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Fast 2D Solution-state NMR

Author : Jean-Nicolas Dumez
Publisher : Royal Society of Chemistry
ISBN 13 : 1839168072
Total Pages : 505 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Fast 2D Solution-state NMR by : Jean-Nicolas Dumez

Download or read book Fast 2D Solution-state NMR written by Jean-Nicolas Dumez and published by Royal Society of Chemistry. This book was released on 2023-05-17 with total page 505 pages. Available in PDF, EPUB and Kindle. Book excerpt: Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.

Annual Reports on NMR Spectroscopy

Author :
Publisher : Elsevier
ISBN 13 : 0443295794
Total Pages : 208 pages
Book Rating : 4.4/5 (432 download)

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Book Synopsis Annual Reports on NMR Spectroscopy by :

Download or read book Annual Reports on NMR Spectroscopy written by and published by Elsevier. This book was released on 2024-07-11 with total page 208 pages. Available in PDF, EPUB and Kindle. Book excerpt: Annual Reports on NMR Spectroscopy, Volume 111 presents the latest release in a series that has established itself as a premier resource for both specialists and non-specialists interested in new techniques and applications pertaining to NMR spectroscopy. Chapters in this new release include Electrophoretic NMR, Traceability and uncertainty in NMR measurements, Quantitative NMR Spectroscopy, Advances in Non-Uniform Sampling NMR, NMR spectroscopy of natural and synthetic fibers, Characterization of transition alkane complexes, and Recent applications of low field NMR to membrane science. Serves as the premier resource for learning new techniques and applications in NMR spectroscopy Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)

Optimising NMR Spectroscopy Through Method and Software Development

Author : Jonathan Yong
Publisher : Springer Nature
ISBN 13 : 3031466845
Total Pages : 307 pages
Book Rating : 4.0/5 (314 download)

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Book Synopsis Optimising NMR Spectroscopy Through Method and Software Development by : Jonathan Yong

Download or read book Optimising NMR Spectroscopy Through Method and Software Development written by Jonathan Yong and published by Springer Nature. This book was released on 2024-02-10 with total page 307 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a comprehensive overview of Nuclear Magnetic Resonance (NMR) theory, its applications, and advanced techniques to improve the quality and speed of NMR data acquisition. In this book, the author expands his outstanding Ph.D. thesis and provides a valuable resource for researchers, professionals, and students in the field of NMR spectroscopy. The book covers quantum mechanics basics, and topics like density operators, pulse sequences, 1D pulse acquisition, INEPT (Insensitive nuclei enhancement by polarization transfer), product operators, and 2D NMR principles. It also explores innovative experiments like States HSQC (Heteronuclear Single Quantum Coherence) and echo-antiecho HSQC with gradients. In the subsequent chapters, the author discusses Pure Shift NMR, including PSYCHE (Pure Shift Yielded by Chirp Excitation) and its optimizations, such as waveform parameterization and time-reversal methods. The 'Discrete PSYCHE' approach and Ultrafast PSYCHE-iDOSY (Diffusion-ordered spectroscopy) are also highlighted. This book presents the POISE (Parameter Optimisation by Iterative Spectral Evaluation) software for real-time NMR experiment optimization, including pulse width calibration and Ernst angle optimization, and demonstrates applications across various NMR experiments. Lastly, the book examines accelerated 2D NMR data collection and the NOAH (NMR by Ordered Acquisition using 1H detection) supersequences, emphasizing automated pulse program creation using GENESIS (GENEration of Supersequences In Silico). Covered NMR experiments include 13C sensitivity-enhanced HSQC, 15N HMQC (Heteronuclear Multiple Quantum Coherence), dual HSQC, HSQC-TOCSY (Total Correlation Spectroscopy), HMBC (Heteronuclear Multiple Bond Correlation), and ADEQUATE (Adequate Sensitivity Double-Quantum Spectroscopy).

Gas Phase NMR

Author : Karol Jackowski
Publisher : Royal Society of Chemistry
ISBN 13 : 1782623817
Total Pages : 419 pages
Book Rating : 4.7/5 (826 download)

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Book Synopsis Gas Phase NMR by : Karol Jackowski

Download or read book Gas Phase NMR written by Karol Jackowski and published by Royal Society of Chemistry. This book was released on 2016-02-09 with total page 419 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers the recent NMR studies with the application of gaseous molecules. Among the comprehensively discussed aspects of the area it includes in particular: new multinuclear experiments that deliver spectral parameters of isolated molecules and provide the most accurate values of nuclear magnetic shielding, isotropic spin–spin coupling and relaxation times; advanced, precise and correct theoretical descriptions of spectral parameters of molecules as well as the application of gas-phase NMR measurements to chemical analysis and medicine. The progress of research in these fields is enormous and has rapidly changed our knowledge and understanding of molecular parameters in NMR spectroscopy. For example, accurate studies of the shielding for isolated molecules allow the exact determination of nuclear magnetic dipole moments, the calculated values of spectral parameters can be verified by precise gas-phase NMR measurements, and the application of hyperpolarized noble gases provides excellent MRI pictures of lungs. Aimed at graduates and researchers in spectroscopy, analytical chemistry and those researching the applications of NMR in medicine, this book presents the connections between sophisticated experiments, the theory of magnetic parameters and the exploration of new methods in practice.

Physical Principles of Chirality in NMR

Author : Piotr Garbacz
Publisher : Royal Society of Chemistry
ISBN 13 : 1839169591
Total Pages : 268 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Physical Principles of Chirality in NMR by : Piotr Garbacz

Download or read book Physical Principles of Chirality in NMR written by Piotr Garbacz and published by Royal Society of Chemistry. This book was released on 2024-09-20 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: How can we study one of the most elusive molecular properties, chirality, using nuclear interactions with the magnetic field that are apparently insensitive to handedness? This book answers this question from the physicochemical point of view by providing a clear, coherent, and comprehensive review of methods used in NMR studies of chirality. Presented arguments based on fundamental physical and chemical laws and in-depth descriptions of new methods utilizing purely physical interactions are mainly addressed to spectroscopists in both academia and industry. The introductory chapters provide the reader with the basics of NMR spectroscopy as a tool for the study of chiral compounds, and those more interested in the methods of chiral discrimination will benefit from the brief description of their common points and reasons why some of them may or may not work. In the following chapters, the book shows rapid progress in a newly emerging field of chirality-sensitive NMR, in particular, a search for effects that give direct information about the absolute configuration of a molecule.

Environment in a Magnet

Author : Pellegrino Conte
Publisher : Royal Society of Chemistry
ISBN 13 : 1837671265
Total Pages : 461 pages
Book Rating : 4.8/5 (376 download)

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Book Synopsis Environment in a Magnet by : Pellegrino Conte

Download or read book Environment in a Magnet written by Pellegrino Conte and published by Royal Society of Chemistry. This book was released on 2024-03-04 with total page 461 pages. Available in PDF, EPUB and Kindle. Book excerpt: Global climate change is the most important challenge humankind is facing in the modern era. One of the main scientific concerns is the monitoring of contaminants in the environment, which require the right environmental remediation strategies. In this context, nuclear magnetic resonance (NMR) techniques have a very important role in enabling the discovery of how pollutants are transformed, how they can move and how they can affect human health. This book discusses the present and the future perspectives of NMR techniques for environmental evaluations. It covers, amongst other topics, the importance of NMR as a contamination discovery tool, how to improve sensitivity in environmental NMR, and multiphase NMR for measurement of samples in their natural state. Samples include lubricant oils, soils and porous media. Due to the direct relationship between the environment and human health, there is information dedicated to the use of magnetic resonance imaging (MRI) to monitor human health as related to environmental pollution. There is also a chapter on how NMR is used in cultural heritage to measure artefacts directly affected by environmental pollution. Filling a gap in the literature, the book is for researchers explaining how to apply their knowledge of NMR techniques to solve environmental problems, and for students who want to deepen their understanding of this topic.

Integrated Structural Biology

Author : Tatyana Polenova
Publisher : Royal Society of Chemistry
ISBN 13 : 1837670161
Total Pages : 349 pages
Book Rating : 4.8/5 (376 download)

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Book Synopsis Integrated Structural Biology by : Tatyana Polenova

Download or read book Integrated Structural Biology written by Tatyana Polenova and published by Royal Society of Chemistry. This book was released on 2023-12-08 with total page 349 pages. Available in PDF, EPUB and Kindle. Book excerpt: Modern research in biology increasingly relies on multiple techniques for describing structures and mechanisms. This book provides an overview of the contemporary integrated biology approaches for solving structures and understanding mechanisms of complex biological systems. It includes several methodology chapters discussing the current developments in the areas of cryo-electron microscopy (EM) and cryo-electron tomography (ET), computational biophysics, solution NMR spectroscopy, solid-state NMR spectroscopy and dynamic nuclear polarization (DNP), electron paramagnetic resonance (EPR), (photo-)chemically induced dynamic nuclear polarization (CIDNP), X-ray crystallography and small-angle X-ray and neutron scattering (SAXS/SANS). Several subsequent chapters demonstrate how these methods are used in synergy to address problems at the forefront of structural biology, with particular emphasis on examples where individual techniques are insufficient. Examples of biological systems include membrane proteins, viral protein assemblies, cytoskeleton protein assemblies, photosynthetic reaction centers, large enzyme complexes and whole cells. The book is targeted to both the current practitioners of structural biology and scientists who are interested in entering the fields of structural biology or biophysical chemistry.

Residual Dipolar Couplings

Author : Lishan Yao
Publisher : Royal Society of Chemistry
ISBN 13 : 1839167904
Total Pages : 319 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Residual Dipolar Couplings by : Lishan Yao

Download or read book Residual Dipolar Couplings written by Lishan Yao and published by Royal Society of Chemistry. This book was released on 2024-02-16 with total page 319 pages. Available in PDF, EPUB and Kindle. Book excerpt: Residual dipolar couplings (RDCs) are NMR measurements widely used to determine structural and dynamic information in small molecules and large macromolecules. This book provides a broad view of RDCs, from basic principles to advanced applications in organic molecules and biomolecules. Exploring the newest developments in RDC measurement and analysis through authoritative accounts written by leaders in the field, this book provides a comprehensive overview on the fundamentals, analysis and applications in one place for the first time. The versatility and accuracy of RDCs have found a large range of applications in NMR, and their measurement and analysis are major research areas. Readers, be they experts or students, will receive a strong understanding of the fundamentals of RDCs and their applications to their research projects.

Biophysics of Molecular Chaperones

Author : Sebastian Hiller
Publisher : Royal Society of Chemistry
ISBN 13 : 1839165995
Total Pages : 344 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Biophysics of Molecular Chaperones by : Sebastian Hiller

Download or read book Biophysics of Molecular Chaperones written by Sebastian Hiller and published by Royal Society of Chemistry. This book was released on 2023-11-01 with total page 344 pages. Available in PDF, EPUB and Kindle. Book excerpt: Molecular chaperones are critical to control protein quality in all living cells. Understanding chaperone function at the atomic level, and in particular its mode of interaction with client proteins, is crucial to understanding the fundamental roles chaperones play in biology. This book fills a gap in the literature by comprehensively summarizing and discussing new advanced experimental techniques for their analysis. Providing a comprehensive overview of advanced biophysical methods for the characterization of molecular mechanisms of molecular chaperones, the majority of the contributions are NMR methodology. This is the method of choice for atomic resolution studies of such systems. Additional notable biophysical approaches are considered to present all relevant current developments in exploring chaperone function and the transient and dynamic interactions with their client proteins. The book is targeted at both current practitioners of structural biology and biophysical chemistry and scientists who are interested in entering the field. It could be useful for graduate students as supplementary reading.

Modern Methods in Solid-state NMR

Author : Paul Hodgkinson
Publisher : Royal Society of Chemistry
ISBN 13 : 1788014197
Total Pages : 452 pages
Book Rating : 4.7/5 (88 download)

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Book Synopsis Modern Methods in Solid-state NMR by : Paul Hodgkinson

Download or read book Modern Methods in Solid-state NMR written by Paul Hodgkinson and published by Royal Society of Chemistry. This book was released on 2018-04-05 with total page 452 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques. In this unique volume, a range of experts in different areas of modern solid-state NMR explain about their area of expertise, emphasising the “practical aspects” of implementing different techniques, and illustrating what questions can and cannot be addressed. Later chapters address complex materials, showing how different NMR techniques discussed in earlier chapters can be brought together to characterise important materials types. The volume as a whole focusses on topics relevant to the developing field of “NMR crystallography” – the use of solids NMR as a complement to diffraction crystallography. This book is an ideal complement to existing introductory texts and reviews on solid-state NMR. New researchers wanting to understand new areas of solid-state NMR will find each chapter to be the equivalent to spending time in the laboratory of an internationally leading expert, learning the hints and tips that make the difference between knowing about a technique and being ready to put it into action. With no equivalent on the market, it will be of interest to every solid-state NMR researcher (academic and postgraduate) working in the chemical sciences.

Microbial Biofilms

Author : Sanket Joshi
Publisher : Elsevier
ISBN 13 : 0323957161
Total Pages : 454 pages
Book Rating : 4.3/5 (239 download)

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Book Synopsis Microbial Biofilms by : Sanket Joshi

Download or read book Microbial Biofilms written by Sanket Joshi and published by Elsevier. This book was released on 2023-06-10 with total page 454 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microbial Biofilms: Challenges and Advances in Metabolomic Study is a volume in the Advances in Biotechnology and Bioengineering Series. The volume covers the metabolomic characteristics of bacterial biofilms and examines the techniques used in the analysis of the metabolomics of the biofilm, its formation, and related infections. The book includes the metabolomics study of various types of biofilms and details new strategies in targeting metabolic pathways for inhibiting the biofilm. The book also describes various types of metabolomics studies like metabolomics of oral biofilm and metabolomics of biofilm by nosocomial microbes. It also points out the recent advancements on various aspects of metabolomics studies pertaining to biofilms, related infections, their pathogenesis, and present-day treatment strategies. Microbial Biofilms: Challenges and Advances in Metabolomic Study is a helpful resource to scientists and researchers engaged in biofilm studies, precisely on the metabolomic changes at molecular level occurring in the participating microorganisms. It is also fascinating and thought provoking for the clinicians and health professionals actively involved in the treatment of biofilm mediated chronic infections, since it depicts the pathogenic consequences of the small molecular interactions of the metabolites in biofilm. Discusses recent trends in biofilms research Details newer strategies in treating the biofilm by targeting metabolic pathways Covers chronic infections caused by biofilm and their metabolomics studies Examines various analytical aspects on the metabolomics study of biofilm as well as how metabolomics regulate the formation of the biofilm Incorporates relevant case studies

Practical NMR for Oil and Gas Exploration

Author : Lizhi Xiao
Publisher : Royal Society of Chemistry
ISBN 13 : 183916459X
Total Pages : 626 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Practical NMR for Oil and Gas Exploration by : Lizhi Xiao

Download or read book Practical NMR for Oil and Gas Exploration written by Lizhi Xiao and published by Royal Society of Chemistry. This book was released on 2023-08-14 with total page 626 pages. Available in PDF, EPUB and Kindle. Book excerpt: Describing comprehensively the development and applications of NMR to oil and gas exploration, this book will bring the literature up to date as it has developed very quickly in the last two decades. Outlining new methodologies, it will provide a thorough and comprehensive document enabling a better understanding of the basics of NMR physics, petrophysics, downhole tools and data interpretation. Written by an author with more than 30 years’ experience in this hot and important topic, this book is designed to meet the needs of the community and encourage applications in low field NMR.

Nuclear Magnetic Resonance

Author : Navin Khaneja
Publisher :
ISBN 13 : 1838804196
Total Pages : 147 pages
Book Rating : 4.8/5 (388 download)

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Book Synopsis Nuclear Magnetic Resonance by : Navin Khaneja

Download or read book Nuclear Magnetic Resonance written by Navin Khaneja and published by . This book was released on 2020-04-08 with total page 147 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Magnetic Resonance and its Applications in Drug Formulation and Delivery

Author : Michael D Mantle
Publisher : Royal Society of Chemistry
ISBN 13 : 1839160020
Total Pages : 390 pages
Book Rating : 4.8/5 (391 download)

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Book Synopsis Magnetic Resonance and its Applications in Drug Formulation and Delivery by : Michael D Mantle

Download or read book Magnetic Resonance and its Applications in Drug Formulation and Delivery written by Michael D Mantle and published by Royal Society of Chemistry. This book was released on 2024-03-27 with total page 390 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book details the latest research and development in the use of magnetic resonance imaging and spectroscopy as tools to give quantitative insights concerning late stage pharmaceutical formulation, tablet manufacturing and drug dissolution behaviour. The book combines different facets of magnetic resonance and highlights the use of spatial resolution (MRI) and how this adds to the knowledge base to further our understanding of the microscopic physicochemical processes occurring during drug release from solid dosage forms. New topics, that have not been thoroughly reviewed elsewhere, are covered including the applications of solution state magnetic resonance in process scale up, reaction monitoring/understanding and process analytical technologies (PAT); dissolution testing; and counterfeit analysis. Solid state NMR and its role in understanding phase separation in dispersions, polymorphism and crystallography are included and magnetic resonance imaging and its use in assessing tablet dissolution performance, mass transport and mixing in hot melt extrusion (HME) are covered. Focusing on late stage development rather than molecular drug discovery provides a unique approach and the book will appeal to a diversity of disciplines using spectroscopy for study. Aimed at researchers in drug development, manufacture and formulation in both industry (pharmaceutical companies) and academia (pharmacy program), it includes examples, where appropriate, of studies on commercially available pharmaceutical products.

Biological NMR Spectroscopy

Author : John L. Markley
Publisher : Oxford University Press
ISBN 13 : 0195357426
Total Pages : 375 pages
Book Rating : 4.1/5 (953 download)

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Book Synopsis Biological NMR Spectroscopy by : John L. Markley

Download or read book Biological NMR Spectroscopy written by John L. Markley and published by Oxford University Press. This book was released on 1997-01-30 with total page 375 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents a critical assessment of progress on the use of nuclear magnetic resonance spectroscopy to determine the structure of proteins, including brief reviews of the history of the field along with coverage of current clinical and in vivo applications. The book, in honor of Oleg Jardetsky, one of the pioneers of the field, is edited by two of the most highly respected investigators using NMR, and features contributions by most of the leading workers in the field. It will be valued as a landmark publication that presents the state-of-the-art perspectives regarding one of today's most important technologies.

Annual Reports on NMR Spectroscopy

Author : Graham A. Webb
Publisher : Academic Press
ISBN 13 : 0323855407
Total Pages : 394 pages
Book Rating : 4.3/5 (238 download)

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Book Synopsis Annual Reports on NMR Spectroscopy by : Graham A. Webb

Download or read book Annual Reports on NMR Spectroscopy written by Graham A. Webb and published by Academic Press. This book was released on 2021-02-26 with total page 394 pages. Available in PDF, EPUB and Kindle. Book excerpt: Annual Reports on NMR Spectroscopy, Volume 102 has established itself as a premier resource for both specialists and non-specialists who are looking to become familiar with new techniques and applications pertaining to NMR spectroscopy. Serves as the premier resource for learning the new techniques and applications of NMR spectroscopy Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)

Nuclear Magnetic Resonance

Author : G A Webb
Publisher : Royal Society of Chemistry
ISBN 13 : 184755847X
Total Pages : 387 pages
Book Rating : 4.8/5 (475 download)

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Book Synopsis Nuclear Magnetic Resonance by : G A Webb

Download or read book Nuclear Magnetic Resonance written by G A Webb and published by Royal Society of Chemistry. This book was released on 2008-05-27 with total page 387 pages. Available in PDF, EPUB and Kindle. Book excerpt: As a spectroscopic method, nuclear magnetic resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive coverage of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Nucleic Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an invaluable source of current methods and applications. Volume 37 covers literature published from June 2006 to May 2007.