunochemical or radioimmunoassay methods. The authors have focused on extraction and cleanup procedures, in order to develop and optimize more fullyautomated and miniaturized methods, including solid-phase extraction, solid-phase microextraction, microwave-assisted extraction, and on-line tandem liquid chromatography (LC/LC) trace enrichment, among others. The protocols offer step-by-step laboratory instructions, an introduction outlining the principles behind the technique, lists of the necessary equipment and reagents, and tips on troubleshooting and avoiding known pitfalls.

Analysis of Pesticides in Food and Environmental Samples

Author : Jose L. Tadeo
Publisher : CRC Press
ISBN 13 : 1420007750
Total Pages : 382 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Analysis of Pesticides in Food and Environmental Samples by : Jose L. Tadeo

Download or read book Analysis of Pesticides in Food and Environmental Samples written by Jose L. Tadeo and published by CRC Press. This book was released on 2008-02-07 with total page 382 pages. Available in PDF, EPUB and Kindle. Book excerpt: Developing safety regulations for pesticides used around the world—in excess of 2.5 million tons annually—requires reliable analytical methods for assessing their impact in food and in the environment. Analysis of Pesticides in Food and Environmental Samples presents the most effective techniques for analyzing pesticide residues and other chemical contaminants in foods as well as in soil, water, and air. Renowned Scientists Report New Data and Advances in the Field The book introduces sample preparation, extraction, and analytical methods specific to each sample type, including foods from vegetal and animal origin. Other chapters discuss important aspects of quality assurance and the applicability of hyphenated analytical techniques. In addition to a practical chapter on the use of biosensors and immunoassays for monitoring and gathering exposure data, the book addresses regulatory aspects and presents current data on the levels of pesticides found in food and environmental matrices. Latest Methods Help Scientists Develop Safer, More Effective Pesticides Analysis of Pesticides in Food and Environmental Samples enables scientists to measure and predict the behavior and toxicity of pesticides with a higher degree of accuracy. The methodologies and insight in this timely work will contribute to the development of more effective, less toxic pesticides as well as better safety regulations.

Analysis of Pesticide Residues

Author : H. Anson Moye
Publisher : John Wiley & Sons
ISBN 13 :
Total Pages : 488 pages
Book Rating : 4.:/5 (44 download)

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Book Synopsis Analysis of Pesticide Residues by : H. Anson Moye

Download or read book Analysis of Pesticide Residues written by H. Anson Moye and published by John Wiley & Sons. This book was released on 1981-02-02 with total page 488 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive guide to the latest techniques and applications of pesticide trace analysis. Methods covered include gas, thin layer, and high-performance liquid chromatography, along with their applications in the analysis of chlorinated hydrocarbons, acidic herbicides, organophosphates, carbamates, and insect pheromones and hormones. Includes a special chapter on residue data requirements of government agencies.

High Performance Liquid Chromatography in Pesticide Residue Analysis

Author : Tomasz Tuzimski
Publisher : CRC Press
ISBN 13 : 1466568828
Total Pages : 583 pages
Book Rating : 4.4/5 (665 download)

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Book Synopsis High Performance Liquid Chromatography in Pesticide Residue Analysis by : Tomasz Tuzimski

Download or read book High Performance Liquid Chromatography in Pesticide Residue Analysis written by Tomasz Tuzimski and published by CRC Press. This book was released on 2015-05-20 with total page 583 pages. Available in PDF, EPUB and Kindle. Book excerpt: HPLC is the principal separation technique for identification of the pesticides in environmental samples and for quantitative analysis of analytes. At each stage of the HPLC procedure, the chromatographer should possess both the practical and theoretical skills required to perform HPLC experiments correctly and to obtain reliable, repeatable, and r

Analysis of Pesticide in Tea

Author : Guo-Fang Pang
Publisher : Elsevier
ISBN 13 : 0128127287
Total Pages : 952 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Analysis of Pesticide in Tea by : Guo-Fang Pang

Download or read book Analysis of Pesticide in Tea written by Guo-Fang Pang and published by Elsevier. This book was released on 2018-08-18 with total page 952 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analysis of Pesticide in Tea: Chromatography-Mass Spectrometry Methodology is a comprehensive book, providing serial, rapid, high-throughput analytical methods for determining more than 600 pesticides in tea. There are increasing numbers of strict limit standards for pesticide residues in edible agricultural products in countries all over the world. The threshold for pesticide residues in tea is high for international trade. At present, 17 countries and international organizations have stipulated MRL levels for over 800 pesticide residues in tea. All methods described in this book are validated by an independent, U.S.-based organization (AOAC International), and all indexes have satisfied AOAC International's criteria. China has a history of 5000 years in growing tea and is a large tea producer with 80 million people involved in tea growing. China exports tea to over 100 countries worldwide, enjoying a high reputation for quality and variety. Covers a wide range of research activities that are highly appropriate to current research methods Reflects the most recent research in nearly all cases, providing an excellent compilation of feasible methods needed for official analysis Describes methods that are internationally validated by an independent, U.S.-based organization (AOAC International) Authored by Dr. Pang, who is internationally recognized in the area of pesticide residues and other contaminants in foods

Guidelines on Analytical Methodology for Pesticide Residue Monitoring

Author : Council on Environmental Quality (U.S.). Federal Working Group on Pest Management. Monitoring Panel
Publisher :
ISBN 13 :
Total Pages : 80 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Guidelines on Analytical Methodology for Pesticide Residue Monitoring by : Council on Environmental Quality (U.S.). Federal Working Group on Pest Management. Monitoring Panel

Download or read book Guidelines on Analytical Methodology for Pesticide Residue Monitoring written by Council on Environmental Quality (U.S.). Federal Working Group on Pest Management. Monitoring Panel and published by . This book was released on 1975 with total page 80 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Analytical Methods for Food Safety by Mass Spectrometry

Author : Guo-Fang Pang
Publisher : Academic Press
ISBN 13 : 0128141689
Total Pages : 882 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Analytical Methods for Food Safety by Mass Spectrometry by : Guo-Fang Pang

Download or read book Analytical Methods for Food Safety by Mass Spectrometry written by Guo-Fang Pang and published by Academic Press. This book was released on 2018-06-29 with total page 882 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Methods for Food Safety by Mass Spectrometry, Volume One: Pesticides systematically introduces the Pesticide and Veterinary Drug Multiresidues Analytical Methods. Volume One includes discussions on 20 pesticide multiresidues chromatic-MS (GC-MS and LC-MS/MS) analytical techniques that have the capability of detecting over 800 pesticides and chemicals in 10 categories of agricultural products, including fruits, vegetables, grains, teas, Chinese medicinal herbs, edible fungus mushrooms, fruit and vegetable juices, animal tissues, aquatic products, raw milk and milk powders, and drinkable water. This book also includes chromatic-MS analytical parameters, linear equations and GPC chromatic behavior parameters for over 800 pesticides. This valuable book can be used as reference for not only university students, but also technical personnel of different specialties who are engaged with study and applications, such as food safety, agricultural environment protection, pesticide development, and utilization in scientific research units, institutions and quality inspection organizations. Provides the chromatic-MS analytical technique for over 1000 commonly-used veterinary and pesticide residues Covers a large varieties of target compounds, including over 800 pesticides (organophosphorus, organochlorine, carbamate, pyrethroids) and over 200 veterinary drugs, including Fluoroquinolone, Sulfonamides, Chloramphenicol, Nitrofurans, Tetracyclines, Nitroimidazole, ß-lactams, Quinoxaline, Benzimidazole, ß-Adrenoceptor agonists, Aminoglycoside, and more Includes the latest information on sophisticated pre-treatment techniques with a single sample pre-treatment and simultaneous detection by GC-MS and LC-MS/MS

Emerging Strategies for Pesticide Analysis

Author : Thomas Cairns
Publisher : CRC Press
ISBN 13 : 9780849379918
Total Pages : 364 pages
Book Rating : 4.3/5 (799 download)

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Book Synopsis Emerging Strategies for Pesticide Analysis by : Thomas Cairns

Download or read book Emerging Strategies for Pesticide Analysis written by Thomas Cairns and published by CRC Press. This book was released on 1992-08-05 with total page 364 pages. Available in PDF, EPUB and Kindle. Book excerpt: Emerging Strategies for Pesticide Analysis presents a selection of reports on analytical technologies in the field of pesticide residue analysis. These reports have been written by international experts in their respective fields. Applications-oriented chapters focus on methods development for extraction and cleanup, in addition to multiresidue analysis of important pesticides. Other chapters describe alternative analytical approaches to conventional detection methods. stressing advantages and disadvantages of techniques such as fiber optic spectroscopy, ion trap mass spectrometry, LC/MS, and others. The final chapter summarizes the future of technological advancement in pesticide analysis.

Guidelines on Analytical Methodology for Pesticide Residue Monitoring

Author : Federal Working Group on Pest Management
Publisher :
ISBN 13 :
Total Pages : 76 pages
Book Rating : 4.:/5 (319 download)

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Book Synopsis Guidelines on Analytical Methodology for Pesticide Residue Monitoring by : Federal Working Group on Pest Management

Download or read book Guidelines on Analytical Methodology for Pesticide Residue Monitoring written by Federal Working Group on Pest Management and published by . This book was released on 1975 with total page 76 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites

Author : Despina Tsipi
Publisher : John Wiley & Sons
ISBN 13 : 1118500172
Total Pages : 288 pages
Book Rating : 4.1/5 (185 download)

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Book Synopsis Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites by : Despina Tsipi

Download or read book Mass Spectrometry for the Analysis of Pesticide Residues and their Metabolites written by Despina Tsipi and published by John Wiley & Sons. This book was released on 2015-04-27 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides an overview of the use of mass spectrometry (MS) for the analysis of pesticide residues and their metabolites. Presents state of the-art MS techniques for the identification of pesticides and their transformation products in food and environment Covers important advances in MS techniques including MS instrumentation and chromatographic separations (e.g. UPLC, HILIC, comprehensive GCxGC) and applications Illustrates the main sample preparation techniques (SPE, QuEChERS, microextraction) used in combination with MS for the analysis of pesticides Describes various established and new ionization techniques as well as the main MS platforms, software tools and mass spectral libraries