Hyphenated and Alternative Methods of Detection in Chromatography

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Publisher : CRC Press
ISBN 13 : 084939077X
Total Pages : 311 pages
Book Rating : 4.8/5 (493 download)

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Book Synopsis Hyphenated and Alternative Methods of Detection in Chromatography by : R. Andrew Shalliker

Download or read book Hyphenated and Alternative Methods of Detection in Chromatography written by R. Andrew Shalliker and published by CRC Press. This book was released on 2011-12-14 with total page 311 pages. Available in PDF, EPUB and Kindle. Book excerpt: Widely employed for separating and detecting chemicals in solution, separation techniques are most often applied in tandem, subsequently referred to as hyphenated methods. Hyphenated and Alternative Methods of Detection in Chromatography details the development and application of mass spectral detection techniques coupled with gas phase and liquid phase chromatographies. With contributions from experts in a variety of fields, as evidenced by the range of topics, the book describes the advantages and disadvantages of various separation techniques and addresses methods for cutting-edge applications such as proteomics research. Specifically, this book covers: The development of the LC-NMR and its application in chromatographic science, particularly in relation to the analysis of natural and environmental samples and in the study of reaction monitoring, biosynthetic analysis, and structural elucidation The application of LC-ICP in biological samples for the speciation of organoarsenic and organoselenium compounds; metal complexes in microorganisms, plants, and foods of plant origin; human body fluids and tissues; and in the detection of chemical warfare agents Electrochemical detection in liquid chromatography, system optimization, and applications in the analysis of flavonoids The use of chemiluminescence for microcolumn and capillary methods of separation The process of employing multidimensional separation methods as a means of identifying components in complex samples A detailed reference for those starting out in the field, this book also suits those who are more experienced yet require assistance in new directions. It is an ideal reference for senior undergraduate and postgraduate students wishing to supplement their learning experience. Containing over 800 references, this book is an excellent source of information within the field of hyphenated methods of chromatographic analysis.

Analyse chimique

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Author :
Publisher : Elsevier Masson
ISBN 13 : 9782225854453
Total Pages : 372 pages
Book Rating : 4.8/5 (544 download)

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Book Synopsis Analyse chimique by : Francis Rouessac

Download or read book Analyse chimique written by Francis Rouessac and published by Elsevier Masson. This book was released on 1997-01-01 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt: Le principe adopté est de relier les aspects pratiques de chaque méthode étudiée aux notions scientifiques qui l'expliquent. L'ouvrage est divisé en trois sections : Les méthodes séparatives (chromatographie et électrophorèse), Les méthodes d'analyse spectrales (RMN, IR, UV, fluorimétrie, fluorescence X, absorption et émission atomique), les autres méthodes (spectrométrie de masse, méthodes avec marquage, électro-chimie)

Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues

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Publisher : Elsevier
ISBN 13 : 0080454402
Total Pages : 509 pages
Book Rating : 4.0/5 (84 download)

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Book Synopsis Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues by : A.R. Fernandez Alba

Download or read book Chromatographic-Mass Spectrometric Food Analysis for Trace Determination of Pesticide Residues written by A.R. Fernandez Alba and published by Elsevier. This book was released on 2004-12-11 with total page 509 pages. Available in PDF, EPUB and Kindle. Book excerpt: The trace determination of pesticides continues to be a topic for analytical chemists working in research centres, government and universities. With four chapters devoted to chromatography-mass spectrometry methods, readers are able to understand the analytical basis, technical characteristics and possibilities to evaluate pesticides in food by gas chromatography (GC) and liquid chromatography (LC) mass spectrometry. The book also provides a well-defined and critical compilation of the sample treatment and clean-up procedures, as well as injection techniques applied in GC and LC food analysis. Finally the book deals with aspects related to analytical quality control requirements for pesticide residues, in addition to pesticide regulation aspects.* Contains specific chapters devoted to chromatography-mass spectrometry methods* Provides a well-defined and critical compilation of the sample treatment and clean-up procedures* Contains aspects related to analytical quality control requirements for pesticide residues

Selected Approaches to Gas Chromatography-mass Spectrometry in Laboratory Medicine

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Publisher :
ISBN 13 :
Total Pages : 196 pages
Book Rating : 4.:/5 (3 download)

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Book Synopsis Selected Approaches to Gas Chromatography-mass Spectrometry in Laboratory Medicine by : Robert S. Melville

Download or read book Selected Approaches to Gas Chromatography-mass Spectrometry in Laboratory Medicine written by Robert S. Melville and published by . This book was released on 1975 with total page 196 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Gas Chromatography and Mass Spectrometry: A Practical Guide

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Publisher : Academic Press
ISBN 13 : 0080920152
Total Pages : 633 pages
Book Rating : 4.0/5 (89 download)

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Book Synopsis Gas Chromatography and Mass Spectrometry: A Practical Guide by : O. David Sparkman

Download or read book Gas Chromatography and Mass Spectrometry: A Practical Guide written by O. David Sparkman and published by Academic Press. This book was released on 2011-05-17 with total page 633 pages. Available in PDF, EPUB and Kindle. Book excerpt: The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensible resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on chromatographic peak deconvolution has been added along with a more in-depth understanding of the use of mass spectral databases in the identification of unknowns. Since the last edition, a number of advances in GC inlet systems and sample introduction techniques have occurred, and they are included in the new edition. Other updates include a discussion on fast GC and options for combining GC detectors with mass spectrometry. The section regarding GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types has the same number of compound types as the original edition, but the information in each section has been expanded to not only explain some of the spectra but to also explain why certain fragmentations take place. The number of Appendices has been increased from 12 to 17. The Appendix on Atomic Masses and Isotope Abundances has been expanded to provide tools to aid in determination of elemental composition from isotope peak intensity ratios. An appendix with examples on "Steps to follow in the determination of elemental compositions based on isotope peak intensities" has been added. Appendices on whether to use GC/MS or LC/MS, third-party software for use in data analysis, list of information required in reporting GC/MS data, X+1 and X+2 peak relative intensities based on the number of atoms of carbon in an ion, and list of available EI mass spectral databases have been added. Others such as the ones on derivatization, isotope peak patterns for ions with Cl and/or Br, terms used in GC and in mass spectrometry, and tips on setting up, maintaining and troubleshooting a GC/MS system have all been expanded and updated. - Covers the practical instruction necessary for successful operation of GC/MS equipment - Reviews the latest advances in instrumentation, ionization methods, and quantitation - Includes troubleshooting techniques and a variety of additional information useful for the GC/MS practitioner - A true benchtop reference - A guide to a basic understanding of the components of a Gas Chromatograph-Mass Spectrometer (GC-MS) - Quick References to data interpretation - Ready source for information on new analyses

Gas Chromatography–Mass Spectrometry

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Author :
Publisher : Royal Society of Chemistry
ISBN 13 : 1782629289
Total Pages : 340 pages
Book Rating : 4.7/5 (826 download)

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Book Synopsis Gas Chromatography–Mass Spectrometry by : Diane C Turner

Download or read book Gas Chromatography–Mass Spectrometry written by Diane C Turner and published by Royal Society of Chemistry. This book was released on 2019-11-28 with total page 340 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas chromatography–mass spectrometry (GC-MS) is a powerful way to analyse a range of substances. It is used in everything from food safety to medicine. It has even been used to protect endangered vultures through analysis of poisonous pesticide molecules in their environment! I want to apply this technique, where do I begin? Is GC-MS is the right technique to use? How do I prepare my samples and calibrate the instruments? This textbook has the answers to all these questions and more. Throughout the book, case studies illustrate the practical process, the techniques used and any common challenges. Newcomers can easily search for answers to their question and find clear advice with coloured images on how to get started and all subsequent steps involved in using GC-MS as part of a research process. Readers will find information on collecting and preparing samples, designing and validating methods, analysing results, and troubleshooting. Examples of pollutant, food, oil and fragrance analysis bring the theory to life. The authors use their extensive experience teaching GC-MS theory and practice and draw on their combined backgrounds applying the technique in academic and industry settings to bring this practical reference together. The authors also design and teach the Royal Society of Chemistry’s Pan Africa Chemistry Network GC-MS course, which is supported by GSK.

Gas Chromatographic Environmental Analysis

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Publisher : John Wiley & Sons
ISBN 13 : 9780471187783
Total Pages : 246 pages
Book Rating : 4.1/5 (877 download)

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Book Synopsis Gas Chromatographic Environmental Analysis by : Fabrizio Bruner

Download or read book Gas Chromatographic Environmental Analysis written by Fabrizio Bruner and published by John Wiley & Sons. This book was released on 1993-09-06 with total page 246 pages. Available in PDF, EPUB and Kindle. Book excerpt: Gas Chromatographic Environmental Analysis ist die erste wirklich komplette, aktuelle und einheitliche Darstellung der analytischen Techniken der Umweltchemie in Buchform. Das Buch beschreibt die Grundlagen der Gaschromatographie in der Umweltuntersuchung. Nach einer Einführung in die Gaschromatographie und einer kritischen Bewertung der verschiedenen Säulentypen beschreibt der Autor sorgfältig die notwendige Meßapparatur. Besonderes Augenmerk gilt der Einspritzung sowie den Nachweis- und Kalibrierungssystemen. Ein Akzent liegt auf der Spurenanalytik, die wichtig ist z.B. für die Erkennung von Fluorkohlenwasserstoffen in der Atmosphäre. Daneben werden auch andere Techniken wie HPLC und Massenspektrometrie vorgestellt, um so ein vollständiges Bild der Umweltanalytik von heute und morgen zu geben. Da das Buch für Chemiker und analytische Chemiker sowohl in Forschung als auch Industrie, für Verfahrenstechniker, Umweltbiologen und -geologen geschrieben ist, beschäftigt sich Gas Chromatographic Environmental Analysis besonders mit den Methoden, die in den USA und anderen hochindustrialisierten Staaten eingeführt sind. Damit ist es eine willkommene Bereicherung für die Bibliotheken von chemischen Betrieben, Verwaltungen, Universitäten und Forschungseinrichtungen.

Manuel de spectrométrie de masse à l'usage des biochimistes

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Publisher : Lavoisier
ISBN 13 : 2743017708
Total Pages : 675 pages
Book Rating : 4.7/5 (43 download)

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Book Synopsis Manuel de spectrométrie de masse à l'usage des biochimistes by : Rusconi, Filippo

Download or read book Manuel de spectrométrie de masse à l'usage des biochimistes written by Rusconi, Filippo and published by Lavoisier. This book was released on 2011 with total page 675 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Liquid Chromatography

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Publisher : CRC Press
ISBN 13 : 9780824719364
Total Pages : 654 pages
Book Rating : 4.7/5 (193 download)

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Book Synopsis Liquid Chromatography by : Wilfried M.A. Niessen

Download or read book Liquid Chromatography written by Wilfried M.A. Niessen and published by CRC Press. This book was released on 1998-09-01 with total page 654 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume comprehensively relates developments, principles, and applications of combined liquid chromatography-mass spectrometry and other techniques such as capillary electrophoresis and supercritical fluid chromatography combined with mass spectrometry. It covers historical developments, currently important interfaces and technologies, and LC-MS applications in environmental analysis, pharmaceuticals and bioanalysis, and additional fields. It offers in-depth coverage of interfaces and technologies currently important in the laboratory, especially electrospray and APCI, contains an expanded applications section, and provides over 2200 references, tables, equations, and drawings.

Analyse chimique

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Publisher :
ISBN 13 : 9782100518616
Total Pages : 511 pages
Book Rating : 4.5/5 (186 download)

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Book Synopsis Analyse chimique by : Francis Rouessac

Download or read book Analyse chimique written by Francis Rouessac and published by . This book was released on 2009-06-03 with total page 511 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ce livre s'adresse à un large public d'étudiants en Licences de Sciences de la Matière ou de Sciences de la Vie, en pharmacie, ainsi qu'en IUT. Il offre un panorama détaillé des méthodes d'analyse présentes dans des secteurs aussi variés que les industries chimiques, agroalimentaires, les laboratoires d'analyse médicale, les sciences de l'environnement. Le principe de ce cours est de relier les aspects pratiques de chaque méthode étudiée aux notions scientifiques qui l'expliquent. Abondamment illustré par plus de 300 figures et photos originales, ce livre est organisé en trois sections : les méthodes séparatives (les différentes techniques de chromatographie et d'électrophorèse), les méthodes spectrométriques (UV, IR et Raman, fluorimétrie, fluorescence X, absorption et émission atomique, RMN), et les autres méthodes (spectrométrie de masse, analyses isotopiques et méthodes de marquage, analyseurs spécifiques, électrochimie). Dans cette nouvelle édition, le cours a été entièrement mis à jour pour tenir compte des progrès technologiques les plus récents (chromatographies, spectrométries, RMN...). Des exercices corrigés ont également été ajoutés.

Fundamentals and Techniques

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Publisher : Elsevier
ISBN 13 : 0080858244
Total Pages : 583 pages
Book Rating : 4.0/5 (88 download)

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Book Synopsis Fundamentals and Techniques by :

Download or read book Fundamentals and Techniques written by and published by Elsevier. This book was released on 2000-04-01 with total page 583 pages. Available in PDF, EPUB and Kindle. Book excerpt: Fundamentals and Techniques

Specific Ion Mass Spectrometric Detection for Gas Chromatographic Pesticide Analysis

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Publisher :
ISBN 13 :
Total Pages : 132 pages
Book Rating : 4.:/5 (3 download)

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Book Synopsis Specific Ion Mass Spectrometric Detection for Gas Chromatographic Pesticide Analysis by : Maynard B. Neher

Download or read book Specific Ion Mass Spectrometric Detection for Gas Chromatographic Pesticide Analysis written by Maynard B. Neher and published by . This book was released on 1974 with total page 132 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Basic Gas Chromatography-Mass Spectrometry

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Publisher :
ISBN 13 :
Total Pages : 222 pages
Book Rating : 4.3/5 (91 download)

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Book Synopsis Basic Gas Chromatography-Mass Spectrometry by : F.W. Karasek

Download or read book Basic Gas Chromatography-Mass Spectrometry written by F.W. Karasek and published by . This book was released on 1988-02 with total page 222 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book begins by covering the basic principles of both gas chromatography (GC) and mass spectrometry (MS) to the extent necessary to understand and deal with the data generated in a GC-MS analysis. The focus then turns to the particular requirements created by a direct combination of these two techniques into a single instrumentation system. The data generated and their use are covered in detail. The role of the computer and its specific software receives special attention, especially in the matter of compound identification via mass spectral search techniques. GC-MS-computer instrumentation has reached such a plateau of excellence today that the present commercial systems will not be obsolete for a long time to come. Therefore, a detailed description of these systems is not only informative but is also pertinent to the subject matter of this book. Finally, representative applications and results obtained with GC-MS-computer techniques are presented and chosen in such a way as to permit extrapolation of specific applications to similar problems encountered by the reader. To aid the reader in mastering the subject matter and increase understanding, interpretation problems and suggested readings are included. The format is instructional, informative and application-oriented with material presented in such a way as to be useful to a broad spectrum of people. The book serves as a text in its own right. The software package Gas Chromatography-Mass Spectrometry: A Knowledge Base, by F.A. Settle, Jr. and M.A. Pleva provides rapid access to a wealth of current information in the GC-MS field. Its three diskettes (51/4 inch) allow the user three ways to access: the index mode, the tree mode and a keyword search mode. The package may be purchased separately and is available for the IBM-PC and compatibles. The software provides a valuable supplement to the book.

Reaction Detection in Liquid Chromatography

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Publisher : Routledge
ISBN 13 : 1351419749
Total Pages : 398 pages
Book Rating : 4.3/5 (514 download)

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Book Synopsis Reaction Detection in Liquid Chromatography by : Ira S. Krull

Download or read book Reaction Detection in Liquid Chromatography written by Ira S. Krull and published by Routledge. This book was released on 2017-10-19 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt: The first book to focus entirely on reactions for analyte detection and characterization,Reaction Detection in Liquid Chromatography depicts off- and on-line, pre- and postcolumnapproaches that have been successfully used for many classes of compounds, bothorganic and inorganic, in high performance liquid chromatography.The book gives special attention to methods and instrumentation associated with postcolumnreaction detection, discussing theory, background, principles, and equations .. .and also highlights major areas of reaction chemistry, such as immobilized ( or solution)enzymatic reactions, homogenous solution chemistry, photochemical derivation, pairedionreagents, solid phase and solid supported reagents, and reactions for inorganic species.In addition, Reaction Detection in liquid Chromatography details the efficiencies of thevarious reactions surveyed ... forecasts how the utility of each reaction is likely to be enhancedby new research ... and gives data that will allow the reader to reproducereaction-detection approaches for new analytes and samples.Reaction Detection in Liquid Chromatography is essential reading for analytical, bioanalytical,quality control, and research and development chemists. It also comprises a finereference for analysts involved in development and applications of liquid chromatographyfor specific qualitative and quantitative analyte identification; and in-house, professionalseminars.

Analyse chimique

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Publisher :
ISBN 13 : 9782100049714
Total Pages : 430 pages
Book Rating : 4.0/5 (497 download)

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Book Synopsis Analyse chimique by : Francis Rouessac

Download or read book Analyse chimique written by Francis Rouessac and published by . This book was released on 2000 with total page 430 pages. Available in PDF, EPUB and Kindle. Book excerpt: Cet ouvrage offre un panorama très détaillé des méthodes actuelles d'analyse présentes dans des secteurs aussi variés que les industries chimiques, agroalimentaires, les laboratoires d'analyse médicale, les sciences de l'environnement. Le principe adopté est de relier les aspects pratiques de chaque méthode étudiée aux notions scientifiques qui l'expliquent. Abondamment illustré par plus de 250 figures et photos originales, ce livre est organisé en trois sections : les méthodes séparatives (les différentes techniques de chromatographie et d'électrophorèse), les méthodes d'analyse spectrale (RMN, IR, UV, fluorimétrie, fluorescence X, absorption et émission atomique), les autres méthodes (spectrométrie de masse, méthodes avec marquage, électrochimie). Quelques notions sur les statistiques et sur la préparation des échantillons sont données en complément. Dans cette nouvelle édition, le texte a été entièrement réécrit et mis à jour pour tenir compte des progrès technologiques les plus récents. Un chapitre a été ajouté, consacré aux méthodes d'analyse des éléments. En fin d'ouvrage, une liste de sites internet invite le lecteur à découvrir des démonstrations de matériels présentés dans le livre. Ce livre s'adresse aux étudiants des 1ers cycles universitaires (DEUG, DEUST, DUT) et de pharmacie. Il sera aussi utile aux étudiants des deuxièmes cycles orientés vers les sciences de la matière et aux personnels des laboratoires et des entreprises confrontés à tous niveaux à des problèmes d'analyse.

Specific Ion Mass Spectrometric Detection for Gas Chromatographic Pesticide Analysis

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Author :
Publisher :
ISBN 13 :
Total Pages : pages
Book Rating : 4.:/5 (114 download)

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Book Synopsis Specific Ion Mass Spectrometric Detection for Gas Chromatographic Pesticide Analysis by : Maynard B. Neher

Download or read book Specific Ion Mass Spectrometric Detection for Gas Chromatographic Pesticide Analysis written by Maynard B. Neher and published by . This book was released on 1974 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Gas Chromatographic Analysis

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Author :
Publisher : Elsevier
ISBN 13 : 1483220834
Total Pages : 802 pages
Book Rating : 4.4/5 (832 download)

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Book Synopsis Gas Chromatographic Analysis by : Gunter Zweig

Download or read book Gas Chromatographic Analysis written by Gunter Zweig and published by Elsevier. This book was released on 2013-10-22 with total page 802 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Methods for Pesticides and Plant Growth Regulators, Volume VI: Gas Chromatographic Analysis covers the topics pesticide analyses by gas chromatography. The book discusses the sample preparation, detectors, qualitative analyses, and formulation analyses, as well as gas chromatography of different classes of pesticides. The text also provides general information concerning specific insecticides, fungicides, herbicides, plant growth regulators, nematicides and soil fumigants, as well as analytical techniques other than gas chromatography. Toxicologists and people involved in agricultural research will find the book invaluable.