Influence Of Phosphoric Acid Surface Treatment On Shear Bond Strength Durability Of Resin Cement To Zirconia Base Ceramic Conditioned With Different Primers

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Influence of Phosphoric Acid Surface Treatment on Shear Bond Strength Durability of Resin Cement to Zirconia-base Ceramic Conditioned with Different Primers

Author : Eman Zuhair Alshehri
Publisher :
ISBN 13 :
Total Pages : 75 pages
Book Rating : 4.:/5 (923 download)

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Book Synopsis Influence of Phosphoric Acid Surface Treatment on Shear Bond Strength Durability of Resin Cement to Zirconia-base Ceramic Conditioned with Different Primers by : Eman Zuhair Alshehri

Download or read book Influence of Phosphoric Acid Surface Treatment on Shear Bond Strength Durability of Resin Cement to Zirconia-base Ceramic Conditioned with Different Primers written by Eman Zuhair Alshehri and published by . This book was released on 2015 with total page 75 pages. Available in PDF, EPUB and Kindle. Book excerpt: BACKGROUND: Phosphoric acid treatment has been reported to be relevant for zirconia cleaning after contamination. However, its interaction with different primers is not well known and needs to be investigated. OBJECTIVES: To compare the shear bond strengths (SBS) of resin cement to Y-TZP after phosphoric acid pretreatment and different chemical conditioning protocols, and to test the durability of SBSs after long term storage and thermal cycling conditions. To investigate the effect of phosphoric acid 75 on the surface roughness of a yttrium-stabilized tetragonal zirconia polycrystal ceramic (Y-TZP). METHODS: Sixty bars of zirconia (30 X 5 X 2 mm) were polished and glued to acrylic tubes. Each bar received 3 different surface treatments (control, phosphoric acid and air-abrasion). The bars were randomly assigned into five groups according to different primers applied (No primer, Clearfil ceramic primer, Monobond Plus, Z-prime plus and AZ primer). After that, resin cement was mixed, injected into a mold, and light cured. The specimens were tested in shear on a universal testing machine. Half of the specimens were tested after 24 h water storage and the other half were tested after 90 days of water storage and thermocycling. Non-contact profilometer was used to assess the effect of the three surface pretreatments on surface roughness of zirconia. Mode of failure and surface roughness were evaluated with SEM. Statistical analyses were conducted with mixed-model ANOVA and chi-square tests. RESULTS: The results indicated that Monobond Plus primer showed higher SBS after phosphoric acid treatment compared to other primers used. SBS of all air abrasion groups were higher than phosphoric acid groups. Long term water storage and thermocycling led to a statistically significant decrease in SBS for all groups except Monobond Plus, Z-prime plus and AZ primer after air abrasion treatment. Surface roughness measurements showed no significant differences among the surface treatments. CONCLUSION: Monobond Plus provided the highest SBS to zirconia after phosphoric acid treatment. The findings suggest that the air abrasion is the best surface treatment after contamination of zirconia surface. Monobond Plus, Z-prime plus and AZ primer showed durable SBS after air abrasion treatment and aging process.

Cumulated Index Medicus

Author :
Publisher :
ISBN 13 :
Total Pages : 1576 pages
Book Rating : 4.:/5 (31 download)

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Book Synopsis Cumulated Index Medicus by :

Download or read book Cumulated Index Medicus written by and published by . This book was released on 1995 with total page 1576 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Some Surface Treatments for Improving the Durability of Zirconia-Based Restorations

Author : Dan Liu
Publisher :
ISBN 13 : 9781361353905
Total Pages : pages
Book Rating : 4.3/5 (539 download)

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Book Synopsis Some Surface Treatments for Improving the Durability of Zirconia-Based Restorations by : Dan Liu

Download or read book Some Surface Treatments for Improving the Durability of Zirconia-Based Restorations written by Dan Liu and published by . This book was released on 2017-01-27 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This dissertation, "Some Surface Treatments for Improving the Durability of Zirconia-based Restorations" by Dan, Liu, 刘丹, was obtained from The University of Hong Kong (Pokfulam, Hong Kong) and is being sold pursuant to Creative Commons: Attribution 3.0 Hong Kong License. The content of this dissertation has not been altered in any way. We have altered the formatting in order to facilitate the ease of printing and reading of the dissertation. All rights not granted by the above license are retained by the author. Abstract: Zirconia has now been increasingly used in modern dental prosthetic practice due to its high mechanical strength, good esthetics, and excellent biocompatibility. However, the application of zirconia-based dental restorations is still constrained by its chemical inertness and the resultant relatively weak bonding properties, including porcelain to zirconia bonding, and resin to zirconia bonding. Therefore, many investigations have been carried out on the development of an effective method of surface modification on zirconia for improving its bonding ability. The aim of this laboratory study was to evaluate the effects of some new modified surface treatments on the adhesion durability of dental zirconia prosthetic system. In Part I and Part II, the application of laser surface treatment was examined. Laser energy was utilized and applied on zirconia surface before porcelain veneering procedure. Its influence on porcelain zirconia integration interface was mechanically tested and compared with sandblasting treatment. The changes in porcelain zirconia shear bond strength and mechanical strength values of zirconia with the modulation of output energy were recorded. In Part III and Part IV, several types of coating treatment, such as tribochemical approach, silica powder coating, and zirconium silicate coating, were compared with their effects on resin zirconia bonding. The changes in resin zirconia shear bond strength under different aging conditions were observed. The elemental analysis was also performed for clarifying the chemical composition of zirconia surface. The application of laser produced a flake-like micro-retentive structure on zirconia surface. Laser irradiation with the output energy higher than 11.3 W/cm2 was effective in increasing porcelain to zirconia bond strength values. The biaxial flexural strength of zirconia was not significantly affected by laser irradiation with the settings in this study. However, most of the laser treatments still demonstrated slightly lower flexural strength values compared with the control group. No changes in crystalline structure were detected after laser treatment with X-ray Diffraction (XRD) technique. Resin to zirconia shear bond strength was significantly increased after surface coatings. Without surface treatment the bonding between resin and zirconia was susceptible to artificial aging effects. Zirconia and silica-coating groups demonstrated the highest resistance to hydrolytic influence. On the other hand, the chemical changes of zirconia surface were still in need of clarification. It was concluded that porcelain zirconia bonding could be effectively enhanced by applying both sandblasting and a new laser irradiation approach. Laser irradiation might be a potential approach as a surface treatment for improving the quality of porcelain zirconia bonding interface. The strong and reliable resin zirconia integration could not be achieved without appropriate surface pre-treatment. This coating treatment is a promising approach for strengthening resin to zirconia adhesion. DOI: 10.5353/th_b5223979 Subjects: Zirconium oxide Dental materials

Influence of Saliva Contamination on Resin Bond Durability to Zirconia - Effect of Cleaning Methods

Author : Dhara Patel
Publisher :
ISBN 13 :
Total Pages : 60 pages
Book Rating : 4.:/5 (927 download)

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Book Synopsis Influence of Saliva Contamination on Resin Bond Durability to Zirconia - Effect of Cleaning Methods by : Dhara Patel

Download or read book Influence of Saliva Contamination on Resin Bond Durability to Zirconia - Effect of Cleaning Methods written by Dhara Patel and published by . This book was released on 2015 with total page 60 pages. Available in PDF, EPUB and Kindle. Book excerpt: Background and Rationale: As compared with glass-based ceramics, zirconia has gained considerable popularity in restorative dentistry due to its superior mechanical properties. Clinically, however, zirconia ceramics pose a significant challenge regarding the achievement of a reliable and durable bond to resin-based cements. Thus far, it has been established that zirconia bond to resin-based cements can be enhanced after different surface conditioning methods, such as airborne particle abrasion with aluminum oxide particles. Meanwhile, another major issue pertaining to bonding of ceramic restorations is related to its potential contamination before cementation. Briefly, after sandblasting and clinical try-in procedures, zirconia can be contaminated with saliva and/or blood. As with many metals, zirconium shows a strong affinity towards the phosphate group found in saliva and other fluids, which reacts with the zirconia surface and makes bonding very difficult. Recently, a new cleaning agent called Ivoclean (Ivoclar-Vivadent), which is an alkaline suspension of zirconium oxide particles, has been introduced in the market to remove contamination from zirconia in an effort to improve bonding to resin cements. Objective: The purpose of this study was to evaluate the influence of saliva contamination and the effect of several cleaning methods, including Ivoclean on resin bond strength to zirconia. Materials and Methods: Eighty square-shaped specimens (phi = 12 mm x 12 mm x 3 mm) of yttria-stabilized full-contour zirconia (Diazir, Ivoclar-Vivadent, Amherst, NY) were sectioned from zirconia blocks using a water-cooled diamond blade. Then, these specimens were embedded in acrylic resin, and their surfaces gradually finished with silicon carbide papers (600 grit to 1200 grit). The prepared zirconia surfaces were sandblasted with 50-microm aluminum oxide particles for 15 s, under 2.5 bars and from distance of 10 mm. After sandblasting the specimens were cleaned in an ultrasonic bath containing distilled water for 5 min and air-dried for 10s. All samples were equally divided into 4 groups (n = 20) according to the cleaning method. Airborne particle abraded specimens without contamination was served as the control group. Remaining groups were contaminated with saliva, and subjected to different cleaning protocols, namely: Ivoclean, 70% isopropanol, and no treatment. Two resin cement buttons (Multilink - Ivoclar-Vivadent, Amherst, NY) were built over each zirconia surface and light-cured following the manufacturer recommendations. The influence of contamination and surface cleaning methods on ceramic bond durability were examined after 24 h on half of the samples in each group (n = 10, n = 20), and the other half (n = 10, n = 20) specimens will undergo 6000 thermocycles (TC) before shear bond testing in the universal testing machine. Conclusion of Expected Outcomes: The shear bond strength of resin cement to zirconia led to a significant improvement after cleaning with Ivoclean both immediately and after thermal aging.

Shear Bond Strength Of Zirconia

Author : Deepak Thomas
Publisher : LAP Lambert Academic Publishing
ISBN 13 : 9783659475511
Total Pages : 52 pages
Book Rating : 4.4/5 (755 download)

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Book Synopsis Shear Bond Strength Of Zirconia by : Deepak Thomas

Download or read book Shear Bond Strength Of Zirconia written by Deepak Thomas and published by LAP Lambert Academic Publishing. This book was released on 2014-06-18 with total page 52 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book evaluated the shear bond strength of zirconia bonded to dentin specimens using a self etch dual cure resin cement after various surface treatments of zirconia. Twenty zirconia rods (3 9 2.5 mm) were prepared from zirconia blocks and assigned into 5 groups for the following surface treatments. (1) Group I: Control (C) no treatment (2) Group II: airborne-particle abrasion (APA), (3) Group III: hydrofluoric acid etching (HF), (4) Group IV: hydrofluoric acid etching followed by silanation (HF/S), and (5) Group V: application of zirconia primer(Z). Dentin Specimens were prepared from extracted molars stored in 0.5% chloramine-T. Zirconia rods were bonded to dentin using resin cement (Multilink Speed), then light polymerized. The specimens tested for failure were tested using the notched shear bond test method in a universal loading apparatus. One way ANOVA followed by Tukey HSD for cell means were used to analyze the data(=0.05). The highest values were obtained with group V (Z) (8.66 MPa) followed by group II (APA) (6.71 MPa), and group IV (HF/S) (4.41 MPa). The least values were obtained for group III (HF) (3.88 MPa) with no significant difference (P value 0.53) between grou

Exploring the Role of Zirconia Surface Treatments on the Properties and the Material's Bonding to Resin Cement

Author : Mahmood Abu Ruja'
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (133 download)

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Book Synopsis Exploring the Role of Zirconia Surface Treatments on the Properties and the Material's Bonding to Resin Cement by : Mahmood Abu Ruja'

Download or read book Exploring the Role of Zirconia Surface Treatments on the Properties and the Material's Bonding to Resin Cement written by Mahmood Abu Ruja' and published by . This book was released on 2019 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Objectives: 1. To evaluate the bond strength of yttria-tetragonal zirconia polycrystalline (Y-TZP), lithium-disilicate, and feldspathic ceramics to 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing and non-MDP resin cements. 2. To evaluate the effect of ultrashort-pulse laser (UPL) on surface treatment on Y-TZP surface properties, the material's bond strength to resin cement, and the effect of thermal stress on bond strength. Methods: Lithium-disilicate (LD), feldspathic porcelain (FP), and Y-TZP blocks received surface treatment according to the manufacturer recommendations (LD and FP: hydrofluoric acid, Y-TZP: alumina-blasting), and were luted to human dentin using MDP-containing (UL) or non-MDP adhesive system (UN). Specimens were microtensile tested. Fully-sintered Y-TZP received either no treatment (CTL) or one treatment of: ALB, SIL, or UPL. UPL consisted of either dots (LSD) or lines (LSL) patterns. Surface roughness, contact angle, and crystalline phases were evaluated. Y-TZP were cemented to composite using resin-based cement combined with a silane and MDP-containing adhesive. Specimens were incubated for 48 hours, then microtensile tested directly or after thermocycling. Results: The type of ceramic and the resin cement both had significant effects on bond strength (P≤.001). Y-TZP showed significantly lower bond strength (p.

Effect of Surface Treatments on Resin-Zirconia Bonding

Author : Fung Yan
Publisher :
ISBN 13 : 9781361026229
Total Pages : pages
Book Rating : 4.0/5 (262 download)

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Book Synopsis Effect of Surface Treatments on Resin-Zirconia Bonding by : Fung Yan

Download or read book Effect of Surface Treatments on Resin-Zirconia Bonding written by Fung Yan and published by . This book was released on 2017-01-26 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This dissertation, "Effect of Surface Treatments on Resin-zirconia Bonding" by Fung, Yan, 忻峰, was obtained from The University of Hong Kong (Pokfulam, Hong Kong) and is being sold pursuant to Creative Commons: Attribution 3.0 Hong Kong License. The content of this dissertation has not been altered in any way. We have altered the formatting in order to facilitate the ease of printing and reading of the dissertation. All rights not granted by the above license are retained by the author. Abstract: Zirconia offers a favorable choice for esthetic indirect dental restorations with excellent mechanical properties and biocompatibility. In the hostile oral environment, the longevity of dental restorations relies heavily on whether a strong and stable bond between the restoration and underlying supporting tooth structures can be achieved. However, unlike conventional ceramics, zirconia is a chemically inert material which makes it notoriously difficult to bond with any dental composite resin cement. This thesis aimed at developing and evaluating different zirconia surface pretreatments for improving the resin-zirconia bonding. The first laboratory experiment evaluated the effect of Er, Cr: YSGG laser treatment on topographic changes of zirconia surface. Laser parameters including power, irradiation time and water spray at different levels were tested and the treated zirconia surfaces were assessed by scanning electron microscope (SEM) and atomic force microscope (AFM). Results showed that all three tested laser parameters could affect the topographic changes of zirconia surface. Significant topographic changes were found when the power was set at 3.0 W with 50% water spray for 120 s or the power was set at 4.0 W with 75% water spray for 60 s. The second experiment evaluated the effects of grit-blasting (sandblasting), selective infiltration etching (SIE), 3.0 W and 4.0 W laser zirconia surface treatments on the resin-zirconia bonding. Resin composite was bonded to the treated zirconia which was then sectioned into resin-zirconia micro-beams of a standard size. Microtensile bond strength (MTBS) tests were performed for adhesion strength testing. In dry storage conditions, SIE, grit-blasting and 3.0 W laser groups showed significantly higher MTBSs than the control group while no difference in MTBSs was found between the 4.0 W laser group and the control group. After water storage, SIE treatment showed significant higher MTBSs than the remaining groups. MTBSs of water storage specimens were significantly less than the dry specimens except the ones in 4.0 W groups. Zirconia surface treatments could enhance the resin-zirconia bonding in dry storage conditions. The SIE treatment appeared to provide the strongest resin-zirconia adhesion despite hydrolytic degradation. The third experiment evaluated the fatigue performance of resin-zirconia bonding with different surface treatments. Resin-zirconia beams were prepared and loaded at 36 N with 1.5 Hz frequency for 104 cycles at room temperature, before sectioned for MTBS tests. In dry storage conditions, SIE and grit-blasting groups showed significantly higher MTBSs than the control group while no differences in MTBSs were found among the 3.0 W, 4.0 W and control groups. After fatigue loading, only the SIE and 3.0 W groups showed significantly lower MTBSs while the other groups did not. After water storage, MTBSs of water storage specimens were significantly less than the dry specimens except the ones in SIE and 4.0 W groups. No significant differences in MTBSs were found in all groups after fatigue loading. The SIE group showed significantly higher MTBSs than the other study groups after water storage and fatigue loading. In general, it could be concluded that water and cyclic fatigue environment could affect the resin-zirconia bonding. Subjects: Dental resins Dental bonding Surface treatments Zirconium oxide

Effect of Phosphoric Acid Etching Prior to Application of Self-etching Primer (SEP) on Shear Bond Strenght

Author : Grace Shao-Chiu Chen
Publisher :
ISBN 13 :
Total Pages : 40 pages
Book Rating : 4.:/5 (795 download)

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Book Synopsis Effect of Phosphoric Acid Etching Prior to Application of Self-etching Primer (SEP) on Shear Bond Strenght by : Grace Shao-Chiu Chen

Download or read book Effect of Phosphoric Acid Etching Prior to Application of Self-etching Primer (SEP) on Shear Bond Strenght written by Grace Shao-Chiu Chen and published by . This book was released on 2010 with total page 40 pages. Available in PDF, EPUB and Kindle. Book excerpt: INTRODUCTION: The objective of this study was to determine the effect of phosphoric acid etching prior to application of self-etching primer on orthodontic bonding in terms of shear bond strength and the adhesive remnant on the enamel surface at debonding. METHODS: Fifty-one extracted human premolars were pumiced, rinsed, dried, and then subjected to three different treatments: Group 1: no phosphoric acid etching + Transbond Plus SEP; Group 2: 15-second etching with 37% phosphoric acid + rinsed + dried + Transbond Plus SEP; Group 3: 30-second etching with 37% phosphoric acid + rinsed + dried + Transbond Plus SEP. Precoated metal brackets (3M Unitek, APC Plus, Victory brackets) were then bonded following the manufacturer's recommendation. An Instron Universal Testing Machine was used to test shear bond strength (SBS) at a crosshead speed of 0.5 mm/min. Adhesive remnant index (ARI) was assigned to all specimens under a 16 times magnification using a light microscope. RESULTS: One-way repeated measured analysis of variance test (ANOVA) revealed no significant differences in shear bond strength among all three groups. Kruskal Wallis test revealed that there was a significant difference in ARI score between Group 1 when compared to Groups 2 and 3. Two-way analysis of variance was used to examine any statistical difference in frequency of enamel fracture craters among the three groups. CONCLUSION: There was no statistical difference in shear bond strength between the three groups. Most specimens demonstrated adequate shear bond strength (>/= 6 MPa) for routine clinical application. Etching enamel with phosphoric acid prior to the use of Transbond Plus SEP resulted in more adhesive remaining on the enamel surface. The removal of this excess surface cement may lead to increased enamel loss during post debonding clean up.

Influence of Surface Treatment on Veneering Porcelain Shear Bond Strength to Zirconia After Cyclic Loading

Author : Atsushi Nishigori
Publisher :
ISBN 13 :
Total Pages : 134 pages
Book Rating : 4.:/5 (111 download)

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Book Synopsis Influence of Surface Treatment on Veneering Porcelain Shear Bond Strength to Zirconia After Cyclic Loading by : Atsushi Nishigori

Download or read book Influence of Surface Treatment on Veneering Porcelain Shear Bond Strength to Zirconia After Cyclic Loading written by Atsushi Nishigori and published by . This book was released on 2013 with total page 134 pages. Available in PDF, EPUB and Kindle. Book excerpt: Statement of problem: Yttria-partially stabilized tetragonal zirconia polycrystal (Y-TZP) all-ceramic restorations have been reported to suffer from chipping or cracking of the veneering porcelain (VP) as the most common complication. There is little information in the literature regarding the influence of surface treatment on VP shear bond strength to Y-TZP after cyclic loading. Purpose of this study: The goals of this study were (1) to investigate the influence of zirconia surface treatments on veneering porcelain shear bond strength and (2) to investigate the influence of cyclic loading on the shear bond strength between VP and Y-TZP. Materials and Methods: 48 cylinder-shaped specimens (6mm in diameter and 4mm in height) were divided into 4 groups containing 12 specimens each according to the surface treatment. As a control group (C), no further treatment was applied to the specimens after grinding. Group H was heat-treated as a pretreatment according to the manufacturer's recommendations. Group S was airborne-particle abraded with 50 μm alumina (Al2O3) particles under a pressure of 0.4 MPa for 10 seconds. In the group SH, the heat-treatment was performed after the airborne-particle abrasion. A VP cylinder (2.4 mm in diameter and 2 mm in height) was applied and fired on the prepared Y-TZP specimens. The shear bond strength was tested using a universal testing machine. Six specimens from each group were subjected to fatigue (10,000cycles, 1.5Hz, 10N load) before testing. Results: The 3-way ANOVA showed no statistically significant effect of surface treatment and cyclic loading on shear bond strength. The highest mean shear bond strength was recorded for the air-particle abrasion group without cyclic loading (34.1 + 10 MPa). The lowest mean shear bond strength was the air-particle abrasion group with cyclic loading (10.7 ± 15.4 MPa). Sidak multiple comparisons procedure demonstrated cyclic loading specimens had significantly lower shear bond strength than non-cyclic loading specimens after air-particle abrasion without heat treatment (p=0.0126) Conclusion: Within the limitations of this study, (1) Shear bond strength between Y-TZP and VP is not affected statistically by surface treatment using heat treatment, airborne-particle abrasion, and heat treatment after airborne-particle abrasion. (2) There is significant difference in shear bond strength with air-particle abrasion between with and without cyclic loading groups. This difference suggested that air-particle abrasion should be avoided in clinical situations as a surface treatment without heat treatment.

Effect of Different Surface Treatments on the Shear Bond Strength of Lithium Disilicate Ceramic

Author : Mai Almujel
Publisher :
ISBN 13 :
Total Pages : 34 pages
Book Rating : 4.:/5 (891 download)

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Book Synopsis Effect of Different Surface Treatments on the Shear Bond Strength of Lithium Disilicate Ceramic by : Mai Almujel

Download or read book Effect of Different Surface Treatments on the Shear Bond Strength of Lithium Disilicate Ceramic written by Mai Almujel and published by . This book was released on 2013 with total page 34 pages. Available in PDF, EPUB and Kindle. Book excerpt: Statement of problem: During clinical try-in, it is almost inevitable that the fitting surfaces of a lithium disilicate ceramic fixed prosthesis be contaminated with saliva and silicone disclosing medium. Purpose: This in vitro study used a shear bond strength (SBS) test to evaluate the effect of saliva and silicone disclosing medium contamination on the adhesive luting material bond to porcelain, and the effectiveness of various materials used to remove such contamination. Hypothesis: The resin-ceramic bond strength and its durability are related to ceramic surface contamination and subsequent surface treatment. Material and methods: Ninety ceramic specimens were milled from lithium disilicate blocks using an electrical high precision saw, crystallized, and then randomly assigned into six groups (n=15). Excluding the control group, each group underwent contamination with saliva and silicon disclosing medium, then received a different surface cleaning treatment. After bonding and thermocycling, shear bond strength values were measured on an Instron machine. Fracture modes were determined by examination with a scanning electron microscope. Results: Salivary contamination of porcelain surfaces significantly reduced the resin cement-to-porcelain bond compared to the control (P

Effect of Primer on the Bond Strength of Resin Cement to Zirconium Oxide Ceramic

Author : Glena Patricia Millan
Publisher :
ISBN 13 :
Total Pages : 132 pages
Book Rating : 4.:/5 (752 download)

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Book Synopsis Effect of Primer on the Bond Strength of Resin Cement to Zirconium Oxide Ceramic by : Glena Patricia Millan

Download or read book Effect of Primer on the Bond Strength of Resin Cement to Zirconium Oxide Ceramic written by Glena Patricia Millan and published by . This book was released on 2010 with total page 132 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Assessment of the Bond Strength Between Resin Cement and Lithium Disilicate Based Glass Ceramics with Different Chemical Composition and Surface Treatments

Download Assessment of the Bond Strength Between Resin Cement and Lithium Disilicate Based Glass Ceramics with Different Chemical Composition and Surface Treatments PDF Online Free

Author : Muna Jr Bebsh
Publisher :
ISBN 13 :
Total Pages : 0 pages
Book Rating : 4.:/5 (135 download)

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Book Synopsis Assessment of the Bond Strength Between Resin Cement and Lithium Disilicate Based Glass Ceramics with Different Chemical Composition and Surface Treatments by : Muna Jr Bebsh

Download or read book Assessment of the Bond Strength Between Resin Cement and Lithium Disilicate Based Glass Ceramics with Different Chemical Composition and Surface Treatments written by Muna Jr Bebsh and published by . This book was released on 2018 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Objective: The purpose of this research project is to evaluate and compare the effect of different surface treatments on surface properties. Also the effect of different surface treatments with silane coupling agents on the bond strengths between resin cement and four CAD/CAM lithium disilicate-based glass ceramics (LDGC). Materials and methods: This study had three levels of analyses. Part I: The physicochemical analyses of four CAD/CAM LDGC surfaces. The surface physicochemical compositions of the four LDGC products (e.max CAD, Vita Suprinity, Celtra Duo, n!ce) were analyzed using X-ray photoelectron spectroscopy (XPS). In addition, scanning electron microscopy (SEM) was used to analyze the microstructure of LDGC. Part II: The effect of different surface treatments on the micromorphology and the roughness of four CAD/CAM lithium disilicate- based glass ceramics Atomic force microscopy (AFM) was used to measure the surface roughness and scanning electron microscopy (SEM) was used to analyze the changes in the surface micromorphology. Part III: The effect of an experimental silane coupling agent (TEOS) with different surface treatments on bond strength of four CAD /CAM lithium disilicate-based glass-ceramics. The shear bond strength between the ceramic surface and resin cement was tested using shear bond testing after a 30 day storage in distilled water. Results: The chemical composition percentage on the nano surfaces of the LGGC changed after hydrofluoric acid treatment. Different surface treatments produced different values of roughness. The highest shear bond strength values were found with the use of hydrofluoric acid treatment and the combination of both hydrofluoric acid and sandblasting followed by manufacturer's recommendation of silane coupling application. Conclusion: Surface treatments and silane coupling agents play a significant role to obtain reliable bond strengths between resin cement and LDGC restorations.

Effects of Etching Duration on the Surface Roughness, Surface Loss, Flexural Strength, and Shear Bond Strength to a Resin Cement of E.max Cad Glass Ceramic

Download Effects of Etching Duration on the Surface Roughness, Surface Loss, Flexural Strength, and Shear Bond Strength to a Resin Cement of E.max Cad Glass Ceramic PDF Online Free

Author : Hanan Al-Johani
Publisher :
ISBN 13 :
Total Pages : 144 pages
Book Rating : 4.:/5 (111 download)

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Book Synopsis Effects of Etching Duration on the Surface Roughness, Surface Loss, Flexural Strength, and Shear Bond Strength to a Resin Cement of E.max Cad Glass Ceramic by : Hanan Al-Johani

Download or read book Effects of Etching Duration on the Surface Roughness, Surface Loss, Flexural Strength, and Shear Bond Strength to a Resin Cement of E.max Cad Glass Ceramic written by Hanan Al-Johani and published by . This book was released on 2017 with total page 144 pages. Available in PDF, EPUB and Kindle. Book excerpt: EFFECTS OF ETCHING DURATION ON THE SURFACE ROUGHNESS, SURFACE LOSS, FLEXURAL STRENGTH OF E. MAX CAD GLASS CERAMIC AND SHEAR BOND STRENGTH TO A RESIN CEMENT Background: Long-term retention of ceramic restorations is dependent on the bond strength of the luting resin to both the tooth and porcelain substrates. In order to achieve successful bonding, the surface of the porcelain substrate must be modified to increase the surface roughness, and this can be achieved chemically by hydrofluoric (HF) acid etching. However, prolonged HF acid etching has shown to have a weakening effect on the evaluated lithium disilicate glass-ceramics. Therefore, it is essential to quantify the required etching duration of HF acid to minimize the possible deleterious effects on ceramic strength while maximizing the bond strength to tooth structure. Objectives: To evaluate the effects of HF acid etching duration on the surface roughness, surface loss, flexural strength, and shear bond strength of IPS e.max CAD (Ivoclar Vivadent) lithium disilicate-based glass ceramic to a resin cement. Hypothesis: The differences in HF acid etching durations will not have a significant effect on the surface roughness, surface loss, flexural strength, or shear bond strength of IPS e.max CAD to a resin cement. Methods: 168 specimens were prepared from IPS e.max CAD blocks. All specimens were polished and sonically cleaned in distilled water. Specimens were fired in the vacuum pump furnace according to the manufacturer's instructions. Specimens were then divided into 4 groups, according to etching durations, then further divided into 3 subgroups, according to the properties tested. Group A was not etched (control), Groups B, C and D were etched with 5-percent HF acid (IPS Ceramic Etching gel, Ivoclar Vivadent) for 20 s, 60 s and 90 s respectively. The morphologies of both etched and non-etched surfaces in specimens of subgroup 1 of each etching group (n = 16/group) were observed under scanning electron microscopy (SEM). In addition, non-contact surface profilometry (Proscan 2000) was used to calculate the surface loss and to examine the surface roughness of the etched ceramic surfaces and roughness values (Ra, Rq) were documented for each group. Furthermore, etched specimens of subgroup 2 (n = 16/group) were silanated (Monobond Plus, Ivoclar Vivadent) and cemented with a resin cement (Multilink Automix, Ivoclar Vivadent). The shear bond strength (SBS) was measured using a universal mechanical testing machine. For each etching group, subgroup 3 specimens (n = 10/group) were loaded to failure in a three-point bending test to measure their flexural strength values using a universal mechanical testing machine. Data for surface roughness, surface loss, and flexural strength were analyzed using one-way analysis of variance (ANOVA), to identify the significant effects of different HF acid etching durations. Data for shear bond strength test were analyzed using two-way ANOVA to test the effects of etching duration, storage for 24 hours/thermocycling, and their interaction. All pair-wise comparisons from ANOVA analysis were made using Fisher's Protected Least Significant Differences to control the overall significance level at 5 percent. Results: Difference in HF etching durations did not have a significant effect on surface roughness values Ra or Rq (p = 0.3408; p = 0.3245) respectively, but had a significant effect on surface loss (p = 0.0006). SBS values were not significantly different between experimental groups (p = 0.4650); however, SBS values after 24-h storage were significantly higher than that found after thermocycling (p = 0.0166) among different etching durations. Finally, different HF etching durations did not have a significant effect on flexural strength values (p = 0.1260). Conclusion: Within the limitations of this study, different HF etching durations did not have a significant effect on surface roughness, flexural strength, or shear bond strength of IPS e.max CAD. However, the different etching durations significantly affected the surface loss of the lithium disilicate glass ceramics.

Advanced Dental Biomaterials

Author : Zohaib Khurshid
Publisher : Woodhead Publishing
ISBN 13 : 0081024770
Total Pages : 758 pages
Book Rating : 4.0/5 (81 download)

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Book Synopsis Advanced Dental Biomaterials by : Zohaib Khurshid

Download or read book Advanced Dental Biomaterials written by Zohaib Khurshid and published by Woodhead Publishing. This book was released on 2019-05-24 with total page 758 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advanced Dental Biomaterials is an invaluable reference for researchers and clinicians within the biomedical industry and academia. The book can be used by both an experienced researcher/clinician learning about other biomaterials or applications that may be applicable to their current research or as a guide for a new entrant into the field who needs to gain an understanding of the primary challenges, opportunities, most relevant biomaterials, and key applications in dentistry. Provides a comprehensive review of the materials science, engineering principles and recent advances in dental biomaterials Reviews the fundamentals of dental biomaterials and examines advanced materials’ applications for tissues regeneration and clinical dentistry Written by an international collaborative team of materials scientists, biomedical engineers, oral biologists and dental clinicians in order to provide a balanced perspective on the field

The Effect of Surface Treatments on Shear Bond Strengths of Different Resin Cements and a Composite Core Material

Author :
Publisher :
ISBN 13 :
Total Pages : 100 pages
Book Rating : 4.:/5 (946 download)

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Book Synopsis The Effect of Surface Treatments on Shear Bond Strengths of Different Resin Cements and a Composite Core Material by :

Download or read book The Effect of Surface Treatments on Shear Bond Strengths of Different Resin Cements and a Composite Core Material written by and published by . This book was released on 2014 with total page 100 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Influence of Silanes on the Shear Bond Strength of Resin Cements to Zirconia

Author : Figen Akyelken Gökkaya
Publisher :
ISBN 13 :
Total Pages : 24 pages
Book Rating : 4.:/5 (819 download)

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Book Synopsis Influence of Silanes on the Shear Bond Strength of Resin Cements to Zirconia by : Figen Akyelken Gökkaya

Download or read book Influence of Silanes on the Shear Bond Strength of Resin Cements to Zirconia written by Figen Akyelken Gökkaya and published by . This book was released on 2012 with total page 24 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Silane Coupling Agents

Author : Edwin P. Plueddemann
Publisher : Springer Science & Business Media
ISBN 13 : 1489903429
Total Pages : 238 pages
Book Rating : 4.4/5 (899 download)

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Book Synopsis Silane Coupling Agents by : Edwin P. Plueddemann

Download or read book Silane Coupling Agents written by Edwin P. Plueddemann and published by Springer Science & Business Media. This book was released on 2013-11-11 with total page 238 pages. Available in PDF, EPUB and Kindle. Book excerpt: * It has been rumored that a bumble bee has such aerodynamic deficiencies that it should be incapable of flight. Fiberglass-reinforced polymer com posites, similarly, have two (apparently) insurmountable obstacles to per formance: 1) Water can hydrolyze any conceivable bond between organic and inorganic phase, and 2) Stresses across the interface during temperature cycling (resulting from a mismatch in thermal expansion coefficients) may exceed the strength of one of the phases. Organofunctional silanes are hybrid organic-inorganic compounds that are used as coupling agents across the organic-inorganic interface to help overcome these two obstacles to composite performance. One of their functions is to use the hydrolytic action of water under equilibrium condi tions to relieve thermally induced stresses across the interface. If equilib rium conditions can be maintained, the two problems act to cancel each other out. Coupling agents are defined primarily as materials that improve the practical adhesive bond of polymer to mineral. This may involve an increase in true adhesion, but it may also involve improved wetting, rheology, and other handling properties. The coupling agent may also modify the inter phase region to strengthen the organic and inorganic boundary layers.