Characterization of Laser-induced Plasma and Application to Surface-assisted LIBS for Powder and Liquid Samples

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Book Synopsis Characterization of Laser-induced Plasma and Application to Surface-assisted LIBS for Powder and Liquid Samples by : Ye Tian

Download or read book Characterization of Laser-induced Plasma and Application to Surface-assisted LIBS for Powder and Liquid Samples written by Ye Tian and published by . This book was released on 2017 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-induced breakdown spectroscopy (LIBS) is an analytical method with optical emission spectroscopy that uses a laser pulse to vaporize, atomize, and excite a hot plasma as the spectroscopic emission source. Although LIBS has demonstrated its versatility and attractive features in many fields, the quantitative analysis ability of LIBS is considered as its Achilles' heel. From a fundamental point of view, this can be due to the complex nature of laserinduced plasma as the spectroscopic emission source for LIBS application. The temporal and spatial characterization of laser-induced plasma is considered as one of the key points for the LIBS technique. On the other hand, from the analytical point of view, LIBS is usually characterized by direct laser ablation. This can be however quite limiting, especially for some types of materials such as powders or liquids. Proper sample preparation or treatment allowing the deposition of a thin homogeneous film on a metallic surface could greatly improve the analytical performance of LIBS for these types of materials. Since the metallic surface is expected to contribute to increase the temperature and the density of the plasma and, consequently, to a better overall sensitivity, we call this technique surface-assisted LIBS. The present thesis work is therefore motivated by two basic aspects of LIBS analysis: the need of an improved knowledge of laser-induced plasma as a spectroscopic emission source, and new methods to improve the analytical performance of LIBS, including a higher sensibility and a reduced matrix effect. The first part of this thesis (Chapter 2) is dedicated to an extensive characterization of the plasma induced on glass samples, as a function of the laser wavelength, infrared (IR) or ultraviolet (UV), and the ambient gas, air or argon. Both the spectroscopic imaging and time- and space-resolved emission spectroscopy are used for plasma diagnostics in this work. The second part of this thesis is to develop a surface-assisted LIBS method for the elemental analysis in powders, and in wines as examples of liquids. We applied the surface-assisted LIBS for the quantitative elemental analysis in cellulose powders, alumina powders, and soils (Chapter 3). Special attentions are paid on the figures-of-merit, matrix effects, and normalization approaches in LIBS analysis. We also used the surfaceassisted LIBS for the classification of French wines according to their production regions (Chapter 4). Two classification models based on the principal component analysis (PCA) and random forest (RF) are used for the classification. Through these applications, this thesis work demonstrates the efficiency of the surface-assisted LIBS method for the analysis of powders (cellulose, alumina and soils) and of liquids (wines), with ppm or sub-ppm sensitivities and a reduced matrix effect.

Proceedings of the 7th International Conference on the Applications of Science and Mathematics 2021

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Publisher : Springer Nature
ISBN 13 : 9811689032
Total Pages : 464 pages
Book Rating : 4.8/5 (116 download)

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Book Synopsis Proceedings of the 7th International Conference on the Applications of Science and Mathematics 2021 by : Aida Binti Mustapha

Download or read book Proceedings of the 7th International Conference on the Applications of Science and Mathematics 2021 written by Aida Binti Mustapha and published by Springer Nature. This book was released on 2022-06-28 with total page 464 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents peer-reviewed articles and recent advances on the potential applications of Science and Mathematics for future technologies, from the 7th International Conference on the Applications of Science and Mathematics (SCIEMATHIC 2021), held in Malaysia. It provides an insight about the leading trends in sustainable Science and Technology. The world is looking for sustainable solutions to problems more than ever. The synergistic approach of mathematicians, scientists and engineers has undeniable importance for future technologies. With this viewpoint, SCIEMATHIC 2021 has the theme “Quest for Sustainable Science and Mathematics for Future Technologies”. The conference brings together physicists, mathematicians, statisticians and data scientists, providing a platform to find sustainable solutions to major problems around us. The works presented here are suitable for professionals and researchers globally in making the world a better and sustainable place.

Spectrochemical Analysis of Solid Samples by Laser-induced Plasma Spectroscopy

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Book Synopsis Spectrochemical Analysis of Solid Samples by Laser-induced Plasma Spectroscopy by :

Download or read book Spectrochemical Analysis of Solid Samples by Laser-induced Plasma Spectroscopy written by and published by . This book was released on 2006 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-induced plasma spectroscopy (LIPS) is a powerful tool for the multi-element analysis of a huge variety of solid, liquid, and gaseous samples of industrial relevance. For LIPS an intense, pulsed laser beam (typically a Nd:YAG or excimer laser) is focused on the sample of interest, resulting in an evaporation, atomization, and partial ionization of the sample in an expanding plasma cloud. After a delay of some hundred nanoseconds to discriminate against the recombination background, the elemental composition of the sample can be determined via the spectrally and temporally resolved detection of the characteristic atomic and ionic emissions. Due to the minimum sample preparation, the low cost for a single measurement, and the potential for an extensive automation, LIPS is an attractive approach to process analysis. The objective of this work to extend the range of elements, which can be analyzed by LIBS, via observation of atomic emission in the VUV range. This permits not only a multielement analysis of metals, but also access to emission lines of metalloids such as S, P, N, O, C, and As. Two experimental set-ups for VUV-LIBS are presented: A set-up for bulk analysis based on conventional Czerny-Turner monochromator and a new echelle spectrograph for high spectral resolution (> 10 000) in the spectral range 150-300 nm. Applying an appropriate beam shaping (3micro focusing4), LIPS allows a fast spatially resolved elemental characterization of surfaces with a typical resolution of 10 mm. Using a UV laser beam (l = 266 nm) for plasma ignition, fractionization effects can be minimized and a quantitative analysis can be performed. Analysis of the spectra from the single pulses permit a depth- and spatially resolved investigation of a sample.

Laser-induced Breakdown Spectroscopy (LIBS)

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ISBN 13 : 9780511246692
Total Pages : 640 pages
Book Rating : 4.2/5 (466 download)

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Book Synopsis Laser-induced Breakdown Spectroscopy (LIBS) by : Andrzej W. Miziolek

Download or read book Laser-induced Breakdown Spectroscopy (LIBS) written by Andrzej W. Miziolek and published by . This book was released on 2014-05-14 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the first comprehensive reference explaining the fundamentals of the LIBS phenomenon, its history and its fascinating applications across eighteen chapters written by recognized leaders in the field. This book will be of significant interest to researchers in chemical and materials analysis within academia and industry.

Space and Time Characterization of Laser-induced Plasmas for Applications in Chemical Analysis and Thin Film Deposition

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ISBN 13 :
Total Pages : pages
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Book Synopsis Space and Time Characterization of Laser-induced Plasmas for Applications in Chemical Analysis and Thin Film Deposition by : Mahmoud Dawood

Download or read book Space and Time Characterization of Laser-induced Plasmas for Applications in Chemical Analysis and Thin Film Deposition written by Mahmoud Dawood and published by . This book was released on 2014 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Laser-induced Plasma on Polymeric Materials and Applications for the Discrimination and Identification of Plastics

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ISBN 13 :
Total Pages : 0 pages
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Book Synopsis Laser-induced Plasma on Polymeric Materials and Applications for the Discrimination and Identification of Plastics by : Myriam Boueri

Download or read book Laser-induced Plasma on Polymeric Materials and Applications for the Discrimination and Identification of Plastics written by Myriam Boueri and published by . This book was released on 2010 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-Induced Breakdown Spectroscopy (LIBS) is an analytical technique that has the potential to detect all the elements present in the periodic table. The limit of detection can go below a few ppm and this regardless of the physical phase of the analyzed sample (solid, liquid or gas). Its simplicity of use, its rapidity to get results and its versatility provide this technique with attractive features. The technique is currently developed for applications in a large number of domains such as online control, spatial explorations and the environment. However the weakness of the LIBS technique, compared to other more conventional ones, is still its difficulty in providing reliable quantitative results, especially for inhomogeneous and complex matrix such as organic or biological materials. The work presented in this thesis includes a study of the properties of plasma induced from different organic materials. First, a study of the plasma induced on the surface of a Nylon sample at short time delays (~ns) was carried out using the time-resolved shadowgraph technique for different experimental parameters (laser energy, pulse duration, wavelength). Then, a complete diagnostics of the plasma was performed using the plasma emission spectroscopy. A detailed analysis of the emission spectra at different detection delays allowed us to determine the evolution of the temperatures of the different species in the plasma (atoms, ions and molecules). The homogeneity and the local thermodynamic equilibrium within the plasma was then experimentally checked and validated. We demonstrated that the optimisation of the signalto- noise ratio and a quantitative procedure, such as the calibration-free LIBS, can be put in place within a properly chosen detection window. In our experiments, such optimised detection configuration was further employed to record LIBS spectra from different families of polymer in order to identify and classify them. For this purpose, the chemometrics procedure of artificial neural networks (ANN) was used to process the recorded LIBS spectroscopic data. The promising results obtained in this thesis makes LIBS stand out as a potentially useful tool for real time identification of plastic materials. Finally, this work can also be considered as a base for the further studies of more complex materials such as biological tissues with LIBS.

Temporal and Spatial Characteristics of Laser-induced Plasma on Organic Materials and Quantitative Analysis of the Contained Inorganic Elements

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Book Synopsis Temporal and Spatial Characteristics of Laser-induced Plasma on Organic Materials and Quantitative Analysis of the Contained Inorganic Elements by : Wenqi Lei

Download or read book Temporal and Spatial Characteristics of Laser-induced Plasma on Organic Materials and Quantitative Analysis of the Contained Inorganic Elements written by Wenqi Lei and published by . This book was released on 2012 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: This PhD work was devoted to the understanding of the laser-induced plasma on organic materials and theapplication of laser-induced breakdown spectroscopy (LIBS) to quantitative analysis of these materials. Itcontributes to deepen our knowledge on the physical mechanisms involved in laser-matter interaction, plasmageneration, evolution and expansion of the plasma into the ambient gas, with emphasis on plasmas induced onorganic targets. It also intends to improve the performance of LIBS for the analysis of organic materials. Thespecificity for organic targets fits the current focus of the international community working on LIBS, toimprove the control of the plasma induced on this kind of material which has a distinguished optical prosperitywith respect to that of metals, better known for laser ablation. It addresses also the growing need to apply theLIBS technique to organic materials for different applications in the environmental, food, or biomedicaldomains. The works in this thesis were therefore presented in this thesis document according to the followingorganization.After the General Introduction which introduces the scientific and technological contexts, Chapter Irecalls the basic theoretical elements necessary to understand the phenomenon of plasma generation by laserablation, and its evolution in the background gas. Ablation of organic material is emphasized. Procedures andtechniques of diagnostics of laser-induced plasma were then presented with a focus on the transient andinhomogeneous nature of the expanding plasma. Chapter II focuses on the generation and the evolution of theplasma induced on the skin of a potato, a typical sample of agricultural product. The characteristics of plasmainduced on a soft and wet organic target, such as a fresh potato, was something unknown when the thesis workstarted. These characteristics provide the necessary basis for the quantitative analysis of the trace andultra-trace metallic elements in these samples. Following this characterization, semi-quantitative analyticalresults were extracted from LIBS spectra corresponding to potato skin. Chapter III is presented in thecontinuity of Chapter II for the application of LIBS to the quantitative analysis of organic materials. Acomparative study on the analytical results with LIBS and ICP-AES for milk powders allows an assessment ofthe performances of quantitative analysis by LIBS for organic materials, and a validation of the CF-LIBSprocedure that we have developed. Different from Chapters II and III where attention was paid to trace metalelements, Chapter IV studies the behavior of the major elements that make up the matrix of organic material,which are 4 known organic elements: H, C, O, N. During the decomposition of organic material by laserablation, these elements can be found in the form of molecular fragments, or recombined into molecularspecies. We then study in this Chapter the evolution of these species as a function of the laser ablationparameters, the laser wavelength in particular. The thesis document ends with a general conclusion andoutlooks.

Investigation of Physical and Spectral Characteristics of Laser-induced Plasmas

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ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (495 download)

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Book Synopsis Investigation of Physical and Spectral Characteristics of Laser-induced Plasmas by : Vincent P. Hohreiter

Download or read book Investigation of Physical and Spectral Characteristics of Laser-induced Plasmas written by Vincent P. Hohreiter and published by . This book was released on 2005 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: ABSTRACT: The physical and optical characteristics of laser-induced plasmas (LIP) and the precision of measurements using laser-induced breakdown spectroscopy (LIBS) for aerosol and gas phase species are explored. In a series of coherent experiments properties of the LIP and the temporal, spatial, and energetic variations of interactions with entrained particles (aerosols) are evaluated from both a standpoint of basic plasma science and applied atomic spectroscopy. First, the evolution of a LIP is characterized in terms of its temporally-resolved spectral absorptivity, spectral emissivity, and free electron density during the first 500 nanoseconds. Transmission measurements reveal near opacity of the LIP at early times (10-50 ns) and essential transparency at longer times (500 ns).

Laser Ablation in Liquids

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Publisher : CRC Press
ISBN 13 : 9814241520
Total Pages : 1166 pages
Book Rating : 4.8/5 (142 download)

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Book Synopsis Laser Ablation in Liquids by : Guowei Yang

Download or read book Laser Ablation in Liquids written by Guowei Yang and published by CRC Press. This book was released on 2012-02-22 with total page 1166 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book focuses on the fundamental concepts and physical and chemical aspects of pulsed laser ablation of solid targets in liquid environments and its applications in the preparation of nanomaterials and fabrication of nanostructures. The areas of focus include basic thermodynamic and kinetic processes of laser ablation in liquids, and its applic

Plasma Imaging as a Diagnostic Tool for Laser-induced Breakdown Spectroscopy

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ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (894 download)

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Book Synopsis Plasma Imaging as a Diagnostic Tool for Laser-induced Breakdown Spectroscopy by : Jessica Mcnutt

Download or read book Plasma Imaging as a Diagnostic Tool for Laser-induced Breakdown Spectroscopy written by Jessica Mcnutt and published by . This book was released on 2014 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-induced breakdown spectroscopy (LIBS) has been identied as a promising technique for the detection and characterization of nuclear materials and other materials relevant for nuclear forensics and international safeguards applications. LIBS is a material characterization method whereby a short-pulse, high-intensity laser is focused on the surface of a target to generate a plasma for spectral analysis to determine the elemental and potentially isotopic composition of the target. Shadowgraphic and fast-frame photographic imaging are two established techniques used to study the time-evolution and the rate of expansion of laser-produced plasmas over hundreds of nanoseconds. The modication of a LIBS experimental setup to include the capability to take photographic images and high-temporal resolution shadowgraphic images is presented. Analysis of uranium samples was performed in air and vacuum conditions. Shadowgraphic imaging was used to analyze laser produced plasma evolution in the rst 8 ns following laser-energy deposition on the surface. Algorithms were developed to measure the plasma radius as a function of time and the results of that analysis were compared to the Sedov-Taylor model.

Laser Produced Plasmas in Liquid Environments

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ISBN 13 :
Total Pages : 0 pages
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Book Synopsis Laser Produced Plasmas in Liquid Environments by : Nichola Walsh

Download or read book Laser Produced Plasmas in Liquid Environments written by Nichola Walsh and published by . This book was released on 2016 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: During the interaction of an intense laser pulse with a solid metal target, a high temperature, high density plasma is formed. Pulsed laser ablation has attracted much interest over the past fifty years with experimental and theoretical work largely focussed on the study of laser produced plasmas in vacuum. The study of pulsed laser ablation has been largely motivated from a materials processing perspective, with the characterisation of thin films using pulsed laser deposition of particular interest. Another application resulting from the study of laser produced plasmas is the use of laser-induced breakdown spectroscopy (LIBS) for elemental composition and quantitative analysis of samples. LIBS is now a widely used technique employed in various fields including environmental analysis, forensics and biomedical applications. While much work has been carried out on pulsed ablation of materials in vacuum and gas ambient, comparatively little research has been done on ablation in liquid media. As a result, the fundamental understanding of laser produced plasmas in liquids remains insufficient. Using techniques such as time resolved imaging and spectroscopy, a full characterisation of the plasma formed in air was undertaken as a comparison to the subsequent investigation of the plasma formed in water ambient. Single pulse studies revealed information on the dynamic evolution of a laser plasma formed in the liquid phase where strong confinement and broadband emission were the main observations. Shadowgraphy measurements were performed to examine the dynamic behaviour of the cavitation bubble that eventually forms post plasma ignition. The results of time resolved optical emission measurements from within the cavitation bubble using a second laser pulse reveal for the first time the full dynamic evolution of the plasma formed in such an environment.

Diagnostic and Analytical Studies of Laser Induced Plasmas

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ISBN 13 :
Total Pages : pages
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Book Synopsis Diagnostic and Analytical Studies of Laser Induced Plasmas by : Heh Young Moon

Download or read book Diagnostic and Analytical Studies of Laser Induced Plasmas written by Heh Young Moon and published by . This book was released on 2010 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: ABSTRACT: Since its early applications, Laser-Induced Breakdown Spectroscopy (LIBS) has been recognized as a useful tool for solid state chemical analysis due to its numerous attractive advantages as an analytical tool: e.g., simultaneous multi-element detection capability, no sample preparation, rapid or real-time analysis, and allowing in situ analysis requiring only optical access to the sample. However, the quantitative accuracy of the technique depends on the complex fundamental processes involved in laser-induced plasma formation, ablation, atomization, excitation and ion recombination. Thus, problems arising from laser target coupling, matrix effects, line interferences, fractionation in target vaporization, the main assumptions of the methods, namely the optically thin emission of spectral lines and the existence of local thermodynamic equilibrium in the plasma should be properly addressed in order to obtain reliable quantitative results [1, 2] . The general scope of this research encompasses two aspects related to the LIBS technique: one aspect is the fundamental study of the plasma characteristics and another is an improved use of the technique in quantitative analysis. The main project is to revisit and investigate some fundamental assumptions such as the existence of local.

Laser-Induced Breakdown Spectroscopy

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Publisher : Elsevier
ISBN 13 : 0128188308
Total Pages : 624 pages
Book Rating : 4.1/5 (281 download)

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Book Synopsis Laser-Induced Breakdown Spectroscopy by : Jagdish P. Singh

Download or read book Laser-Induced Breakdown Spectroscopy written by Jagdish P. Singh and published by Elsevier. This book was released on 2020-06-02 with total page 624 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser-Induced Breakdown Spectroscopy, Second Edition, covers the basic principles and latest developments in instrumentation and applications of Laser Induced Breakdown Spectroscopy (LIBS). Written by active experts in the field, it serves as a useful resource for analytical chemists and spectroscopists, as well as graduate students and researchers engaged in the fields of combustion, environmental science, and planetary and space exploration. This fully revised second edition includes several new chapters on new LIBS techniques as well as several new applications, including flame and off-gas measurement, pharmaceutical samples, defense applications, carbon sequestration and site monitoring, handheld instruments, and more. LIBS has rapidly developed into a major analytical technology with the capability of detecting all chemical elements in a sample, of real- time response, and of close-contact or stand-off analysis of targets. It does not require any sample preparation, unlike conventional spectroscopic analytical techniques. Samples in the form of solids, liquids, gels, gases, plasmas, and biological materials (like teeth, leaves, or blood) can be studied with almost equal ease. This comprehensive reference introduces the topic to readers in a simple, direct, and accessible manner for easy comprehension and maximum utility. Covers even more applications of LIBS beyond the first edition, including combustion, soil physics, environment, and life sciences Includes new chapters on LIBS techniques that have emerged in the last several years, including Femtosecond LIBS and Molecular LIBS Provides inspiration for future developments in this rapidly growing field in the concluding chapter

Characterization of Laser Induced Plasmas

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ISBN 13 :
Total Pages : 94 pages
Book Rating : 4.:/5 (26 download)

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Book Synopsis Characterization of Laser Induced Plasmas by : David Scott Jebens

Download or read book Characterization of Laser Induced Plasmas written by David Scott Jebens and published by . This book was released on 1990 with total page 94 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Emission Characteristics of Laser-Induced Plasma Using Collinear Long and Short Dual-Pulse Laser-Induced Breakdown Spectroscopy (LIBS).

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ISBN 13 :
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Book Synopsis Emission Characteristics of Laser-Induced Plasma Using Collinear Long and Short Dual-Pulse Laser-Induced Breakdown Spectroscopy (LIBS). by :

Download or read book Emission Characteristics of Laser-Induced Plasma Using Collinear Long and Short Dual-Pulse Laser-Induced Breakdown Spectroscopy (LIBS). written by and published by . This book was released on with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Lasers-Induced Plasmas and Applications

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Publisher : CRC Press
ISBN 13 : 1000147371
Total Pages : 474 pages
Book Rating : 4.0/5 (1 download)

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Book Synopsis Lasers-Induced Plasmas and Applications by : Leon J. Radziemski

Download or read book Lasers-Induced Plasmas and Applications written by Leon J. Radziemski and published by CRC Press. This book was released on 2020-09-11 with total page 474 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book discusses the physics of plasma initiation and reviews the features of dissipating, propagating plasmas. It deals with advances in diagnostics for high-energy, laser-fusion plasmas. The book reviews the basic physical processes, plasma characteristics of the "continuous optical discharge".

Lasers-Induced Plasmas and Applications

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Publisher : CRC Press
ISBN 13 : 9780824780784
Total Pages : 476 pages
Book Rating : 4.7/5 (87 download)

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Book Synopsis Lasers-Induced Plasmas and Applications by : Radziemski

Download or read book Lasers-Induced Plasmas and Applications written by Radziemski and published by CRC Press. This book was released on 1989-06-28 with total page 476 pages. Available in PDF, EPUB and Kindle. Book excerpt: Providing an interdisciplinary approach to plasma engineering and techniques, the book contains a timely examination of the physics of laser-induced breakdown.