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Bench Scale Development Of Mild Gasification Char Desulfurization Technical Report 1 March 31 May 1994
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Book Synopsis Bench-scale Development of Mild Gasification Char Desulfurization. Technical Report, 1 March--31 May 1994 by :
Download or read book Bench-scale Development of Mild Gasification Char Desulfurization. Technical Report, 1 March--31 May 1994 written by and published by . This book was released on 1994 with total page 23 pages. Available in PDF, EPUB and Kindle. Book excerpt: The goal of this project is to scale up a process, developed under a previous ICCI grant, for desulfurization of mild gasification char by treatment with hydrogen-rich process-derived fuel gas at 650--760 C and 7--15 atm. The char can be converted into a low-sulfur metallurgical form coke. In the prior study, IBC-105 coal with 4.0 wt% sulfur was converted to chars with less than 1.0 wt% sulfur in a laboratory-scale batch reactor. The susceptibility of the char to desulfurization was correlated with physicochemical char properties and mild gasification conditions. Acid pretreatment of the coal prior to mild gasification was also shown to significantly enhance subsequent sulfur removal. In this study, IGT is conducting continuous bench-scale tests in a 1-lb/h fluidized-bed reactor to determine the preferred process conditions and obtain steady-state data necessary for process design and scale-up. The desulfurized chars are to be used to produce low-sulfur form coke, which will be evaluated for density, reactivity, and strength properties relevant to utilization in blast furnaces. This quarter, 2,500 g of mild gasification char was produced from untreated IBC-105 coal in the bench-scale reactor. Half of this char will be subjected to sulfuric acid treatment to enhance subsequent desulfurization. Char-producing runs were also initiated with acid-pretreated coal, which will produce about 1,250 g of char.
Book Synopsis Bench-scale Development of Mild Gasification Char Desulfurization. Technical Report, 1 December 1993--28 February 1994 by :
Download or read book Bench-scale Development of Mild Gasification Char Desulfurization. Technical Report, 1 December 1993--28 February 1994 written by and published by . This book was released on 1994 with total page 21 pages. Available in PDF, EPUB and Kindle. Book excerpt: The goal of this project is to scale up a process, developed under a previous ICCI grant, for desulfurization of mild gasification char by treatment with hydrogen-rich process-derived fuel gas at 650--760 C and 7-15 atm. The char can be converted into a low-sulfur metallurgical form coke. In the prior study, IBC-105 coal with 4.0 wt % sulfur was converted to chars with less than 1.0 wt% sulfur was converted to chars with less than 1.0 wt % sulfur in a laboratory-scale batch reactor. The susceptibility of the char to desulfurization was correlated with physicochemical char properties and mild gasification conditions. Acid pretreatment of the coal prior to mild gasification was also shown to significantly enhance subsequent sulfur removal. In this study, IGT is conducting continuous bench-scale tests in a 1-lb/h fluidized-bed reactor to determine the preferred process conditions and obtain steady-state data necessary for process conditions and obtain steady-state data necessary for process design and scale-up. The desulfurized chars are to be used to produce low-sulfur form coke, which will be evaluated for density, reactivity, and strength properties relevant to utilization in blast furnaces. During the second quarter, the authors completed the acid pretreatment of 25 lb (11 kg) of the 40 x 80-mesh IBC-105 coal and 7 lb (3 kg) of carbonizer char. Modifications of the bench-scale fluidized-bed reactor were completed, permitting extended-duration char-producing runs with caking coal. Char-producing runs were initiated at 1100 F and 20 psig in nitrogen, and will continue into the third quarter.
Book Synopsis Bench-scale Development of Mild Gasification Char Desulfurization: Technical Report, September 1, 1993 Through November 30, 1993 by :
Download or read book Bench-scale Development of Mild Gasification Char Desulfurization: Technical Report, September 1, 1993 Through November 30, 1993 written by and published by . This book was released on 1994 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Energy Research Abstracts written by and published by . This book was released on 1994-12 with total page 508 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Bench-scale Development of Mild Gasification Char Desulfurization by :
Download or read book Bench-scale Development of Mild Gasification Char Desulfurization written by and published by . This book was released on 1994 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Response apologétique aux prétendus moyens de nullité proposés par les Doyen et Chanoines de l'Eglise de Rouen sur le rétablissement de la discipline ecclésiastique by :
Download or read book Response apologétique aux prétendus moyens de nullité proposés par les Doyen et Chanoines de l'Eglise de Rouen sur le rétablissement de la discipline ecclésiastique written by and published by . This book was released on 1855 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Bench-scale Demonstration of Hot-gas Desulfurization Technology. Quarterly Technical Progress Report, January 1--March 31, 1994 by :
Download or read book Bench-scale Demonstration of Hot-gas Desulfurization Technology. Quarterly Technical Progress Report, January 1--March 31, 1994 written by and published by . This book was released on 1994 with total page 11 pages. Available in PDF, EPUB and Kindle. Book excerpt: The U.S. Department of Energy (DOE), Morgantown Energy Technology Center (METC), is sponsoring research in advanced methods for controlling contaminants in hot coal gasifier gas (coal gas) streams of integrated gasification combined-cycle (IGCC) power systems. Through bench-scale development, both fluidized-bed zinc titanate and Direct Sulfur Recovery Process (DSRP) technologies have been shown to be technically and economically attractive. In the zinc titanate approach, sulfur dioxide is the produced and must be disposed of in an environmentally sound manner. In the DSRP, elemental sulfur is the catalytic product.
Book Synopsis Government Reports Announcements & Index by :
Download or read book Government Reports Announcements & Index written by and published by . This book was released on 1995 with total page 682 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Investigation of a Technique for Sulfur Reduction of Mild Gasification Char. Technical Report, March 1--May 31, 1992 by :
Download or read book Investigation of a Technique for Sulfur Reduction of Mild Gasification Char. Technical Report, March 1--May 31, 1992 written by and published by . This book was released on 1992 with total page 19 pages. Available in PDF, EPUB and Kindle. Book excerpt: The object of this program is to investigate the desulfurization of mild gasification char using H2:CH4 mixtures at the laboratory scale. Mild gasification is a coal conversion technique which produces solid, liquid, and gaseous co-products at 1100°--1500°F and near-ambient pressure. Char comprises about 60 to 70% of the dry coal yield. Form coke for steelmaking and foundries presents potential high-value markets for chars from eastern bituminous coals. Conventional metallurgical cokes generally contain less than 1 wt% sulfur, and mild gasification char from high-sulfur Illinois coals must be upgraded to meet these criteria. One method to accomplish this is desulfurization with reducing gases derived from the co-product gases. Because form coke has a market value up to $200/ton, it can accommodate desulfurization costs and still be economically attractive. In the first year of the two-year program, granular char is being treated with H2:CH4 blends at temperatures of 1100°--1600°F and pressures of 50--200 psig. The effects of temperature, pressure, residence time, gas velocity, and gas composition on sulfur removal and carbon gasification are being determined. During the third quarter, 10 tests were performed with four chars. Fluidized-bed tests were conducted at 1400--1600°F, 50--200 psig, and 120--240 min residence time. Future tests will focus on determining the key properties that determine the susceptibility of char to hydrodesulfurization with minimal carbon conversion.
Book Synopsis Investigation of a Sulfur Reduction Technique for Mild Gasification Char. [Quarterly] Technical Report, March 1--May 31, 1993 by :
Download or read book Investigation of a Sulfur Reduction Technique for Mild Gasification Char. [Quarterly] Technical Report, March 1--May 31, 1993 written by and published by . This book was released on 1993 with total page 26 pages. Available in PDF, EPUB and Kindle. Book excerpt: The objective of this program is to investigate the desulfurization of mild gasification char using H2:CH4 mixtures. Mild gasification of coal produces char, liquids, and gases at 1000°--1500°F and near-ambient pressure. Char, comprising 60--70% of the product, can be used to make high-value form coke for steel making and foundries. However, a sulfur content below 1 wt% is desirable, and char from high-sulfur Illinois coals must be upgraded to meet this criterion. Illinois No. 6 chars were treated in a batch fluidized bed with H2:CH4 blends containing 9--24 vol% CH4 at 1100°--1600°F and 50--200 psig. Sulfur removal up to 92.5 wt% were obtainer, and the char desulfurization susceptibility was related to porosity, density, and crystallite size. The relationships among mild gasification parameters, char properties, and char desulfurization susceptibility are being studied. Acid washing of coal to remove Ca and Fe is being explored for its effect on subsequent sulfur removal, and secondary desulfurization of form coke produced from the desulfurized chars is also being studied. Desulfurization tests of entrained and fluidized-bed reactor chars from IBC-105 coal (4.1--4.3 wt% sulfur) were completed. Desulfurization conditions were 1400°F, 100--200 psig and reactant gas compositions of 15-49 vol% CH4 in H2. Sulfur removal ranged from 28 to 95%, with carbon losses from 5 to 29%. Acid-washing of the coal prior to mild gasification or the char prior to desulfurization increased its susceptibility to desulfurization, with sulfur content reduced to as low as 0.10 wt% dry char. Fluidized-bed chars were easier to desulfurize than entrained chars, and were less affected by acid-washing.
Book Synopsis Bench-scale Demonstration of Hot-gas Desulfurization Technology. Quarterly Technical Progress Report, July 1, 1994-September 30, 1994 by :
Download or read book Bench-scale Demonstration of Hot-gas Desulfurization Technology. Quarterly Technical Progress Report, July 1, 1994-September 30, 1994 written by and published by . This book was released on 1995 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Government Reports Annual Index by :
Download or read book Government Reports Annual Index written by and published by . This book was released on 1994 with total page 1692 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Book Synopsis Investigation of a Technique for Sulfur Reduction of Mild Gasification Char. Final Technical Report, September 1, 1991--August 31, 1992 by :
Download or read book Investigation of a Technique for Sulfur Reduction of Mild Gasification Char. Final Technical Report, September 1, 1991--August 31, 1992 written by and published by . This book was released on 1992 with total page 34 pages. Available in PDF, EPUB and Kindle. Book excerpt: The objective of this program is to investigate the desulfurization of mild gasification char using H2:CH4, mixtures at the laboratory scale. Mild gasification produces solid, liquid, and gaseous co-products at 1000° to 1500°F and near-ambient pressure. Char comprises about 60 to 70% of the dry coal yield. Form coke for steelmaking and foundries presents potential high-value markets for chars from eastern bituminous coals, Metallurgical cokes generally contain less than 1 wt% sulfur, and mild gasification char from high-sulfur Illinois coals must be upgraded to meet these criteria. One method to accomplish this is desulfurization with reducing gases derived from the.co-product gases. In the first year of the two-year program, granular chars were treated with H2:CH4, blends at temperatures of 1100° to 1600°F and pressures of 50 to 200 psig. During the year, 23 tests were performed with 10 chars. Fluidized-bed tests were conducted for 120 to 240 minutes with superficial gas velocities from 0.067 to 0.150 ft/s. The desulfurization medium was H2 gas containing 9 to 24 vol% CH4. The data from these tests show sulfur conversions ranging from 6.0 to 92.5 wt%, with carbon conversions from zero to 35.3 wt%. The maximum sulfur conversion was 92.5 wt% at 1400°F and 200 psig in 76% H, for 120 minutes residence time, using IFFR char produced from IBC-106 coal at 1200°F in helium. The sulfur content of the char in that test was reduced from 3.78 to 0.39 wt%.
Book Synopsis Mild Gasification Technology Development Process by :
Download or read book Mild Gasification Technology Development Process written by and published by . This book was released on 1990 with total page 51 pages. Available in PDF, EPUB and Kindle. Book excerpt: The overall objective of this program is to develop mild gasification technology and co-product utilization. The objective of Task 3 was to investigate the necessary steps for upgrading the mild gasification char into potential high-market-value solid products. Recommendations of the Task 1 market survey section formed the basis for selecting three value-added solid products from mild gasification char: form coke, smokeless fuel, and activated adsorbent char. The formation and testing for the form coke co-product involved an evaluation of its briquette strength and reactivity. The measured tensile strength and reactivity of the form coke sample briquettes were in the range of commercial coke, and development tests on a larger scale are recommended. The reaction rate of the form coke carbon with carbon dioxide at 1825°F was measured using a standard procedure. A smokeless fuel briquette with limestone added to control sulfur can be made from mild gasification char in a simple manner. Test results have shown that briquettes with limestone have a heating value comparable to other solid fuels and the limestone can retain up to 88% of the sulfur during combustion in a simple bench-scale combustion test, almost all of it as a stable calcium sulfate. Adsorbent chars were prepared with a standard steam activation procedure and tested for a variety of pertinent property and performance values. Such adsorbents may be better suited for use in some areas, such as the adsorption of low-molecular-weight substances, because of the smaller pore sizes measured in the char. 5 refs., 17 figs., 6 tabs.
Book Synopsis Investigation of a Sulfur Reduction Technique for Mild Gasification Char. Final Technical Report, September 1, 1992--August 31, 1993 by :
Download or read book Investigation of a Sulfur Reduction Technique for Mild Gasification Char. Final Technical Report, September 1, 1992--August 31, 1993 written by and published by . This book was released on 1993 with total page 42 pages. Available in PDF, EPUB and Kindle. Book excerpt: The objective of this program is to investigate the desulfurization of mild gasification char using H2:CH4 mixtures. Mild gasification of coal produces char, liquids, and gases at 1000°--1500°F and near-ambient pressure. Char, comprising 60--70% of the product, can be used to make high-value form coke for steel making and foundries. A sulfur content below 1 wt% is desirable, and char from high-sulfur Illinois coals must be upgraded to meet this criterion. In the first year of the program, Illinois No. 6 chars were treated in a batch fluidized bed with H2:CH4 blends containing 9--24 vol% CH4 at 1100°--1600°F and 50--200 psig. Sulfur removals up to 92.5 wt% were obtained, and the char desulfurization susceptibility was related to porosity, density, and carbon crystallite size. During the second year, the relationships among mild gasification parameters, char properties, char desulfurization susceptibility, and form coke properties were studied. Acid washing of coal to remove Ca and Fe was explored for its effect on subsequent sulfur removal, and secondary desulfurization of form coke produced from the desulfurized chars was studied. Desulfurization tests of entrained and fluidized-bed reactor chars from IBC-105 coal were completed. Acid-washing of the coal prior to mild gasification or the char prior to desulfurization increased its susceptibility to desulfurization, with sulfur content reduced to as low as 0.10 wt % dry char. Fluidized-bed chars were easier to desulfurize than entrained chars, with or without acid-washing. Form coke briquettes were prepared from selected chars and mild gasification pitch binder, and then carbonized under both N2 and H2:CH4 atmospheres. carbonization in H2:CH4 removed additional sulfur from the form coke. Adequate tensile strength (837 psi) was achieved in briquettes with 1.2 wt% sulfur made from desulfurized char.
Book Synopsis Investigation of a Sulfur Reduction Technique for Mild Gasification Char. Technical Report, September 1, 1991--November 30, 1991 by :
Download or read book Investigation of a Sulfur Reduction Technique for Mild Gasification Char. Technical Report, September 1, 1991--November 30, 1991 written by and published by . This book was released on 1991 with total page 14 pages. Available in PDF, EPUB and Kindle. Book excerpt: The object of this program is to investigate the desulfurization of mild gasification char using hydrogen/methane mixtures in a laboratory-scale experimental study. In the first year of the two- year program, char is being treated with mixtures of H2 and CH4 at temperatures of 1100°C to 1550°F and pressures of 50 to 100 psig. The effects of temperature, pressure, residence time, gas velocity, and gas composition on sulfur removal and carbon gasification are being determined. The batch experiments are being performed in a nominal 2-inch-ID stainless-steel, batch, fluidized-bed reactor. The char to be desulfurized was produced by the IGT mild gasification process research unit (PRU) in a recently completed DOE/METC-sponsored technology development program. The parent coal was Illinois No. 6 from a preparation plant, and the char from the selected test contains 4.58 wt% sulfur. In the first quarter, we have obtained and prepared a char for the desulfurization tests. Ultimate and proximate analyses were performed on this char, and its pore size distribution and surface area were determined. Also this quarter, the fluidized-bed reactor system was constructed and equipped with high pressure mass flow controllers and a high pressure sintered metal filter to remove fines from the effluent gas stream.
Book Synopsis Bench-scale Demonstration of Hot-gas Desulfurization Technology. Quarterly Report, October 1 - December 31, 1995 by :
Download or read book Bench-scale Demonstration of Hot-gas Desulfurization Technology. Quarterly Report, October 1 - December 31, 1995 written by and published by . This book was released on 1995 with total page 28 pages. Available in PDF, EPUB and Kindle. Book excerpt: The US Department of Energy (DOE) Morgantown Energy Technology Center (METC) is sponsoring research in advanced methods for controlling contaminants in hot coal gasifier gas (coal gas) streams of integrated gasification combined-cycle (IGCC) power systems. The programs focus on hot-gas particulate removal and desulfurization technologies that match or nearly match the temperatures and pressures of the gasifier, cleanup system, and power generator. The work seeks to eliminate the need for expensive heat recovery equipment, reduce efficiency losses due to quenching, and minimize wastewater treatment costs. The goal of this project is to continue further development of the zinc titanate desulfurization and direct sulfur recovery process (DSRP) technologies by (1) scaling up the zinc titanate reactor system; (2) developing an integrated skid-mounted zinc titanate desulfurization-DSRP reactor system; (3) testing the integrated system over an extended period with real coal-gas from an operating gasifier to quantify the degradative effect, if any, of the trace contaminants present in coal gas; (4) developing an engineering database suitable for system scaleup; and (5) designing, fabricating and commissioning a larger DSRP reactor system capable of operating on a six-fold greater volume of gas than the DSRP reactor used in the bench-scale field test. The work performed during the October 1 through December 31, 1995 is described.
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