Liquid Chromatography-tandem Mass Spectrometry of Fire Debris Evidence at Suspected Clandestine Methamphetamine Laboratories

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ISBN 13 :
Total Pages : 33 pages
Book Rating : 4.:/5 (932 download)

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Book Synopsis Liquid Chromatography-tandem Mass Spectrometry of Fire Debris Evidence at Suspected Clandestine Methamphetamine Laboratories by : Matthew Kevin Green

Download or read book Liquid Chromatography-tandem Mass Spectrometry of Fire Debris Evidence at Suspected Clandestine Methamphetamine Laboratories written by Matthew Kevin Green and published by . This book was released on 2014 with total page 33 pages. Available in PDF, EPUB and Kindle. Book excerpt: The "One-Pot" methamphetamine production method involves the combination and use of highly reactive and flammable materials. Individuals attempting this method are creating clandestine laboratories within residences and other occupied structures, and the likelihood of a subsequent fire puts anyone nearby at risk. In the State of Oklahoma, if the production of methamphetamine causes a fire, the crime falls under the first degree arson statute, which can involve a prison sentence of 35 years, as opposed to 7 years for the production of drugs. The ability to detect methamphetamine and the One-Pot precursors in fire debris would strengthen the arson investigation. One-Pot methamphetamine reactions were carried out and the liquid and solid products were used to recreate a fire. Small burn cells were used to represent a residential environment. Several fire debris sample types were collected, including wall wipe samples, burned bottles, wood, and carpet. Each sample was analyzed for ignitable liquids using headspace extraction and gas chromatography-mass spectrometry (GC/MS). Following arson analysis, liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used to detect methamphetamine and pseudoephedrine, the methamphetamine precursor, in the fire debris. Additionally, fire debris samples were provided to local law enforcement and GC/MS was also able to detect methamphetamine in the fire debris. This work demonstrates that fire debris analysis can prove the presence of clandestine methamphetamine laboratories that result in arson fires.

The Development of a Liquid Chromatography/tandem Mass Spectrometry Method Using Selected Markers for Establishing a Chemical Fingerprint for Seized Clandestine Methamphetamine

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ISBN 13 :
Total Pages : 206 pages
Book Rating : 4.:/5 (268 download)

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Book Synopsis The Development of a Liquid Chromatography/tandem Mass Spectrometry Method Using Selected Markers for Establishing a Chemical Fingerprint for Seized Clandestine Methamphetamine by : Sri Bharat Madireddy

Download or read book The Development of a Liquid Chromatography/tandem Mass Spectrometry Method Using Selected Markers for Establishing a Chemical Fingerprint for Seized Clandestine Methamphetamine written by Sri Bharat Madireddy and published by . This book was released on 2008 with total page 206 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Forensic Investigation of Clandestine Laboratories

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Publisher : CRC Press
ISBN 13 : 9780849312274
Total Pages : 394 pages
Book Rating : 4.3/5 (122 download)

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Book Synopsis Forensic Investigation of Clandestine Laboratories by : Donnell R. Christian, Jr.

Download or read book Forensic Investigation of Clandestine Laboratories written by Donnell R. Christian, Jr. and published by CRC Press. This book was released on 2003-07-28 with total page 394 pages. Available in PDF, EPUB and Kindle. Book excerpt: Clandestine lab operators are not the mad scientists whose genius keeps them pent up in the laboratory contemplating elaborate formulas and mixing exotic chemicals. In fact, their equipment is usually simple, their chemicals household products, and their education basic. Most of the time the elements at the scene are perfectly legal to sell and own. It is only in the combination of all these elements that the lab becomes the scene of a criminal operation. Forensic Investigation of Clandestine Laboratories guides you, step-by-step, through the process of recognizing these illegal manufacturing operations. Then it shows you how to prove it in the courtroom. In non-technical language this book details: How to recognize a clandestine lab How to process the site of a clandestine lab How to analyze evidence in the examination laboratory What to derive from the physical evidence How to present the evidence in court The identification and investigation of a clandestine lab, and the successful prosecution of the perpetrators, is a team effort. A collaboration of law enforcement, forensic experts, scientists, and criminal prosecutors is required to present a case that definitively demonstrates how a group of items with legitimate uses are being used to manufacture an illegal controlled substance. Providing an understanding of how the pieces of the clandestine lab puzzle fit together, this book outlines the steps needed to identify and shut down these operations, as well as successfully prosecute the perpetrators.

Fire Debris Analysis

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Publisher : Academic Press
ISBN 13 : 0080556264
Total Pages : 683 pages
Book Rating : 4.0/5 (85 download)

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Book Synopsis Fire Debris Analysis by : Eric Stauffer

Download or read book Fire Debris Analysis written by Eric Stauffer and published by Academic Press. This book was released on 2007-12-10 with total page 683 pages. Available in PDF, EPUB and Kindle. Book excerpt: The study of fire debris analysis is vital to the function of all fire investigations, and, as such, Fire Debris Analysis is an essential resource for fire investigators. The present methods of analysis include the use of gas chromatography and gas chromatography-mass spectrometry, techniques which are well established and used by crime laboratories throughout the world. However, despite their universality, this is the first comprehensive resource that addresses their application to fire debris analysis. Fire Debris Analysis covers topics such as the physics and chemistry of fire and liquid fuels, the interpretation of data obtained from fire debris, and the future of the subject. Its cutting-edge material and experienced author team distinguishes this book as a quality reference that should be on the shelves of all crime laboratories. Serves as a comprehensive guide to the science of fire debris analysis Presents both basic and advanced concepts in an easily readable, logical sequence Includes a full-color insert with figures that illustrate key concepts discussed in the text

Basic Principles of Forensic Chemistry

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Publisher : Springer Science & Business Media
ISBN 13 : 1597454370
Total Pages : 360 pages
Book Rating : 4.5/5 (974 download)

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Book Synopsis Basic Principles of Forensic Chemistry by : JaVed I. Khan

Download or read book Basic Principles of Forensic Chemistry written by JaVed I. Khan and published by Springer Science & Business Media. This book was released on 2011-11-16 with total page 360 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on a marvel approach that blends chemistry with forensic science and is used for the examination of controlled substances and clandestine operations. The book will particularly interest forensic chemists, forensic scientists, criminologists, and biochemists.

Forensic Chemistry Handbook

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Publisher : John Wiley & Sons
ISBN 13 : 111806223X
Total Pages : 544 pages
Book Rating : 4.1/5 (18 download)

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Book Synopsis Forensic Chemistry Handbook by : Lawrence Kobilinsky

Download or read book Forensic Chemistry Handbook written by Lawrence Kobilinsky and published by John Wiley & Sons. This book was released on 2011-11-17 with total page 544 pages. Available in PDF, EPUB and Kindle. Book excerpt: A concise, robust introduction to the various topics covered by the discipline of forensic chemistry The Forensic Chemistry Handbook focuses on topics in each of the major chemistry-related areas of forensic science. With chapter authors that span the forensic chemistry field, this book exposes readers to the state of the art on subjects such as serology (including blood, semen, and saliva), DNA/molecular biology, explosives and ballistics, toxicology, pharmacology, instrumental analysis, arson investigation, and various other types of chemical residue analysis. In addition, the Forensic Chemistry Handbook: Covers forensic chemistry in a clear, concise, and authoritative way Brings together in one volume the key topics in forensics where chemistry plays an important role, such as blood analysis, drug analysis, urine analysis, and DNA analysis Explains how to use analytical instruments to analyze crime scene evidence Contains numerous charts, illustrations, graphs, and tables to give quick access to pertinent information Media focus on high-profile trials like those of Scott Peterson or Kobe Bryant have peaked a growing interest in the fascinating subject of forensic chemistry. For those readers who want to understand the mechanisms of reactions used in laboratories to piece together crime scenes—and to fully grasp the chemistry behind it—this book is a must-have.

Handbook of Solid Phase Microextraction

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Publisher : Elsevier
ISBN 13 : 0123914493
Total Pages : 497 pages
Book Rating : 4.1/5 (239 download)

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Book Synopsis Handbook of Solid Phase Microextraction by : Janusz Pawliszyn

Download or read book Handbook of Solid Phase Microextraction written by Janusz Pawliszyn and published by Elsevier. This book was released on 2011-12-01 with total page 497 pages. Available in PDF, EPUB and Kindle. Book excerpt: The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner

Strengthening Forensic Science in the United States

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Publisher : National Academies Press
ISBN 13 : 0309142393
Total Pages : 348 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Strengthening Forensic Science in the United States by : National Research Council

Download or read book Strengthening Forensic Science in the United States written by National Research Council and published by National Academies Press. This book was released on 2009-07-29 with total page 348 pages. Available in PDF, EPUB and Kindle. Book excerpt: Scores of talented and dedicated people serve the forensic science community, performing vitally important work. However, they are often constrained by lack of adequate resources, sound policies, and national support. It is clear that change and advancements, both systematic and scientific, are needed in a number of forensic science disciplines to ensure the reliability of work, establish enforceable standards, and promote best practices with consistent application. Strengthening Forensic Science in the United States: A Path Forward provides a detailed plan for addressing these needs and suggests the creation of a new government entity, the National Institute of Forensic Science, to establish and enforce standards within the forensic science community. The benefits of improving and regulating the forensic science disciplines are clear: assisting law enforcement officials, enhancing homeland security, and reducing the risk of wrongful conviction and exoneration. Strengthening Forensic Science in the United States gives a full account of what is needed to advance the forensic science disciplines, including upgrading of systems and organizational structures, better training, widespread adoption of uniform and enforceable best practices, and mandatory certification and accreditation programs. While this book provides an essential call-to-action for congress and policy makers, it also serves as a vital tool for law enforcement agencies, criminal prosecutors and attorneys, and forensic science educators.

Indoor Environment

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Publisher : John Wiley & Sons
ISBN 13 : 3527609202
Total Pages : 467 pages
Book Rating : 4.5/5 (276 download)

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Book Synopsis Indoor Environment by : Lidia Morawska

Download or read book Indoor Environment written by Lidia Morawska and published by John Wiley & Sons. This book was released on 2006-12-13 with total page 467 pages. Available in PDF, EPUB and Kindle. Book excerpt: Covering the fundamentals of air-borne particles and settled dust in the indoor environment, this handy reference investigates: * relevant definitions and terminology, * characteristics, * sources, * sampling techniques and instrumentation, * exposure assessment, * monitoring methods. The result is a useful and comprehensive overview for chemists, physicists and biologists, postgraduate students, medical practitioners, occupational health professionals, building owners and managers, building, construction and air-conditioning engineers, architects, environmental lawyers, government and regulatory professionals.

Technology in Forensic Science

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Publisher : John Wiley & Sons
ISBN 13 : 3527347623
Total Pages : 412 pages
Book Rating : 4.5/5 (273 download)

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Book Synopsis Technology in Forensic Science by : Deepak Rawtani

Download or read book Technology in Forensic Science written by Deepak Rawtani and published by John Wiley & Sons. This book was released on 2020-11-02 with total page 412 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book "Technology in Forensic Science" provides an integrated approach by reviewing the usage of modern forensic tools as well as the methods for interpretation of the results. Starting with best practices on sample taking, the book then reviews analytical methods such as high-resolution microscopy and chromatography, biometric approaches, and advanced sensor technology as well as emerging technologies such as nanotechnology and taggant technology. It concludes with an outlook to emerging methods such as AI-based approaches to forensic investigations.

Drugs and Poisons in Humans

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Publisher : Springer Science & Business Media
ISBN 13 : 3540275797
Total Pages : 653 pages
Book Rating : 4.5/5 (42 download)

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Book Synopsis Drugs and Poisons in Humans by : Osamu Suzuki

Download or read book Drugs and Poisons in Humans written by Osamu Suzuki and published by Springer Science & Business Media. This book was released on 2006-01-16 with total page 653 pages. Available in PDF, EPUB and Kindle. Book excerpt: Unique analysis of drugs and poisons to facilitate testing in all laboratories even by inexperienced chemists Includes source of chemicals needed for the experiments Texts are composed by 67 experts in analyzing the respective compounds Clear and uniform structure of chapters for ease of reading The text is illustrated by many diagrams and tables

Gas Chromatography In Forensic Science

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Publisher : CRC Press
ISBN 13 : 0203016416
Total Pages : 198 pages
Book Rating : 4.2/5 (3 download)

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Book Synopsis Gas Chromatography In Forensic Science by : Ian Tebbett

Download or read book Gas Chromatography In Forensic Science written by Ian Tebbett and published by CRC Press. This book was released on 1992-10-31 with total page 198 pages. Available in PDF, EPUB and Kindle. Book excerpt: Describes the application of gas chromatography to various aspects of forensic chemistry. Following an introduction to the basic theory of chromatographic separations, the text discusses specific issues, such as drug analysis, fires and explosives, alcohol and toxicology.

Clarke's Analytical Forensic Toxicology

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Publisher : Pharmaceutical Press
ISBN 13 : 0857110543
Total Pages : 657 pages
Book Rating : 4.8/5 (571 download)

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Book Synopsis Clarke's Analytical Forensic Toxicology by : Gail Cooper

Download or read book Clarke's Analytical Forensic Toxicology written by Gail Cooper and published by Pharmaceutical Press. This book was released on 2013-05-28 with total page 657 pages. Available in PDF, EPUB and Kindle. Book excerpt: This invaluable textbook, written by international experts, covers all the main elements of forensic toxicology and analytical toxicology techniques as well as the important parts of pharmacokinetics, drug metabolism, and pharmacology in general, with a particular focus on drugs of abuse.

Forensic Analysis of Fire Debris and Explosives

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Publisher : Springer Nature
ISBN 13 : 3030258343
Total Pages : 356 pages
Book Rating : 4.0/5 (32 download)

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Book Synopsis Forensic Analysis of Fire Debris and Explosives by : Kenyon Evans-Nguyen

Download or read book Forensic Analysis of Fire Debris and Explosives written by Kenyon Evans-Nguyen and published by Springer Nature. This book was released on 2019-10-08 with total page 356 pages. Available in PDF, EPUB and Kindle. Book excerpt: This text provides training on the fundamental tools and methodologies used in active forensic laboratories for the complicated analysis of fire debris and explosives evidence. It is intended to serve as a gateway for students and transitioning forensic science or chemistry professionals. The book is divided between the two disciplines of fire debris and explosives, with a final pair of chapters devoted to the interplay between the two disciplines and with other disciplines, such as DNA and fingerprint analysis. It brings together a multi-national group of technical experts, ranging from academic researchers to active practitioners, including members of some of the premier forensic agencies of the world. Readers will gain knowledge of practical methods of analysis and will develop a strong foundation for laboratory work in forensic chemistry. End-of-chapter questions based on relevant topics and real-world data provide a realistic arena for learners to test newly-acquired techniques.

Investigating Chemistry

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Publisher : Macmillan
ISBN 13 : 1429209895
Total Pages : 508 pages
Book Rating : 4.4/5 (292 download)

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Book Synopsis Investigating Chemistry by : Matthew Johll

Download or read book Investigating Chemistry written by Matthew Johll and published by Macmillan. This book was released on 2008-12-22 with total page 508 pages. Available in PDF, EPUB and Kindle. Book excerpt: In its new second edition, Investigating Chemistry: A Forensic Science Perspective remains the only book that uses the inherently fascinating topics of crime and criminal investigations as a context for teaching the fundamental chemical concepts most often covered in an introductory nonmajors course. Covering all the standard topics, Matthew Johll capitalizes on the surge of interest in the scientific investigation of crime (as sparked by CSI and other television shows), bringing together the theme of forensic science and the fundamentals of chemistry in ways that are effective and accessible for students. This edition features refined explanations of the chemical concepts, which are the core of the book, as well as a more thoroughly integrated forensic theme, updated features, and an expanded media/supplements package.

Technologies underlying weapons of mass destruction

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Publisher : DIANE Publishing
ISBN 13 : 1428921109
Total Pages : 266 pages
Book Rating : 4.4/5 (289 download)

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Book Synopsis Technologies underlying weapons of mass destruction by :

Download or read book Technologies underlying weapons of mass destruction written by and published by DIANE Publishing. This book was released on with total page 266 pages. Available in PDF, EPUB and Kindle. Book excerpt:

LC-MS in Drug Analysis

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Publisher : Humana Press
ISBN 13 : 9781617799334
Total Pages : 0 pages
Book Rating : 4.7/5 (993 download)

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Book Synopsis LC-MS in Drug Analysis by : Loralie J. Langman

Download or read book LC-MS in Drug Analysis written by Loralie J. Langman and published by Humana Press. This book was released on 2012-07-06 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Liquid-Chromatography-Mass-Spectrometry procedures have been shown to be successful when applied to drug development and analysis. LC-MS in Drug Analysis: Methods and Protocols provides detailed LC-MS/MS procedures for the analysis of several compounds of clinical significance. The first chapters provide the reader with an overview of mass spectroscopy, its place in clinical practice, its application of MS to TDM and toxicology, and the merits of LC-MS(/MS) and new sample preparation techniques. The following chapters discuss different approaches to screening for drugs of abuse and for general unknowns, as well as targeted measurement of specific analytes or classes of analytes including abused drugs, toxic compounds, and therapeutic agents. Written in the successful Methods in Molecular BiologyTM series format, chapters include introductions to their respective topics, lists of the necessary materials and reagents, step-by-step, readily reproducible protocols, and notes on troubleshooting and avoiding known pitfalls. Authoritative and easily accessible, LC-MS in Drug Analysis: Methods and Protocols seeks to serve both professionals and novices with its well-honed methodologies.