Hyphenated Techniques In Speciation Analysis

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Hyphenated Techniques in Speciation Analysis

Author : Ryszard Lobinski
Publisher : Royal Society of Chemistry
ISBN 13 : 1847551092
Total Pages : 234 pages
Book Rating : 4.8/5 (475 download)

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Book Synopsis Hyphenated Techniques in Speciation Analysis by : Ryszard Lobinski

Download or read book Hyphenated Techniques in Speciation Analysis written by Ryszard Lobinski and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 234 pages. Available in PDF, EPUB and Kindle. Book excerpt: Speciation analysis is a field of trace element analytical chemistry that deals with detection, identification and determination of individual chemical forms of metals and metalloids. There has been increased awareness of the importance of elemental speciation over the last 20 years and this has lead to growing demand for analytical techniques capable of providing species-specific information. Hyphenated Techniques in Speciation Analysis offers a brief but comprehensive overview of hyphenated techniques and their various applications for the determination of chemical forms of trace elements. It brings a succinct presentation of the concept of speciation analysis, gives an overview of techniques based on coupling of chromatography with element and molecule specific detection and summarises their applications in the fields of environmental and industrial chemistry, biochemistry, nutrition, toxicology and medicine. Fully referenced, Hyphenated Techniques in Speciation Analysis is an invaluable introduction to elemental speciation analysis and also provides a practising analyst with a critical overview of research carried out in the field.

Hyphenated and Alternative Methods of Detection in Chromatography

Author : R. Andrew Shalliker
Publisher : CRC Press
ISBN 13 : 1000654567
Total Pages : 311 pages
Book Rating : 4.0/5 (6 download)

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Book Synopsis Hyphenated and Alternative Methods of Detection in Chromatography by : R. Andrew Shalliker

Download or read book Hyphenated and Alternative Methods of Detection in Chromatography written by R. Andrew Shalliker and published by CRC Press. This book was released on 2011-12-14 with total page 311 pages. Available in PDF, EPUB and Kindle. Book excerpt: Widely employed for separating and detecting chemicals in solution, separation techniques are most often applied in tandem, subsequently referred to as hyphenated methods. Hyphenated and Alternative Methods of Detection in Chromatography details the development and application of mass spectral detection techniques coupled with gas phase and liquid

Liquid Chromatography

Author : B. Michalke
Publisher : Elsevier Inc. Chapters
ISBN 13 : 0128071273
Total Pages : 688 pages
Book Rating : 4.1/5 (28 download)

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Book Synopsis Liquid Chromatography by : B. Michalke

Download or read book Liquid Chromatography written by B. Michalke and published by Elsevier Inc. Chapters. This book was released on 2013-01-08 with total page 688 pages. Available in PDF, EPUB and Kindle. Book excerpt: This chapter describes strategies and methods for speciation investigations using mainly hyphenated techniques of liquid chromatography with element-specific detection. Complete speciation schemes are discussed, starting with the sources of error and problem solutions for sampling and ending with more dimensional, orthogonally chosen coupled-speciation techniques for quality controlled results. The focus in each section is directed to the specific problems being faced with respect to speciation analysis: species stability during sample storage and processing, the choice of the most suitable speciation approaches (direct methods or hyphenated techniques), species separation techniques ranging from ultrafiltration to various forms of liquid chromatography, and capillary electrophoresis, discussing their advantageous as well as their (undesired) potential of changing species. Further, problems in interfacing to element-specific detectors, mainly plasma-based detectors like ICP OES and ICP MS are reported. The chapter concludes with aspects of quality control, including sources of errors and strategies to overcome such problems, such as orthogonal speciation concepts.

Trace Metal Analysis and Speciation

Author : I.S. Krull
Publisher : Elsevier
ISBN 13 : 9780080858548
Total Pages : 301 pages
Book Rating : 4.8/5 (585 download)

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Book Synopsis Trace Metal Analysis and Speciation by : I.S. Krull

Download or read book Trace Metal Analysis and Speciation written by I.S. Krull and published by Elsevier. This book was released on 1991-10-08 with total page 301 pages. Available in PDF, EPUB and Kindle. Book excerpt: The aim of this volume is to describe the most recent advances in areas of analytical chemistry that relate to the trace determination of metals and inorganics, as well as their distribution and forms (species) present, sample dependent. Analytical approaches are described that encompass a number of separation methods, such as gas and high performance liquid chromatography, interfaced with selective and sensitive detection methods that become unique for metal species/forms present in various samples. Hyphenated techniques are emphasized, such as interfacing HPLC with plasma induced emission spectroscopy, electrochemistry, post-column reaction chemistry, etc. Each chapter describes the latest instrumental and methodology advances that utilize some form of chromatography together with element-specific detection or mass spectrometry to provide absolute identification of the specific species of a metal present in various samples. The book will be of value to those concerned with the determination of trace levels of individual metal species present or suspected present in any given sample and to those involved in trace metal toxicology, metabolism of metal-containing drugs or chemicals, environmental exposures to metals and chemical speciation of real world samples. Government regulatory laboratories striving to detect and determine absolute levels of a metal species in any regulated sample will be interested in this volume, as will academic institutes involved in environmental toxicology, environmental chemistry, metal-DNA/protein interactions and researchers working with metal species.

Elemental Speciation

Author : Joseph A. Caruso
Publisher : Elsevier Science Limited
ISBN 13 : 9780444500472
Total Pages : 581 pages
Book Rating : 4.5/5 (4 download)

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Book Synopsis Elemental Speciation by : Joseph A. Caruso

Download or read book Elemental Speciation written by Joseph A. Caruso and published by Elsevier Science Limited. This book was released on 2000 with total page 581 pages. Available in PDF, EPUB and Kindle. Book excerpt: Hardbound. This book provides a comprehensive discussion of the major aspects involved in elemental speciation. Sample preparation, separation techniques, instrumentation and quality assurance are all discussed. In addition, individual chapters are devoted to speciation of environmental samples and speciation of biological, clinical, and nutritional samples. Individual chapters are written by leaders in the field, and the book has been organized so that the reader may learn how to collect a sample and prepare it. Ways to separate and detect analytes of interest, and steps to take to ensure the validity of the measurements are also discussed. This book is unique in its comprehensive treatment of this subject.

Hyphenated and Alternative Methods of Detection in Chromatography

Author : R. Andrew Shalliker
Publisher : CRC Press
ISBN 13 : 142000848X
Total Pages : 308 pages
Book Rating : 4.4/5 (2 download)

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Book Synopsis Hyphenated and Alternative Methods of Detection in Chromatography by : R. Andrew Shalliker

Download or read book Hyphenated and Alternative Methods of Detection in Chromatography written by R. Andrew Shalliker and published by CRC Press. This book was released on 2011-12-14 with total page 308 pages. Available in PDF, EPUB and Kindle. Book excerpt: Widely employed for separating and detecting chemicals in solution, separation techniques are most often applied in tandem, subsequently referred to as hyphenated methods. Hyphenated and Alternative Methods of Detection in Chromatography details the development and application of mass spectral detection techniques coupled with gas phase and liquid

Recent Advances in Trace Elements

Author : Katarzyna Chojnacka
Publisher : John Wiley & Sons
ISBN 13 : 1119133807
Total Pages : 584 pages
Book Rating : 4.1/5 (191 download)

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Book Synopsis Recent Advances in Trace Elements by : Katarzyna Chojnacka

Download or read book Recent Advances in Trace Elements written by Katarzyna Chojnacka and published by John Wiley & Sons. This book was released on 2018-02-23 with total page 584 pages. Available in PDF, EPUB and Kindle. Book excerpt: Comprehensive and multidisciplinary presentation of the current trends in trace elements for human, animals, plants, and the environment This reference provides the latest research into the presence, characterization, and applications of trace elements and their role in humans, animals, and plants as well as their use in developing novel, functional feeds, foods, and fertilizers. It takes an interdisciplinary approach to the subject, describing the biological and industrial applications of trace elements. It covers various topics, such as the occurrence, role, and monitoring of trace elements and their characterization, as well as applications from the preliminary research to laboratory trials. Recent Advances in Trace Elements focuses on the introduction and prospects of trace elements; tackles environmental aspects such as sources of emission, methods of monitoring, and treatment/remediation processes; goes over the biological role of trace elements in plants, animals, and human organisms; and discusses the relevance of biomedical applications and commercialization. A compendium of recent knowledge in interdisciplinary trace element research Uniquely covers production and characterization of trace elements, as well as the industrial and biomedical aspects of their use Paves the way for the development of innovative products in diverse fields, including pharmaceuticals, food, environment, and materials science Edited by well-known experts in the field of trace elements with contributions from international specialists from a wide range of areas Unique in presenting comprehensive and multidisciplinary information of the key aspects of trace elements research in a digestible form, this book is essential reading for the novice and expert in the fields of environmental science, analytical chemistry, biochemistry, materials science, pharmaceutical science, nutraceutical, and pharmaceutical sciences. It is also valuable for companies that implement new products incorporating trace elements to the market.

Handbook of Elemental Speciation

Author :
Publisher : John Wiley & Sons
ISBN 13 : 0470868376
Total Pages : 670 pages
Book Rating : 4.4/5 (78 download)

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Book Synopsis Handbook of Elemental Speciation by :

Download or read book Handbook of Elemental Speciation written by and published by John Wiley & Sons. This book was released on 2004-01-09 with total page 670 pages. Available in PDF, EPUB and Kindle. Book excerpt: This international collection of chapters comprehensively covers different aspects of procedures for speciation analysis at all levels starting from sample collection and storage, through sample preparation approaches to render the species chromatographable, principles of separation techniques used in speciation analysis, to the element specific detection. International renowned editors and contributors Includes coverage of electrochemical methods, biosensors for metal ions, radioisotope techniques and direct solid speciation techniques Provides information on quality assurance and risk assessment, and speciation-relevant legislation Each chapter is a stand-alone reference covering a given facet of elemental speciation analysis written by an expert in a given field with the volume as a whole providing an excellent introductory text and reference handbook.

Speciation Studies in Soil, Sediment and Environmental Samples

Author : Sezgin Bakirdere
Publisher : CRC Press
ISBN 13 : 1466594845
Total Pages : 614 pages
Book Rating : 4.4/5 (665 download)

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Book Synopsis Speciation Studies in Soil, Sediment and Environmental Samples by : Sezgin Bakirdere

Download or read book Speciation Studies in Soil, Sediment and Environmental Samples written by Sezgin Bakirdere and published by CRC Press. This book was released on 2013-09-26 with total page 614 pages. Available in PDF, EPUB and Kindle. Book excerpt: Recent developments clearly indicate that speciation studies in biological and environmental matrices are much more important than the total element determination due to the tremendous difference in bioavailability and toxicity of various chemical forms of a particular element. Different separation-detection techniques and hyphenated systems—each with its own advantages and disadvantages with respect to precision, sensitivity and detection limit—have been developed for the identification and quantification of the species present in systems at ultra-trace levels. This book aims to evaluate the speciation analysis in depth and present a comprehensive review of state-of-the-art analytical approaches used for the speciation of elements in environmental samples.

Analytical Methods in the Determination of Bioactive Compounds and Elements in Food

Author : Magdalena Jeszka-Skowron
Publisher : Springer Nature
ISBN 13 : 303061879X
Total Pages : 380 pages
Book Rating : 4.0/5 (36 download)

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Book Synopsis Analytical Methods in the Determination of Bioactive Compounds and Elements in Food by : Magdalena Jeszka-Skowron

Download or read book Analytical Methods in the Determination of Bioactive Compounds and Elements in Food written by Magdalena Jeszka-Skowron and published by Springer Nature. This book was released on 2021-02-02 with total page 380 pages. Available in PDF, EPUB and Kindle. Book excerpt: Most bioactive compounds have antioxidant activity, particularly tocochromanols, phenolics (flavonoids and phenolic acids), methylxantines and capsaicinoids. Some of these compounds have also other properties important for human health. For example, vitamin E protects against oxidative stress, but it is also known for its “non-antioxidant” functions, including cell signalling and antiproliferation. Selenium compounds and indoleamins are the components of the antioxidant enzymes. Selenium makes vitamin E acquisition easier and controls its physiological functions. In taking part in enzymatic reactions and protecting the cell against free radicals, selenium shows immunomodulative, antiphlogistic, and antiviral activity. Capsaicinoids possess not only antioxidant, but also antibacterial, analgesic, weight-reducing and thermoregulation properties. Studies have also demonstrated their gastroprotective and anticancer properties. Analytical Methods in the Determination of Bioactive Compounds and Elements in Food explores both the influence of particular compounds on human health and the methods used for their determination. Chapters describe various aspects of food and plant analysis, including chromatographic and non‐chromatographic approaches as well as hyphenated techniques. Readers of this book will gain a comprehensive understanding of the important groups of bioactive compounds relevant to human health.

Metallomics

Author : Yasumitsu Ogra
Publisher : Springer
ISBN 13 : 4431564632
Total Pages : 364 pages
Book Rating : 4.4/5 (315 download)

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Book Synopsis Metallomics by : Yasumitsu Ogra

Download or read book Metallomics written by Yasumitsu Ogra and published by Springer. This book was released on 2017-03-01 with total page 364 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on recent topics in metallomics, a study of the metallome, or metal-containing biomolecules. Metals can induce various physiological and toxicological effects in a very small amounts, in other words, the concentrations of biometals are very low in organisms. Thus, analytical techniques for a trace amount of metal are crucial to understand the biological and toxicological functions of metals.This volume begins with an overview of metallomics including the history and development of the field. Subsequent parts provide basic and advanced techniques for metallomics. Speciation and imaging of metals are basic approaches to reveal the function of the metallome. The applications of speciation using an HPLC hyphenated with inductively coupled plasma mass spectrometry (LC-ICP-MS) and flow cytometry ICP-MS are described. As advanced approaches, the applications using a micro-flow injection-ICP-MS, an ICP-triple quadrupole mass spectrometer, an ICP-sector field mass spectrometer, and an ICP-multi-collector mass spectrometer are mentioned. For the imaging of metals, basic principles and applications of several techniques such as scanning X-ray fluorescence microscopy and ICP-MS equipped with laser ablation (LA-ICP-MS) are presented. Speciation analyses using electrospray ionization mass spectrometry (ESI-MS), X-ray Absorption Spectroscopy (XAS), and nuclear magnetic resonance spectroscopy (NMR) are also introduced. The last part highlights the medical and pharmaceutical applications of metallomics. Molecular biological approaches to reveal the effects of toxic metals, metal functions in brain and neurodegenerative diseases, and metallodrugs are explained. The topic of metal transporters is also presented.

Application of IC-MS and IC-ICP-MS in Environmental Research

Author : Rajmund Michalski
Publisher : John Wiley & Sons
ISBN 13 : 1118862007
Total Pages : 284 pages
Book Rating : 4.1/5 (188 download)

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Book Synopsis Application of IC-MS and IC-ICP-MS in Environmental Research by : Rajmund Michalski

Download or read book Application of IC-MS and IC-ICP-MS in Environmental Research written by Rajmund Michalski and published by John Wiley & Sons. This book was released on 2016-06-07 with total page 284 pages. Available in PDF, EPUB and Kindle. Book excerpt: Introduces the reader to the field of ion chromatography, species analysis and hyphenated methods IC-MS and IC-ICP-MS including the theory and theirs applications Covers the importance of species analysis and hyphenated methods in ion chromatography Includes practical applications of IC-MS and IC-ICP-MS in environmental analysis Details sample preparation methods for ion chromatography Discusses hyphenated methods IC-MS and IC-ICP-MS used in determining both the total element contents and its elements Details speciation analysis used in studying biochemical cycles of selected chemical compounds; determining toxicity and ecotoxicity of elements; food and pharmaceuticals quality control; and in technological process control and clinical analytics

Encyclopedia of Chromatography

Author : Jack Cazes
Publisher : CRC Press
ISBN 13 : 1439870675
Total Pages : 2968 pages
Book Rating : 4.4/5 (398 download)

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Book Synopsis Encyclopedia of Chromatography by : Jack Cazes

Download or read book Encyclopedia of Chromatography written by Jack Cazes and published by CRC Press. This book was released on 2009-10-12 with total page 2968 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thoroughly revised and expanded, this third edition offers illustrative tables and figures to clarify technical points in the articles and provides a valuable, reader-friendly reference for all those who employ chromatographic methods for analysis of complex mixtures of substances. An authoritative source of information, this introductory guide to specific chromatographic techniques and theory discusses the relevant science and technology, offering key references for analyzing specific chemicals and applications in industry and focusing on emerging technologies and uses.

Analysis of Food Toxins and Toxicants

Author : Yiu-Chung Wong
Publisher : John Wiley & Sons
ISBN 13 : 1118992717
Total Pages : 816 pages
Book Rating : 4.1/5 (189 download)

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Book Synopsis Analysis of Food Toxins and Toxicants by : Yiu-Chung Wong

Download or read book Analysis of Food Toxins and Toxicants written by Yiu-Chung Wong and published by John Wiley & Sons. This book was released on 2017-07-03 with total page 816 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analysis of Food Toxins and Toxicants consists of five sections, providing up-to-date descriptions of the analytical approaches used to detect a range of food toxins. Part I reviews the recent developments in analytical technology including sample pre-treatment and food additives. Part II covers the novel analysis of microbial and plant toxins including plant pyrrolizidine alkaloids. Part III focuses on marine toxins in fish and shellfish. Part IV discusses biogenic amines and common food toxicants, such as pesticides and heavy metals. Part V summarizes quality assurance and the recent developments in regulatory limits for toxins, toxicants and allergens, including discussions on laboratory accreditation and reference materials.

Chemical Speciation of Organic and Inorganic components of Environmental and Biological Interest in Natural Fluids

Author : Francesco Crea
Publisher : MDPI
ISBN 13 : 3039284525
Total Pages : 218 pages
Book Rating : 4.0/5 (392 download)

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Book Synopsis Chemical Speciation of Organic and Inorganic components of Environmental and Biological Interest in Natural Fluids by : Francesco Crea

Download or read book Chemical Speciation of Organic and Inorganic components of Environmental and Biological Interest in Natural Fluids written by Francesco Crea and published by MDPI. This book was released on 2020-03-25 with total page 218 pages. Available in PDF, EPUB and Kindle. Book excerpt: The International Union of Pure and Applied Chemistry (IUPAC) defines the term “speciation” as the distribution of an element amongst defined chemical species in a system, while the process leading to quantitative estimation of the content of different species is called speciation analysis. The chemical speciation of elements in natural waters and biological fluids is a key topic, essential for discussing the chemical reactivity of constituents in these systems. It is well understood that it is the chemical form of a metal or metalloids that determines its reactivity, lifetime, and fate in the environment. Chemical speciation now involves various sectors of the sciences, from chemistry to biology, biochemistry, and environmental sciences, since—as is well known—the total concentration, alone, of an inorganic or organic component (metal or ligand) in a multicomponent natural system (fresh water, sea water, biological fluids, soil, etc.) is insufficient for a comprehensive understand of its behavior in those contests.

Advances in Food Science and Technology, Volume 1

Author : Visakh P. M.
Publisher : John Wiley & Sons
ISBN 13 : 1118121023
Total Pages : 336 pages
Book Rating : 4.1/5 (181 download)

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Book Synopsis Advances in Food Science and Technology, Volume 1 by : Visakh P. M.

Download or read book Advances in Food Science and Technology, Volume 1 written by Visakh P. M. and published by John Wiley & Sons. This book was released on 2013-03-04 with total page 336 pages. Available in PDF, EPUB and Kindle. Book excerpt: Written in a systematic and comprehensive manner, the book reports recent advances in the development of food science and technology areas. Advances in Food Science and Technology discusses many of the recent technical research accomplishments in the areas of food science and technology, such as food security as a global issue, food chemistry, frozen food and technology, as well as state-of-the-art developments concerning food production, properties, quality, trace element speciation, nanotechnology, and bionanocomposites for food packing applications. Specifically, this important book details: New innovative methods for food formulations and novel nanotechnology applications such as food packaging, enhanced barrier, active packaging, and intelligent packaging Freezing methods and equipment such as freezing by contact with cold air, cold liquid, and cold surfaces, cryogenic freezing, and a combination of freezing methods Chemical and functional properties of food components Bionanocomposites for natural food packing and natural biopolymer-based films such as polysaccharide films and protein films Regulatory aspects of food ingredients in the United States with the focus on the safety of enzyme preparations used in food

Environmental Health

Author : Jacques Oosthuizen
Publisher : BoD – Books on Demand
ISBN 13 : 9533078545
Total Pages : 338 pages
Book Rating : 4.5/5 (33 download)

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Book Synopsis Environmental Health by : Jacques Oosthuizen

Download or read book Environmental Health written by Jacques Oosthuizen and published by BoD – Books on Demand. This book was released on 2012-02-03 with total page 338 pages. Available in PDF, EPUB and Kindle. Book excerpt: Environmental health practitioners worldwide are frequently presented with issues that require further investigating and acting upon so that exposed populations can be protected from ill-health consequences. These environmental factors can be broadly classified according to their relation to air, water or food contamination. However, there are also work-related, occupational health exposures that need to be considered as a subset of this dynamic academic field. This book presents a review of the current practice and emerging research in the three broadly defined domains, but also provides reference for new emerging technologies, health effects associated with particular exposures and environmental justice issues. The contributing authors themselves display a range of backgrounds and they present a developing as well as a developed world perspective. This book will assist environmental health professionals to develop best practice protocols for monitoring a range of environmental exposure scenarios.