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Electrochemical Ammonia Synthesis
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Book Synopsis Photo-Electrochemical Ammonia Synthesis by : Mohammadreza Nazemi
Download or read book Photo-Electrochemical Ammonia Synthesis written by Mohammadreza Nazemi and published by . This book was released on 2021 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: "This book covers the synthesis of novel hybrid plasmonic nanomaterials and their application in photo-electrochemical systems to convert low energy molecules to high value-added molecules and looks specifically at photo-electrochemical nitrogen reduction reaction (NRR) for ammonia synthesis as an attractive alternative to the long-lasting thermochemical process. This book will be of high interest to researchers, advanced students, and industry professionals in working in sustainable energy storage and conversion across the disciplines of Chemical Engineering, Mechanical Engineering, Materials Science and Engineering, Environmental Engineering, and related areas"--
Book Synopsis Sustainable Ammonia Production by : Inamuddin
Download or read book Sustainable Ammonia Production written by Inamuddin and published by Springer Nature. This book was released on 2020-01-09 with total page 136 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents sustainable synthetic pathways and modern applications of ammonia. It focuses on the production of ammonia using various catalytic systems and its use in fuel cells, membrane, agriculture, and renewable energy sectors. The book highlights the history, investigation, and development of sustainable pathways for ammonia production, current challenges, and state-of-the-art reviews. While discussing industrial applications, it fills the gap between laboratory research and viable applications in large-scale production.
Book Synopsis Photo-Electrochemical Ammonia Synthesis by : Mohammadreza Nazemi
Download or read book Photo-Electrochemical Ammonia Synthesis written by Mohammadreza Nazemi and published by CRC Press. This book was released on 2021-07-27 with total page 160 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ammonia holds great promise as a carbon-neutral liquid fuel for storing intermittent renewable energy sources and power generation due to its high energy density and hydrogen content. Photo-Electrochemical Ammonia Synthesis: Nanocatalyst Discovery, Reactor Design, and Advanced Spectroscopy covers the synthesis of novel hybrid plasmonic nanomaterials and their application in photo-electrochemical systems to convert low energy molecules to high value-added molecules and looks specifically at photo-electrochemical nitrogen reduction reaction (NRR) for ammonia synthesis as an attractive alternative to the long-lasting thermochemical process. Provides an integrated scientific framework, combining materials chemistry, photo-electrochemistry, and spectroscopy to overcome the challenges associated with renewable energy storage and transport Reviews materials chemistry for the synthesis of a range of heterogeneous (photo) electrocatalysts including plasmonic and hybrid plasmonic-semiconductor nanostructures for selective and efficient conversion of N2 to NH3 Covers novel reactor design to study the redox processes in the photo-electrochemical energy conversion system and to benchmark nanocatalysts’ selectivity and activity toward NRR Discusses the use of advanced spectroscopic techniques to probe the reaction mechanism for ammonia synthesis Offers techno-economic analysis and presents performance targets for the scale-up and commercialization of electrochemical ammonia synthesis This book is of value to researchers, advanced students, and industry professionals working in sustainable energy storage and conversion across the disciplines of Chemical Engineering, Mechanical Engineering, Materials Science and Engineering, Environmental Engineering, and related areas.
Book Synopsis Catalytic Ammonia Synthesis by : J.R. Jennings
Download or read book Catalytic Ammonia Synthesis written by J.R. Jennings and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 462 pages. Available in PDF, EPUB and Kindle. Book excerpt: The phenomenon of catalysis is found in many homogeneous and heterogeneous systems undergoing chemical change, where it effects the rates of approach to the equilibrium state in processes as diverse as those found in the stars, the earth's mantle, living organisms, and the various chemistries utilized by industry. The economies and the living standards of both developed and developing countries depend to varying degrees upon the efficacy of their chemical industries. Con sequently, this century has seen a wide exploration and expansion of catalytic chemistry together with an intensive investigation of specific, essential processes like those contributing to life-supporting agricultures. Prime among the latter must surely be the "fixation" of atmospheric nitrogen by catalytic hydrogenation to anhydrous ammonia, still the preferred synthetic precursor of the nitrogenous components of fertilizers. In each decade contemporary concepts and techniques have been used to further the understanding, as yet incomplete, of the catalyst, the adsorbates, the surface reactions, and the technology of large-scale operation. The contributors to the present volume review the state of the art, the science, and the technology; they reveal existing lacunae, and suggest ways forward. Around the turn of the century, Sabatier's school was extending the descriptive catalytic chemistry of hydrogenation by metals to include almost all types of multiple bond. The triple bond of dinitrogen, which continued to be more resistant than the somewhat similar bonds in carbon monoxide and ethyne, defied their efforts.
Book Synopsis Plasma Catalysis by : Annemie Bogaerts
Download or read book Plasma Catalysis written by Annemie Bogaerts and published by MDPI. This book was released on 2019-04-02 with total page 248 pages. Available in PDF, EPUB and Kindle. Book excerpt: Plasma catalysis is gaining increasing interest for various gas conversion applications, such as CO2 conversion into value-added chemicals and fuels, N2 fixation for the synthesis of NH3 or NOx, methane conversion into higher hydrocarbons or oxygenates. It is also widely used for air pollution control (e.g., VOC remediation). Plasma catalysis allows thermodynamically difficult reactions to proceed at ambient pressure and temperature, due to activation of the gas molecules by energetic electrons created in the plasma. However, plasma is very reactive but not selective, and thus a catalyst is needed to improve the selectivity. In spite of the growing interest in plasma catalysis, the underlying mechanisms of the (possible) synergy between plasma and catalyst are not yet fully understood. Indeed, plasma catalysis is quite complicated, as the plasma will affect the catalyst and vice versa. Moreover, due to the reactive plasma environment, the most suitable catalysts will probably be different from thermal catalysts. More research is needed to better understand the plasma–catalyst interactions, in order to further improve the applications.
Book Synopsis Ammonia Synthesis Catalysts: Innovation And Practice by : Huazhang Liu
Download or read book Ammonia Synthesis Catalysts: Innovation And Practice written by Huazhang Liu and published by World Scientific. This book was released on 2013-03-21 with total page 895 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a review of worldwide developments in ammonia synthesis catalysts over the last 30 years. It focuses on the new generation of Fe1-xO based catalysts and ruthenium catalysts — both are major breakthroughs for fused iron catalysts. The basic theory for ammonia synthesis is systematically explained, covering topics such as the chemical components, crystal structure, preparation, reduction, performance evaluation, characterization of the catalysts, the mechanism and kinetics of ammonia synthesis reaction. Both theory and practice are combined in this presentation, with emphasis on the research methods, application and exploitation of catalysts.The comprehensive volume includes an assessment of the economic and engineering aspects of ammonia plants based on the performance of catalysts. Recent developments in photo-catalysis, electro-catalysis, biocatalysis and new uses of ammonia are also introduced in this book.The author, Professor Huazhang Liu, has been engaged in research and practice for more than 50 years in this field and was the inventor of the first Fe1-xO based catalysts in the world. He has done a lot of research on Fe3O4 based- and ruthenium based-catalysts, and has published more than 300 papers and obtained 21 patents during his career.
Book Synopsis Electrochemical Ammonia Synthesis by : John Anthony Schwalbe
Download or read book Electrochemical Ammonia Synthesis written by John Anthony Schwalbe and published by . This book was released on 2019 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Due to the development of the Haber-Bosch process, humanity accounts for over half of the nitrogen fixation that occurs on Earth, the other half being microbial activity and lightning. This leads to a large footprint in terms of runoff, energy usage, and plant growth. Due to its use of methane as a source of hydrogen, the Haber-Bosch process emits 1% of all anthropogenic carbon dioxide. The high temperature and pressure required by the Haber-Bosch process also necessitates large, centralized plants. In this thesis, I explore a possible alternative, electrochemical ammonia synthesis. This process uses proton-electron pairs to reduce nitrogen at a cathode in an electrochemical cell. The only inputs are air, water, and electricity. If successful, an electrochemical ammonia cell could operate at ambient temperature and pressure due to the high driving force provided by the electric potential. The challenge of electrochemical ammonia synthesis comes from the inert nature of dinitrogen and the ease of the competing hydrogen evolution reaction. In the Haber-Bosch process, high temperatures are used to help break the N-N triple bond. In electrochemical ammonia synthesis, voltage and reactive catalysts are used. Unfortunately, at these conditions protons can be readily reduced to hydrogen rather than added to the nitrogen to form ammonia. Not only is ammonia synthesis difficult from a fundamental standpoint, it is also difficult from the standpoint of experimental validation. Because the amounts of ammonia detected are generally small, contamination is easily mistaken for positive results. For example, a human breath contains enough ammonia to produce what appears to be a promising result. Many common materials, epoxy, nitric acid, rubber gloves, etc., contain nitrogen compounds that can be reduced more easily than dinitrogen. Working with our collaborators in Ib Chorkendorff's group at DTU and other SUNCAT researchers at Stanford University we developed rigorous protocols to overcome these challenges. The only way to definitively prove ammonia synthesis is with quantitative isotopically labeled experiments with purified 15N2 gas. However, the contamination found in many commercially available cylinders of 15N2 means that such an experiment could easily be fooled. Our work on proton limitations combined with rigorous verification led to the first unambiguous demonstration of electrochemical ammonia synthesis using a lithium mediated strategy, described in chapter 3. The lithium-mediated protocol was first explored in 1993 by Tsuneto et. al., but they did not possess the techniques necessary to truly prove ammonia synthesis. Our definitive result is important for two reasons. First, it validated our theoretical framework and should inspire future research into non-aqueous systems for nitrogen reduction and other challenging reactions. Second, it allowed for a positive demonstration of ammonia synthesis. we investigated the nature of the ammonia synthesis as well as the reaction at the counter electrode. The lithium mediated system uses a THF electrolyte with dissolved lithium perchlorate as a lithium source and electrolyte and ethanol as a proton donor. The cell is operated at a voltage where lithium is plated onto the cathode. The nature of the catalyst is not obvious. Using electrochemical characterization and density functional theory, we show that lithium metal, lithium nitride, and lithium hydride are all plausible candidate catalysts. Experiments show that appreciable amount of the current ends up as lithium on the surface. Surprisingly, relatively little of this reacts to form fixed nitrogen on the cathode. Density Functional Theory experiments support this observation by showing that lithium nitride should be unstable relative to lithium metal and ammonia at the operating conditions. These calculations also suggest that lithium hydride and nitride can both act as catalysts for ammonia synthesis, opening up exciting options for materials that are stable at less reducing conditions.
Download or read book Graphdiyne written by Yuliang Li and published by John Wiley & Sons. This book was released on 2022-01-10 with total page 404 pages. Available in PDF, EPUB and Kindle. Book excerpt: Graphdiyne Discover the most cutting-edge developments in the study of graphdiyne from a pioneer of the field In Graphdiyne: Fundamentals and Applications in Renewable Energy and Electronics, accomplished chemist Dr. Yuliang Li delivers a practical and insightful compilation of theoretical and experimental developments in the study of graphdiyne. Of interest to both academics and industrial researchers in the fields of nanoscience, organic chemistry, carbon science, and renewable energies, the book systematically summarizes recent research into the exciting new material. Discover information about the properties of graphdiyne through theoretical simulations and experimental characterizations, as well as the development of graphdiyne with appropriate preparation technology. Learn to create new graphdiyne-based materials and better understand its intrinsic properties. Find out about synthetic methodologies, the controlled growth of aggregated state structures, and structural characterization. In addition to demonstrating the interdisciplinary potential and relevance of graphdiyne, the book also offers readers: A thorough introduction to basic structure and band gap engineering, including molecular and electronic structure, mechanical properties, and the layers structure of bulk graphdiyne Explorations of Graphdiyne synthesis and characterization, including films, nanotube arrays and nanowires, nanowalls, and nanosheets, as well as characterization methods Discussions of the functionalization of graphdiyne, including heteroatom doping, metal decoration, and absorption of guest molecules Rigorous treatments of Graphdiyne-based materials in catalytic applications, including photo- and electrocatalysts Perfect for organic chemists, electronics engineers, materials scientists, and physicists, Graphdiyne: Fundamentals and Applications in Renewable Energy and Electronics will also find its place on the bookshelves of surface and solid-state chemists, electrochemists, and catalytic chemists seeking a one-stop reference on this rising-star carbon material.
Book Synopsis Photo- and Electro-Catalytic Processes by : Jianmin Ma
Download or read book Photo- and Electro-Catalytic Processes written by Jianmin Ma and published by John Wiley & Sons. This book was released on 2022-01-25 with total page 596 pages. Available in PDF, EPUB and Kindle. Book excerpt: Explore green catalytic reactions with this reference from a renowned leader in the field Green reactions—like photo-, photoelectro-, and electro-catalytic reactions—offer viable technologies to solve difficult problems without significant damage to the environment. In particular, some gas-involved reactions are especially useful in the creation of liquid fuels and cost-effective products. In Photo- and Electro-Catalytic Processes: Water Splitting, N2 Fixing, CO2 Reduction, award-winning researcher Jianmin Ma delivers a comprehensive overview of photo-, electro-, and photoelectron-catalysts in a variety of processes, including O2 reduction, CO2 reduction, N2 reduction, H2 production, water oxidation, oxygen evolution, and hydrogen evolution. The book offers detailed information on the underlying mechanisms, costs, and synthetic methods of catalysts. Filled with authoritative and critical information on green catalytic processes that promise to answer many of our most pressing energy and environmental questions, this book also includes: Thorough introductions to electrocatalytic oxygen reduction and evolution reactions, as well as electrocatalytic hydrogen evolution reactions Comprehensive explorations of electrocatalytic water splitting, CO2 reduction, and N2 reduction Practical discussions of photoelectrocatalytic H2 production, water splitting, and CO2 reduction In-depth examinations of photoelectrochemical oxygen evolution and nitrogen reduction Perfect for catalytic chemists and photochemists, Photo- and Electro-Catalytic Processes: Water Splitting, N2 Fixing, CO2 Reduction also belongs in the libraries of materials scientists and inorganic chemists seeking a one-stop resource on the novel aspects of photo-, electro-, and photoelectro-catalytic reactions.
Book Synopsis Low Temperature Electrochemical Ammonia Synthesis by : Adrian Denvir
Download or read book Low Temperature Electrochemical Ammonia Synthesis written by Adrian Denvir and published by . This book was released on 2005 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Selective Hydrocarbon Activation by : Julian A. Davies
Download or read book Selective Hydrocarbon Activation written by Julian A. Davies and published by Wiley-VCH. This book was released on 1990 with total page 592 pages. Available in PDF, EPUB and Kindle. Book excerpt: A review of the principles, current research and ideas related to taking naturally occurring petroleum by-products and making them into useful products. This book aims to introduce nonspecialists to the field and provide them with current knowledge contributed by experts in inorganic, organic, catalysis chemistries and biochemistry. The focus is on homogeneous metal-based chemistry with an emphasis on mechanism and energetics. Selective Hydrocarbon Activation is a blend of theory and experiment and is of interest to both academics and those in industry.
Book Synopsis Enriching the Earth by : Vaclav Smil
Download or read book Enriching the Earth written by Vaclav Smil and published by MIT Press. This book was released on 2004-02-27 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt: Dr. Smil is the world's authority on nitrogenous fertilizer. The industrial synthesis of ammonia from nitrogen and hydrogen has been of greater fundamental importance to the modern world than the invention of the airplane, nuclear energy, space flight, or television. The expansion of the world's population from 1.6 billion people in 1900 to today's six billion would not have been possible without the synthesis of ammonia. In Enriching the Earth, Vaclav Smil begins with a discussion of nitrogen's unique status in the biosphere, its role in crop production, and traditional means of supplying the nutrient. He then looks at various attempts to expand natural nitrogen flows through mineral and synthetic fertilizers. The core of the book is a detailed narrative of the discovery of ammonia synthesis by Fritz Haber—a discovery scientists had sought for over one hundred years—and its commercialization by Carl Bosch and the chemical company BASF. Smil also examines the emergence of the large-scale nitrogen fertilizer industry and analyzes the extent of global dependence on the Haber-Bosch process and its biospheric consequences. Finally, it looks at the role of nitrogen in civilization and, in a sad coda, describes the lives of Fritz Haber and Carl Bosch after the discovery of ammonia synthesis.
Download or read book Ammonia written by Anders Nielsen and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 352 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ammonia is one of the 10 largest commodity chemicals produced. The editor, Anders Nielsen, is research director with one of the largest industrial catalyst producers. He has compiled a complete reference on all aspects of catalytical ammonia production in industry, from thermodynamics and kinetics to reactor and plant design. One chapter deals with safety aspects of ammonia handling and storage.
Book Synopsis Ammonia Fuel Cells by : Ibrahim Dincer
Download or read book Ammonia Fuel Cells written by Ibrahim Dincer and published by Elsevier. This book was released on 2020-04-09 with total page 266 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ammonia Fuel Cells covers all aspects of ammonia fuel cell technologies and their applications, including their theoretical analysis, modeling studies and experimental investigations. The book analyzes the role of integrated ammonia fuel cell systems within various renewable energy resources and existing energy systems. Covers the types of ammonia fuel cells that have been developed over history Features explanations of the underlying fundamentals and principles of ammonia fuel cells, along with methods to assess the performance of different types of cell Includes case studies considering different applications of ammonia fuel cells and their significance in the future of clean energy
Book Synopsis The Alchemy of Air by : Thomas Hager
Download or read book The Alchemy of Air written by Thomas Hager and published by Crown. This book was released on 2008-09-09 with total page 338 pages. Available in PDF, EPUB and Kindle. Book excerpt: A sweeping history of tragic genius, cutting-edge science, and the Haber-Bosch discovery that changed billions of lives—including your own. At the dawn of the twentieth century, humanity was facing global disaster: Mass starvation was about to become a reality. A call went out to the world’ s scientists to find a solution. This is the story of the two men who found it: brilliant, self-important Fritz Haber and reclusive, alcoholic Carl Bosch. Together they discovered a way to make bread out of air, built city-sized factories, and saved millions of lives. But their epochal triumph came at a price we are still paying. The Haber-Bosch process was also used to make the gunpowder and explosives that killed millions during the two world wars. Both men were vilified during their lives; both, disillusioned and disgraced, died tragically. The Alchemy of Air is the extraordinary, previously untold story of a discovery that changed the way we grow food and the way we make war–and that promises to continue shaping our lives in fundamental and dramatic ways.
Book Synopsis Ammonothermal Synthesis and Crystal Growth of Nitrides by : Elke Meissner
Download or read book Ammonothermal Synthesis and Crystal Growth of Nitrides written by Elke Meissner and published by Springer Nature. This book was released on 2021-02-07 with total page 351 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a collection of contributed chapters, delivering a comprehensive overview of topics related to the synthesis and crystal growth of nitride compounds under supercritical ammonia conditions. Focusing on key chemical and technological aspects of ammonothermal synthesis and growth of functional nitride compounds, the book also describes many innovative techniques for in-situ observation and presents new data fundamental for materials synthesis under ammonothermal conditions. With its detailed coverage of many thermodynamic and kinetics aspects, which are necessary for understanding and controlling crystal growth, this contributed volume is the ideal companion to materials chemists and engineers at any point in their journey in this rich and exciting field.
Book Synopsis Microwaves in Catalysis by : Satoshi Horikoshi
Download or read book Microwaves in Catalysis written by Satoshi Horikoshi and published by John Wiley & Sons. This book was released on 2015-12-14 with total page 426 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive overview covering the principles and preparation of catalysts, as well as reactor technology and applications in the field of organic synthesis, energy production, and environmental catalysis. Edited and authored by renowned and experienced scientists, this reference focuses on successful reaction procedures for applications in industry. Topics include catalyst preparation, the treatment of waste water and air, biomass and waste valorisation, hydrogen production, oil refining as well as organic synthesis in the presence of heterogeneous and homogeneous catalysts and continuous-flow reactions. With its practical relevance and successful methodologies, this is a valuable guide for chemists at universities working in the field of catalysis, organic synthesis, pharmaceutical or green chemistry, as well as researchers and engineers in the chemical industry.
